SDACM-IIIb Calorimeter
ATTENTION: Reliably earthing wire shall be provided for the instrument power socket.
1.1 Applications
The instrument is applicable for the determination of the calorific values of solid or liquid
combustibles in the coal and petroleum products in the fields of coal, electricity, paper
making, petrochemicals, cement, agriculture, animal husbandry, scientific research and
schools.
2.1 Makeup
SD
SD cntrol
Ignitor
computer
Electronic
Temp.control
displayer
control
O2
Agitation printer
bomb
3
7
Start the computer to enter the measurement and control software. When the test is
ready (oxygen bomb is properly connected, test parameters correctly input and the
water temperature in the internal and external barrels is up to the specification), the
system will automatically enter the test status. The temperature data is accurately
acquired through the probe and measurement and control electric circuit. The whole
test procedures are finished automatically based on the program convention and the
testing results will be calculated, printed out and saved automatically. During the
testing, in case of abnormal operation of some part of the system, clear prompt will be
shown for easy maintenance.
Attentions
During the installation and debugging of the instrument, the operator should
a
follow the instructions strictly.
During the water addition, the fibers or metallic wires shall not fall into the
b
external barrel to avoid instrument failure.
When the instrument is being installed , the chassis shall be earthed reliably
c
1
3 1Hardware environment
Basic configuration
CPU 1G
Memory>128MB
Display card standard VGA 800600 display mode
Hard disk 20G
Drive CDROM and 1.44M floppy drive
Other deviceMouse and keyboard, etc.
1
3 2 Soft environment
2Installation procedures
3
2
3 1 Preparation prior to the installation
a. The lab environment shall be in line with the requirement as described in Chapter
1.2
b. Check the instrument configuration against the shipping list to see if they are intact
c. Prepare about 30Kg distilled water or deionized water
d. Provide the analytical balance with 0.1mg sensibility and industrial balance with
1g sensibility and proper drying vessel;
e. Provide oxygen cylinder with oxygen and pressure up to the standard.
f. Provide the basic tools such as tweezers, scissors, spanners, screw drivers, pliers and
horn scoops, etc.
2
3 2 Hardware installation
2
3 1
Arrangement and connection
a. PCI interface card needs no jumper and the address can be assigned automatically. The
barrel number is defined as follows: The first interface card close to the display card is
1# barrel, the second interface card close to the display card is 2# barrel ,and so on. If
there are sufficient PCI slots, generally the first PCI slot close to the display card is not to
be used.
b. If there are many PCI interface cards, it is suggested to install the cards one by one, i.e.
first insert one interface card boot the computer install the driver as prompted by
the system power off the computer insert another interface card boot the
computer install the driver as prompted by the system.
c. In case PCI card and ISA card are simultaneously inserted into the computer
mainframethe system will preferentially identify the ISA card . For example, when
ISA card means 1# barrel, the first PCI card close to the display card means 2# barrel.
d. After the driver is installed , check in accordance with the procedures as follows
Start set up control panel system device manager Sundyclick +to view
the card identification name.
2
3 3 Software installation
1. Automatic installation
Run the Sundy.exe file ,the computer will be automatically rebooted several
times during the installation .One has to run repeatedly Sundy.exe file until the
shortcut icon SDACM-IIIb Heat Calorimeter is shown on the desktop
Upon the installation of the database MSDE ,right click the icon in the taskbar
on the lower right of the desktop MSSQL Server open SQL Server -
click Start /Continue - select "When start OS, automatically start service "
2.Manual installation
Since the measurement and control system of the SDACM-IIIb Heat
Calorimeter consists of measurement and control software main program
and data management( as described in details in Chapter IV and
V) ,independent from each other for the manual installation , the necessary
modules and main program of the measurement and control software are to be
separately installed as follows:
Install the necessary modules
Attention: When manual installation is selected, Necessary module
shall be installed first. During the module installation, if it is
prompted to Reboot the computer, the computer is to be
rebooted before carry out the next procedure .
aRun CD-ROM \Product measurement and control software \Install the
necessary module \IE60SP1\ie6setup.exe file
bRun CD-ROM \Product measurement and control software \Install the
necessary module \dotNetFramework\dotnetfx.exe file
cRun CD-ROM \Product measurement and control software \Install the
necessary module \dotNetFramework\langpack.exefile
dRun CD-ROM \Product measurement and control software \Install the
necessary module \MSDERel\setup.exe file, after installation, reboot the
computer.
eright click the icon in the taskbar on the lower right of the desktop MSSQL
Server - open SQL Server - click Start /Continue - select "When start OS ,
automatically start service "
f For the Windows98 Operating System, you need also run CD-ROM\
Product measurement and control software \Install the necessary module
\dcom98.exe file
Install the measurement and control software
In case the above modules are installed previously, direct run CD-ROM\
Product measurement and control software \Sundy.exe .During the installation,
one need only select Next step or YES, the program can automatically
finish the whole installation process after setting the installation option.
