Designation: E 494 95 (Reapproved 2001) An American National Standard

Standard Practice for

Measuring Ultrasonic Velocity in Materials1
This standard is issued under the fixed designation E 494; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

This specification has been approved for use by agencies of the Department of Defense.

1. Scope 1.5 This standard does not purport to address all of the
1.1 This practice covers a test procedure for measuring safety concerns, if any, associated with its use. It is the
ultrasonic velocities in materials with conventional ultrasonic responsibility of the user of this standard to establish appro-
pulse echo flaw detection equipment in which results are priate safety and health practices and determine the applica-
displayed in an A-scan display. This practice describes a bility of regulatory limitations prior to use.
method whereby unknown ultrasonic velocities in a material
2. Referenced Documents
sample are determined by comparative measurements using a
reference material whose ultrasonic velocities are accurately 2.1 ASTM Standards:
known. C 597 Test Method for Pulse Velocity Through Concrete2
1.2 This procedure is intended for solid materials 5 mm (0.2 E 317 Practice for Evaluating Performance Characteristics
in.) thick or greater. The surfaces normal to the direction of of Ultrasonic Pulse-Echo Examination Instruments and
energy propagation shall be parallel to at least 63. Surface Systems Without the Use of Electronic Measurement
finish for velocity measurements shall be 3.2 m (125 in.) rms Instruments3
or smoother. E 797 Practice for Measuring Thickness by Manual Ultra-
sonic Pulse-Echo Contact Method3
NOTE 1Sound wave velocities are cited in this practice using the E 1316 Terminology for Nondestructive Examinations3
fundamental units of meters per second, with inches per second supplied
for reference in many cases. For some calculations, it is convenient to 3. Terminology
think of velocities in units of millimeters per microsecond. While these
units work nicely in the calculations, the more natural units were chosen 3.1 DefinitionsFor definitions of terms used in this prac-
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---

for use in the tables in this practice. The values can be simply converted tice, see Terminology E 1316.
from m/sec to mm/sec by moving the decimal point three places to the
left, that is, 3500 m/s becomes 3.5 mm/sec. 4. Summary of Practice
1.3 Ultrasonic velocity measurements are useful for deter- 4.1 Several possible modes of vibration can propagate in
mining several important material properties. Youngs modulus solids. This procedure is concerned with two velocities of
of elasticity, Poissons ratio, acoustic impedance, and several propagation, namely those associated with longitudinal (vl) and
other useful properties and coefficients can be calculated for transverse (vt) waves. The longitudinal velocity is independent
solid materials with the ultrasonic velocities if the density is of sample geometry when the dimensions at right angles to the
known (see Appendix X1). beam are very large compared with beam area and wave length.
1.4 More accurate results can be obtained with more spe- The transverse velocity is little affected by physical dimensions
cialized ultrasonic equipment, auxiliary equipment, and spe- of the sample. The procedure described in Section 6 is, as noted
cialized techniques. Some of the supplemental techniques are in the scope, for use with conventional pulse echo flaw
described in Appendix X2. (Material contained in Appendix detection equipment only.
X2 is for informational purposes only.)
5. Apparatus
NOTE 2Factors including techniques, equipment, types of material, 5.1 The ultrasonic testing system to be used in this practice
and operator variables will result in variations in absolute velocity
readings, sometimes by as much as 5%. Relative results with a single
shall include the following:
combination of the above factors can be expected to be much more 5.1.1 Test InstrumentAny ultrasonic instrument compris-
accurate (probably within a 1% tolerance). ing a time base, transmitter (pulser), receiver (echo amplifier),
and an A-scan indicator circuit to generate, receive, and display
electrical signals related to ultrasonic waves. Equipment shall
1
This practice is under the jurisdiction of ASTM Committee E07 on Nonde- allow reading the positions of Ak, As, At, Al (defined in 6.1.4
structive Testing and is the direct responsibility of Subcommittee E07.06 on
Ultrasonic Method.
2
Current edition approved January 15, 1995. Published March 1995. Originally Annual Book of ASTM Standards, Vol 04.02.
3
published as E 494 73. Last previous edition E 494 92a. Annual Book of ASTM Standards, Vol 03.03.

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and 6.2.4), along the A-scan base line within 60.5 mm (0.020
in.). For maximum accuracy, the highest possible frequency
that will present at least two easily distinguishable back
echoes, and preferably five, shall be used.
5.1.2 Search UnitThe search unit containing a search unit
that generates and receives ultrasonic waves of an appropriate
size, type and frequency, designed for tests by the contact
method shall be used. Contact straight beam longitudinal mode
shall be used for longitudinal velocity measurements, and
contact straight beam shear mode for transverse velocity
measurements.
5.1.3 CouplantFor longitudinal velocity measurements,
the couplant should be the material used in practice, for
example, clean light-grade oil. For transverse velocity mea-
surements, a high viscosity material such as resin or solid bond
shall be used. In some materials isopolybutene, honey, or other
high-viscosity materials have been used effectively. Most
liquids will not support transverse waves. In porous materials
special nonliquid couplants are required. The couplant must
not be deleterious to the material.
5.1.4 Standard Reference Blocks:
5.1.4.1 Velocity StandardAny material of known velocity,
that can be penetrated by the acoustical wave, and that has an
appropriate surface roughness, shape, thickness, and parallel-
ism. The velocity of the standard should be determined by
some other technique of higher accuracy, or by comparison
with water velocity that is known (see Appendix X2.5 and
Appendix X4). The reference block should have an attenuation
similar to that of the test material.
5.1.4.2 For horizontal linearity check, see Practice E 317.
6. Procedure
6.1 Longitudinal Wave VelocityDetermine bulk, longitu-
dinal wave velocity (v l) by comparing the transit time of a
longitudinal wave in the unknown material to the transit time
of ultrasound in a velocity standard (vk).
6.1.1 Select samples of each with flat parallel surfaces and
measure the thickness of each to an accuracy of 60.02 mm
(0.001 in.) or 0.1%, whichever is greater.
6.1.2 Align the search unit over each sample and obtain a
nominal signal pattern (see Fig. 1) of as many back echoes as
are clearly defined. The time base (sweep control) must be set
the same for both measurements.
6.1.3 Using a scale or caliper measure the distance at the
base line between the leading edge of the first back echo and
the leading edge of the last back echo that is clearly defined on
the known and unknown sample. For better accuracy, adjust the
amplitude of the last back echo by means of the gain control to
FIG. 1 Initial Pulse and 7 Back Echoes
Copyright ASTM International
Reproduced by IHS under license with ASTM
E 494
approximately the same height as the first back echo, after the
position of the leading edge of the first back echo has been
fixed. This allows more accurate time or distance measure-
ments. The position of the leading edge of the last back echo is
then determined. The signal has traversed a distance twice the
thickness of the specimen between each back echo. The signal
traversing the specimen and returning is called a round trip. In
Fig. 1 the signal has made six round trips between Echo 1 and
Echo 7. Count the number of round trips from first echo used
to the last echo measured on both samples. This number will be
one less than the number of echoes used. Note that the sample
thickness, number of round trips, and distance from front to last
back echo measured need not be the same.
6.1.4 Calculate the value of the unknown velocity as fol-
lows:
v1 5 ~Ak nl tl vk!/~Al nk tk! (1)
where:
A k = distance from first to Nth back echo on the known
material, m (in.), measured along the baseline of the
A-scan display,
nl = number of round trips, unknown material,
t l = thickness of unknown material, m (in.),
vk = velocity in known material, m/s (in./s),
A l = distance from the first to the Nth back echo on the
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
unknown material, m (in.), measured along the
baseline of the A-scan display,
n k = number of round trips, known material, and
tk = thickness, known material, m (in.).
NOTE 3The units used in measurement are not significant as long as
the system is consistent.
6.2 Transverse VelocityDetermine transverse velocity (vs)
by comparing the transit time of a transverse wave in an
unknown material to the transit time of a transverse wave in a
material of known velocity (vt).