3 Operating method
3
3
3 1 Installation and use of the automatic oxygenator
Use
2
Open the valve of the oxygen cylinderThe oxygen pressure indicated by the high
pressure gauge of the relief valve should be > 5Mpaput the oxygen bomb onto the
oxygenator oxygen bomb locating tray to direct the oxygen bomb head at the
oxygenator air tap, press down the oxygenator handle. The required pressure is 2.8
3MPa (as indicated by the low pressure gauge ), oxygenation duration 15 60 seconds.
Slowly release the handle after sufficient oxygenation. Take out the oxygen bomb, then
one can see the valve core projected up, indicating the oxygen bomb oxygenated.
Precautions
a. Each day when the experiment is over, close the master oxygen valve and bleed the
oxygen from the air circuitMethodclose the oxygen cylinder valve , oxygenate the
oxygen bomb until the oxygen pressure gauge indicates zero.
b. No fire in the area where the oxygenator and oxygen cylinder are put.
c. Bending or twisting of the oxygenation duct is forbidden.
d. Regularly check the pressure gauge on the oxygenator and low pressure gauge on the
relief valve to see if the indicated values are in line with each other
e. No grease is to be used for the connecting nuts in the whole air circuit
f. After oxygenation, slowly release the oxygenator handle.
3
3 2 The use of the oxygen bomb
Attentions
a. Fire damper to short circuit the two electrode rod is prohibited,
b. Each time prior to mounting of the ignition wire, the ignition wire left over on
the junk ring or other foreign materials on the electrode rod
c. Over-pressure ogygenation (normal pressure is 2.8 3Mpa is prohibited, the
oxygenation duration should be relatively similar generally 15 60 seconds
d. Dont screw the oxygen bomb lid too tight , just to screw it in the right position
with a little more force
e. After the experiment is over, clean the bomb barrel and lid and dry them in the
air
f. Regular quality check is to be done to the oxygen bomb, and hydraulic
test( oxygen bomb may sent to Sundy Company for testing) should be made
minimum once a year.
3
3 3 On-line experiment
After the hardware and software are installed, on-line experiment may start .When there
is nothing abnormal, the installation is deemed as completed .Otherwise, check item by
item the hardware and software installation in accordance with the troubleshooting
method, correctly solve the problem or reinstall.
Attention: After the instrument debugging, components movement or pulling of the signal
wire is prohibited to avoid any failures.
Chapter Instrument Operating Instructions
1
4 Start-up and Exit of the Measuring and Control Software
1
4 1 Start- up
Way I : When the software is properly installed, shortcut is set up automatically on the
Windows desktop and menu item will be set up in Windows program package.
Directly click shortcut icon SDACM-IIIb Calorimeter or start from Start
->Program ->SDACM-IIIb Calorimeter.
Way II: Set item Enter Windows Automatic Run Program in the System Setup of the
measuring and control software to automatic start the measuring and control software
of SDACM-IIIb Calorimeter the nest time when you boot the Windows.
1
4 2 Exit
The measuring and control software is to be closed before exit the Windows or cut-off the
computer to ensure the experiment data and parameters file not destroyed.
Set Cut off the Computer when Exit in the in the System Setup of the measuring and
control software to automatically cut off the computer when exit the program.
The main forms of the measuring and control software for SDACM-IIIb Calorimeter
mainly consists of shortcut button bar ,forms and status bar.
The forms for SDACM-IIIb Calorimeter system ready to work is shown in Fig. 4-1
The forms for SDACM-IIIb Calorimeter system under testing is shown in Fig. 4-2.
2
4 1 System menu
1 System setting For details, see Fig. 4-3Setting Login Window Fig. 4-4
System Basic Setting Window and Fig 4-5 System Advanced Setting Window
Click System Setting button to login and enter the system parameter setting
form.
2. Expert Diagnosis For details ,see Fig. 4-6Instrument Diagnosis
Click Expert Diagnosis button to enter this form.
1. Data Processing
Click Data Processing button to login and enter this form.