6.2.1 Select samples of each with flat parallel surfaces and
measure the thickness of each to an accuracy of 60.02 mm
(0.001 in.) or 0.1 %, whichever is greater.
6.2.2 Align the search unit (see Fig. 1) over each sample and
obtain an optimum signal pattern of as many back echoes as are
clearly defined. The time base (sweep control) must be the
same for both measurements.
6.2.3 Using a scale or caliper measure the distance at the
base line between the leading edge of the first back echo and
the leading edge of the last back echo that is clearly defined on
the known and unknown sample. For better accuracy, adjust the
amplitude of the last back echo by means of the gain control to
approximately the same height as the first back echo, after the
position of the leading edge of the first back echo has been
fixed. This adds high-frequency components of the signal
which have been attenuated. Then determine the position of the
leading edge of the last back echo. Count the number of round
trips from first echo used to the last echo measured on both
samples. This number will be one less than the number of
echoes used. Note that the sample thickness, number of round
trips, and distance from first to last back echo measured need
not be the same.
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 E 494
6.2.4 Calculate the value of the unknown velocity as fol- 7.1.2 Transverse Wave:
lows: 7.1.2.1 At = _________m (in.)
vs 5 ~A t ns ts vt!/~As nt tt! (2) 7.1.2.2 ns = _________
7.1.2.3 ts = _________m (in.)
where: 7.1.2.4 vt = _________m/s (in./s)
At = distance from first to Nth back echo on the known 7.1.2.5 As = _________m (in.)
material, m (in.), measured along the baseline of the 7.1.2.6 nt = _________
A-scan display, 7.1.2.7 tt = _________m (in.)
ns = number of round trips, unknown material, 7.1.2.8 vs (using Eq 2) = ___m/s (in./s)
ts = thickness of unknown material, m (in.),
7.1.3 Horizontal linearity
vt = velocity of transverse wave in known material, m/s
(in./s), 7.1.4 Test frequency
As = distance from the first to the Nth back echo on the 7.1.5 Couplant
unknown material, m (in.), measured along the base- 7.1.6 Search unit:
line of the A-scan display, 7.1.6.1 Frequency
nt = number of round trips, known material, and 7.1.6.2 Size
tt = thickness, known material, m (in.). (See Note 3). 7.1.6.3 Shape
7.1.6.4 Type
7. Report 7.1.6.5 Serial number
7.1 The following are data which should be included in a 7.1.7 Sample geometry
report on velocity measurements: 7.1.8 Instrument:
7.1.1 Longitudinal Wave: 7.1.8.1 Name
7.1.1.1 Ak = _________m (in.) 7.1.8.2 Model number
7.1.1.2 nl = _________ 7.1.8.3 Serial number
7.1.1.3 tl = _________m (in.) 7.1.8.4 Pertinent control settings
7.1.1.4 vk = _________m/s (in./s)
7.1.1.5 Al = _________m (in.) 8. Keywords
7.1.1.6 nk = _________ 8.1 measure of ultrasonic velocity; nondestructive testing;
7.1.1.7 tk = _________m (in.) ultrasonic properties of materials; ultrasonic thickness gages;
7.1.1.8 vl (using Eq 1) = ___m/s (in./s) ultrasonic velocity

APPENDIXES

(Nonmandatory Information)

X1. FORMULAS

X1.1 Using the technique of this practice will give results r density, kg/m3 (or lb/in.3),
=
in some instances which are only approximate calculations. vl =
longitudinal velocity, m/s (or in./s),
The determination of longitudinal and transverse velocity of vs =
transverse velocity, m/s (or in./s), and
sound in a material makes it possible to approximately calcu- E Youngs modulus of elasticity, N/m 2 (or lb/in.2) (see
=
late the elastic constants, Poissons ratio, elastic moduli, Notes X1.2 and X1.3).
acoustic impedance, reflection coefficient, and transmission X1.1.3 Acoustic Impedance (see Note X1.3):
coefficient. In this Appendix, the formulas for calculating some z 5 r vl
of these factors are as follows (see Note X1.1):
where:
X1.1.1 Poissons Ratio: z = acoustic impedance (kg/m2 s (or lb/in.2 s)).
s 5 @1 2 2~vs/vl! 2#/2@1 2 ~vs/vl! 2# X1.1.4 Shear Modulus (see Note X1.3):
where: G 5 r vs 2
s = Poissons ratio, X1.1.5 Bulk Modulus (see Note X1.3):
vs = ultrasonic transverse velocity, m/s (or in./s), and
vl = ultrasonic longitudinal velocity, m/s (or in./s). K 5 r @vl 2 2 ~4/3!vs 2#
X1.1.2 Youngs Modulus of Elasticity: X1.1.6 Reflection Coeffcient for Energy (R):
E 5 ~r vs 2 ~3v l 2 2 4v s 2!#/~vl2 2 v s 2! R 5 ~Z 2 2 Z1! 2/~Z2 1 Z 1! 2

where: where:
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---

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Z 1 = acoustic impedance in Medium 1, and
Z2 = acoustic impedance in Medium 2.
X1.1.7 Transmission Coeffcient for Energy (T):
T 5 ~4Z 2Z1!/~Z2 1 Z1! 2
NOTE X1.1The dynamic elastic constants may differ from those
determined by static tensile measurements. In the case of metals,
ceramics, and glasses, the differences are of the order of 1 %, and may be
X2. IMPORTANT TECHNIQUES FOR MEASURING ULTRASONIC VELOCITY IN MATERIALS
X2.1 Introduction
X2.1.1 Several techniques are available for precise mea-
surement of ultrasonic velocity in materials. Most of these
techniques require specialized or auxiliary equipment.
X2.1.2 Instruments are available commercially which auto-
matically measure sound velocity or time interval or both.
There is a growing list of manufacturers who make ultrasonic
instruments, including pulser, receiver, and display designed
specifically for making these measurements automatically or
which can be used for these measurements even though
designed primarily for other measurements (for example,
thickness gages).
X2.1.3 Various methods have been introduced to solve the
problem of the accurate measurement of time interval or
number of waves in the specimen. It would be beyond the
scope of this Appendix to attempt to include all these tech-
niques. However, it is considered of value to those using this
practice to know some of these techniques. This Appendix will
be useful to those who have more refined equipment or
auxiliary equipment available and to those who wish more
accurate results.
X2.1.4 This Appendix will include some techniques that are
only suitable for the laboratory. It is only under strictly
controlled conditions such as are available in the laboratory
that the greatest accuracy can be achieved. Such measurements
may be slow and require very carefully prepared specimens. A
list of references (1-28)4 is provided for more detailed infor-
mation.
X2.2 Special Features Built Into the Ultrasonic
Equipment
X2.2.1 Ultrasonic equipment is available that provides
means adequate for the measurement of acoustic wave propa-
gation with respect to time.
X2.3 Precision Oscilloscope
X2.3.1 An auxiliary precision cathode ray oscilloscope can
be used to observe the echo pattern. Using the precision
standardized horizontal display of the oscilloscope, the transit
time between successive multiple back reflections is deter-
mined. Calculate velocity as follows:
Velocity ~m/s ~or in./s!! 5 @2 thickness ~m or in.!#/@Time ~s!#
4
The boldface numbers in parentheses refer to the list of references appended to
this practice.
Copyright ASTM International
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E 494
corrected by known theoretical formulas. For plastics the differences may
be larger, but can be corrected by correlation.
NOTE X1.2Conversion factor: 1 N/m2 = 1.4504 3 10 4lb/in.2.
NOTE X1.3When using pounds per cubic inch for density and inches
per second for velocity, results must be divided by g (acceleration due to
gravity) to obtain results in pounds per square inch for E, G, or K and also
to obtain results for Z in pounds per square inch per second. Acceleration
due to gravity (g) = 386.4 in./s s.
X2.4 Electronic Time Marker
X2.4.1 An accessory is frequently available that displays
one or more visual marks, usually a step, on the display of the
basic instrument. It is usually superimposed on the standard
echo pattern. The mark is moved using a standardized control.