2. Help For details , see Fig. 4-7Help
Click Help button to enter the system Help.
3. Exit the system
Click Exit button to exit the measuring and control system.
Attention When the computer is ON never pull out the plug board card to
avoid damage to the computer and the corresponding line CRD cards .
Fig 41
Fig 42
3 System setting
4
Fig 43
44
Description of the system basic setting options
4 Expert Diagnosis
4
The function of the Expert Diagnosis is to facilitate the debugging staff to detect the
instrument hardware, the user operation is invalid.
Fig.4-6
5 Date processing
4
The data processing system is aimed to manage the testing data in more efficient way. It
covers the data management on the heat capacity and calorific value. During the experiment,
it allows for access to the database. For details, see Chapter V.
6 Help
4
Fig.4-7
Click Help buttonthe information on the Revision of the measuring and control
software will appear as shown in Fig. 4-7. Press YES to enter the Help file of the measuring
and control software for SDACM-IIIb Calorimeter, press Cancelto come back to the main
form.
Experiment Preparations
1. Prepare the dry, fully cooled test purpose special crucible with constant mass
2. Prepare the qualified O2, O2 bomb, oxygenator and special rags
Boot the computerdouble click icon on the desktop SDACM-IIIb Calorimeter
Parameter setting
1 Open the System setting window to set the testing method.
2 Open the Sample parameter window to set the sample parameters (e.g. testing type).
3 Open the Data processing software to set
Experiment testing
1 Put the inner barrel (with water temperature adjusted) into the thermostatic tank, cover the barrel before
put the probe to the inner barrel ,then the prompt column should display Oxygen bomb connected .
2 Put in the sample mass and other parameters , the program will automatically enter the Testing status until
the experiment is over.
3 When the experiment is over, the program will enter the next sample testing Ready condition with the
procedures as above mentioned.
Data Save and Printing
1.When the experiment is over, the experiment data will be automatically saved into the database.
2.Click Data processing to enter Data management software to modify , delete and print the data ( In case of
automatic printing is set, the program will automatically print when the experiment is over otherwise, manual
printing is to be done).
.
Chapter V Data Management of the Measuring and Control Software
1 User Login
5
Fig.51
2 Main form
5
The main forms of the data management system of the SDACM-IIIb Calorimeter
consists of title bar, menu bar, shortcut bar, data display field, etc, which are described in
detail as follows:
Fig.52
Fig. 53
2
5 1 Main Menu
The main menu covers the conversion of the calorific value and colorific capacity ,
the colorific capacity data or calorific value data form is shown in Fig.5-2 or 5-3
respectively
2
5 2 Main Menu Setting
Fig 5 4
Basic setting
Fig 55
This page is for the setting of the print content, the tabular form, etc.
a. Print reportDuring print preview, the report will be displayed based on the
single-record format.
b. Print the parallel sampleDuring the print preview, test the parallel sample based on the
manual numbering of the currently checked records. In case the manual numbering is
not null and the parallel sample is satisfactory, the records of the parallel sample
decision conditions will be displayed.
c. Print the reportDuring the print preview, based on the report format display, two
kinds of calorific value reports are provided. One kind of calorific capacity report is
provided .During the calorific capacity print preview, no matter the report setting at
Default or Format I, the printing will be based on Default print.
d. Print assayerSelect this check box to print the assayer in Print Preview and Automatic
Print, otherwise the assayer not printed.
e. Print the procedure parametersSelect this item to print the system testing procedure
parameters in the Print Preview and Automatic Print
f. Automatically print the new dataSelect this item to automatically print the reports and
parallel sample when the calorific value or calorific capacity testing results are obtained.
For the printer without Paper Setup function (Such as laser printer), it is recommended
to cancel this option in order to save the paper.
g. Print standard, instrument code and oxygen bomb No.: The calorific value report form
is set at Format 2 or parallel sample pattern. Select this item to print the basic
standard, instrument code and oxygen bomb No.
h. Print copiesDuring the printing, print is done based on the set copies.
Advanced setting
Fig.56
Fig. 57
3. User managementThis option is to add, modify and delete the user and confirm the
permissionFor details, see Fig 5-8.
Fig.58
a. The user with 0 ID cannot be deleted, or cannot be modified to Inactive Status ,i.e.