The control reads time directly in microseconds.
X2.4.2 The technique is to align the step on the display, first
with the first back reflection, and then, using the second
marker, if available, with the second back reflection. Based on
control readings at both instances, the elapsed time for a round
trip through the specimen is determined. (Calculation is the
same as in X2.3).
X2.5 Ultrasonic Interferometer (Velocity Comparator)
X2.5.1 The measurement of ultrasonic velocity is carried
out by comparing transmission times of a pulse in a specimen
and in the comparison travel path. The ultrasonic velocities in
liquids (for example, water) are well known and consequently
the velocity in the specimen can be determined with an
accuracy of about 0.1 %.
X2.5.2 In practice, the echo in the specimen is made to
coincide with the echo from the interferometer travel path
which is obtained by altering the latter to the point of
interference. The ultrasonic velocities of the specimen and
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
interferometer liquid are in the ratio of their lengths and these
two quantities must be exactly measurable.
X2.5.3 A normal probe is clamped to the open tank by
means of a clasp on one side. The frequency of the probe
should be equal to that which is required for the specimen. The
attenuation member must be inserted between the interferom-
eter probe and the cable. It serves to change the height of the
interferometer echo independently of other conditions of test.
X2.5.4 A reflector dips into the tank containing the liquid
and is held on an adjustable mechanism so that it cannot be
tilted. This mechanism can be moved to and fro rapidly by
disengagement. The fine adjustment is carried out by means of
a spindle. One complete revolution of the spindle changes the
travel path by 1 mm. One scale division of the spindle knob
represents 1100 mm (0.0004 in.).
X2.5.5 The tank must be filled with liquid in which the
ultrasonic velocity is known. In the case of water at 20C,
velocity = 1483.1 m/s. The temperature coefficient is Dv/Dt
= + 2.5 m/s C. A check of the temperature in the case of
water is therefore absolutely necessary (see Appendix X4).
X2.5.6 Mixtures can also be used, for example, water
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alcohol (18% weight percentage), whose temperature coeffi-
cient is zero at room temperature.
X2.5.7 Calculate velocity as follows:
Velocitywater ~m/s! 3 Thickness x ~m!
Velocityx ~m/s! 5 Distancein water ~m!
or
Velocitywater ~in./s! 3 Thicknessx ~in.!
Velocityx ~in./s! 5 Distancein water ~in.!
X2.6 Pulse Velocity Through Concrete (see Test Method
C 597)
X2.6.1 Frequency of pulse generator 10 to 50 kHz
Repetitive pulses at rate not less than 50/s.
X2.6.2 Press the faces of the search units against the faces
of the concrete after establishing contact through a coupling
medium. Wetting the concrete with water, oil, or other viscous
materials may be used to exclude entrapped air from between
the contact surfaces of the diaphragms of the search unit and
the surface of the concrete. Measure the length of the shortest
direct path between the centers of the diaphragms and the time
of travel on the A-scan display by aligning the strobe marker
pulse opposite the received wave front and reading the stan-
dardized dial, or by counting the number of cycles of the
timing wave between the transmitted and received pulse.
X2.7 Pulse Echo Twin-Probe Method
X2.7.1 This method uses a single-probe housing containing
two elements: one a sender, the other a receiver.
X2.7.2 Since ultrasonic velocity measurements are princi-
pally measurements of time, based on the thickness of a
specimen, and since many thickness measuring instruments
successfully measure thickness to a high degree of accuracy
using this method it seems appropriate to include this method
of velocity measurement in the practice.
FIG. X2.1 Instrument Setup to Avoid Errors Due to Parallax
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
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NOTE X2.1With the twin-probe method the pulse-echo transit time is
a non-linear function of specimen thickness, which may introduce
significant errors when that technique is used for velocity measurements.
The non-linearity is discussed in Practice E 797. Errors in velocity
measurement can be minimized by use of a reference block having both
velocity and thickness nearly equal to that of the specimen to be measured.
Single search unit systems are generally more suitable for precision
velocity measurements.
X2.7.3 All instruments where the twin-probe method of
thickness measurement is recommended, including A-scan
display units as well as meter read-out units, have precisely
standardized scales. The parallax problem is removed from
many of the A-scan display units since the scale is engraved on
the inside face of the display or is integral with the output
signal. Parallax is not a major problem with meter read-out
units or digital read-out units.
X2.7.4 Most twin-probe thickness measuring instruments
use the first echo for measurement read-out. Thus the test
ranges are usually fixed and precisely standardized. There is no
need to produce several back echoes to obtain an average
transit time.
X2.7.5 Specimens with curved surfaces present less mea-
suring problems as the first back echo is more representative of
depth or time than a later back echo, say the fifth from a tube
wall. In small diameter tubing the error may be greater than for
equivalent flat specimens.
X2.7.6 Procedure:
X2.7.6.1 Standardize the instrument and probe on a steel
step block of known velocity. By adjustment of sweep delay
and range controls, ensure that thickness readings for two or
more thicknesses (high and low) occur at their proper distances
(Fig. X2.1). The instrument and probe are properly standard-
ized for (1020 or 1095) steel at 5900 m/s (2.32 3 10 5 in./s).
X2.7.6.2 Measure the thickness of part with unknown ve-
locity without changing sweep or range controls on the
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instrument. Check the actual thickness of the test area with
calipers or a micrometer.
X2.7.6.3 Calculate unknown velocity as follows:
actual thickness
Vx 5 V steel 3 indicated thickness
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
where:
Vx = unknown velocity.
X2.8 Harmonic Wave Method (Zero Method)
X2.8.1 Wall thickness measurement by means of ultrasonic,
echo-sounding instruments will become inaccurate if only a
few echoes can be utilized because of either high absorption,
corrosion, or unfavorable radiation geometry. In such cases, the
accuracy of the results can be improved by the tuning of the
wall thickness meter to the harmonic waves of the echo
frequency (harmonic wave method).
X2.8.2 Up to now the interferometer method has been used
for the precision measurement of sound propagation. Further
development of the harmonic wave method can replace the
rather complicated and time-consuming interferometer method
in all those cases where the ultimate accuracy of the latter is not
required. Under normal conditions, a measuring accuracy of
0.5 % or better can be obtained with the so-called zero-
method.
X2.8.3 A modification of the method utilizes bursts of radio
frequency (rf) radiated from a search unit into a long buffer rod
and then into the sample, which is a few wavelengths thick.
The buffer rod is long enough to contain the entire rf bursts,
while the burst is long enough to occupy the three round-trips
in the specimen. Thus the burst interferes with itself as it
reverberates within the specimen. One characteristic echo
pattern occurs when the round-trip distance in the specimen is
equal to an odd number of half-wavelengths; an even number
gives a different pattern. The two patterns alternate as the rf
frequency is changed. One plots phase versus frequency in
units of cycles versus MHz. One cycle of phase occurs for each
repetition of one of the characteristic patterns; between the two
patterns there is 12 cycle of phase. The slope of the phase
versus frequency line is the delay time t in microseconds, and
for a specimen of thickness L, the velocity is
v 5 2L/t
X2.9 Phase Comparison Method
X2.9.1 This method consists of superimposing the echoes of
two pulses which have made different numbers of round trips.
If the echoes are made exactly in phase by a critical adjustment
of frequency, the expression for phase angles may be written
as:
g 2 @~2L Wn!/v# 5 22 pn
where:
v = velocity of propagation,
Wn = 2 p times resonant frequency (fn),
L = thickness,
n = number of waves, and
g = phase angle due to the seal between the search unit
and the specimen.
Consequently, the velocity is expressed by:
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v 5 ~2L fn!/@n 1 ~g/2p!#
X2.9.2 It has been experimentally proven that size and
shape effects are reduced to effectively zero whenever there are
at least 100 wave lengths of sound in the specimen thickness.
High frequencies (10 to 20 MHz) are generally used to
minimize this effect.