False Status
b. It cannot modify ID or add the data of the same user name
c. The currently landed user cannot be deleted
d. The main program has selected a user and the test is on going, the user cannot be
deleted ,otherwise the data Save will fail
e. For the users with Permission ID > 9, they cannot login in the main program System
Setting
2
5 3 Edit the main menu (As shown in Fig. 5-9)
Fig.59
Modify Click and automatically open the Single-record Browse and enter the Edit
status
Delete the checked recordsDelete all checked records in the Multi--record Browse
Delete all records Delete all records in the Multi--record Browse
PrintPrint the checked records in the Multi--record Browse
Print previewPreview the records in the Multi--record Browse as shown in Fig.
5-10.
Fig.510
2
5 4 Main menu configuration
Fig.511
User menuPermission configuration for the current logged-in users as shown in Fig.
5-12
a. For the configuration of the current logged-in user permission
b. Directly select or cancel the menu item in User Menu Configuration click Renew
display to immediately renew the user menuSetting ,User Login ,
Configuration , User menu are always visible
c. Selecting User menu means that the user can directly configure own or others user
passwords and menu permissions. Thus, User menu permissions can be assigned
usually only to the system administrator
d. When the User menu is cancelled , if you want to Configure the User menu , the
identity has to be confirmed with the system administrator permissions
e. stands for the menu bar separator , only for display purpose
Fig.512
Fig. 513
2
5 5 Display the main menu As shown in Fig. 5-14
Fig. 514
b)When select this item, open the single-record browseas shown in Fig.5-14forms,
otherwise close the single-record browse display.
Save the current column width: save the column width in the modified current multi-
record browse window ;
2
5 6 Find the main menu as shown in Fig. 5-15
Fig. 515
Parallel sampleDisplay all current records identical with manual numbering, and
display the corresponding parallel sample message, such as average value and
precision
Barrel numberDisplay all day data of some barrel
Current recordDisplay the data identical with the manual numbering of the current
checked records, and the data of the same testing date
Day recordsDisplay all records tested on the same date with the that of the current
checked records;
All recordsTo display all records in the database
User-defined FindTo provide several ways for user-defined findas shown in Fig.
5-16
Fig.516
DeleteSelect in the left condition list a line of the condition records and click delete .
e. Select all recordsAfter selection, click Start to Find all records in the multi-record
Browse Tables will be displayed.
2
5 7 Help
1
6 Maintenance of the Thermostatic Tank
2
6 Oxygen Bomb Maintenance
a Every day before the test, the empty oxygen bomb shall be fully aerated and put
into the water for several minutes to see if the sealing property of the oxygen bomb is
good so as to ensure reliable testing results.
b Each time when the test is over, the oxygen components must be washed with
distilled water and dry the components with special towel
c In case of air leakage in the oxygen bomb, replace with stand-by ring seal.
Otherwise, the oxygen bomb cannot be used.
d In case of any thread breakage, the oxygen bomb service is prohibited.
e Regularly check the oxygen bomb quality, water pressure test should be done
minimum once a year (may sent to Sundy Company for the testing )
f Carefully take out and put in the oxygen bomb to avoid inner barrel damage due
to the collision.
g After use, the crucible should be cleaned and better to put it to the electric oven
for 3~5 min baking .After drying, the crucible should be cooled down before reuse.
a The test oxygen shall conform to Chinese standard GB213-200the use of the
electrolytic oxygen is prohibited. The oxygen cylinder should be placed in the area
up to the safety regulation.
b The oxygenator is to be put on the flat and sable working table.
c The oxygenator (include oxygen duct and relief valve) shall not be in contact
with various greases.
d The oxygen duct in the oxygenator should be protected against bending, torsion or
bumping.
e Open fire around the oxygenator is prohibited.
f In case the oxygen pressure in the oxygen cylinder is <5MPa, the oxygen should
be renewed. In case the oxygenation pressure in the oxygen bomb is > 3MPa, the
oxygen is to be evacuated and reinstall the oxygen bomb and reoxygenate the bomb.
The common instrument failures and simple maintenance are described. In case the users
fail to remedy the failures by themselves, please call up Sundy Company
Inner and external barrel temperature difference not up to the requirement Sample weight
not put in /oxygen bomb poor contact
n
Exit the measuring and control software, and reenter
When the failure is not remedied, please contact Sundy Company
Probe damaged
n
System set ignition failed , temperature rise set value too high The recommended set value
0.1?
n
Oxygen bomb external electrode short circuited
n
Oxygen bomb inner electrode short circuited
n
Not Oxygenated or insufficient oxygenation or sample not put in
n
Ignition wire not properly installed
n
Agitator refused to work or work with low efficiency
n
When the failure is not remedied, please contact Sundy Company