X2.9.3 The main advantage of the phase comparison
method is the fact that the absolute velocity can be determined
very accurately without the error introduced from coupling,
since the search unit coupling effect can be evaluated. This
method also makes it possible to measure the velocity on a very
small specimen with linear dimensions as small as 2 mm (0.08
in.).
X2.10 Pulse Superposition Method
X2.10.1 This method uses an rf pulse applied to the search
unit at the intervals approximately equal to the round-trip delay
time of waves traveling in the specimen. In order to observe the
superimposed echoes just after the last applied pulse, a few
applied pulses are omitted periodically. When the echoes are
brought into phase adjusting the time spacing T between
signals, a maximum in the resulting pulse amplitude occurs. In
this condition, the following equation is satisfied:
d 5 ~T/p! 2 ~L/f! @m/p 2 ~g/2p!#
where:
d = round trip delay time,
f = rf frequency in the pulse,
m = an integer which may take on both positive and
negative values, and
g = a phase angle associated with wave reflected at the
search unit end, and
p = an integer (1, 2, 3. . .).
Since T is approximately some multiple of the round-trip
delay time d, the applied pulse occurs once for every round trip
delay for p = 1. Usually, a number of measurements of T at
different frequencies between f, the resonance frequency of the
search unit, and 0.9 fr are made to obtain the difference in T
between fr and another frequency f. The negative value of DT
that is smallest in magnitude corresponds to n = 0; except for
specimens of very low mechanical impedance, the delay time
is then given by d = T + (g/2pf). The velocity in the sample is
V = 2 L/d, where L is the sample length.
X2.10.2 The advantage of this particular method is that the
coupling to the search unit is taken into account so that this
method is well suited to measurements aimed at pressure and
temperature variations. With this method, the effect of coupling
between search unit and specimen can be made negligibly
small. So far as the accuracy of this method is concerned, it is
within a few parts in 105 in ideal conditions, while that of the
phase comparison in X2.9 is within one part in 10 4. In this
method, however, it is possible to send a strong signal into the
specimen, so that the velocity measurement can be made even
if the attenuation is high.
X2.10.3 The limitation of both techniques is expected to
depend on various factors besides porosity, such as grain size
and grain boundary conditions.
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X2.11 Phase Velocity by Pulse-Echo-Overlap Method
X2.11.1 In this method, pairs of echoes are compared by
driving the x-axis of a viewing oscilloscope at a frequency
equal to the reciprocal of the travel time between the echoes.
By choosing the correct cyclic overlap for the rf within the
echoes by the DT method explained in X2.10, accurate mea-
surement of ultrasonic phase velocity can be made. When
corrections for the phase advance due to ultrasonic diffraction
are applied to the travel times between various pairs of echoes,
the accuracy of the average round-trip travel time is improved.
Delay times are accurate to 0.2 ns or better, which may be as
low as 5 parts in 10 6 in some cases. For dispersive materials,
the group delay may be obtained by overlapping the rectified
and detected envelopes of Gaussian (bell curve-shaped rf
bursts, which have narrow bandwidths. Thus, group velocity
may be measured. In nondispersive materials (most solids),
broadband digital pulses may be used instead of rf bursts.
X2.12 Sonic Resonance
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
X2.12.1 The dynamic resonance method, or the sonic
method, has been developed to the point that this technique can
be considered a standard method of obtaining sonic velocity
and elastic constants of solids. The flexural, transverse, and
torsional resonance frequencies of a solid body are determined.
From these values, the velocities can be computed.
X2.12.2 The advantage of this method is its convenience
and simplicity of the measurement without losing a high degree
of accuracy. It is possible by this method to determine the
elastic moduli of very porous aggregate compounds.
X2.12.3 The disadvantage of this method arises only from
the limitation on the size of the specimen to be examined.
When the length becomes shorter than 3 in. (76 mm), the
torsional fundamental resonance frequency of a material of
high elastic moduli exceeds 40 kHz, so that special equipment
and experimental techniques are required to obtain accurate
results. Moreover, all three dimensions (length, width, and
thickness) are critically involved in the calculation of the
elastic moduli from the resonance frequency. From a practical
point of view, it is quite difficult to fabricate small specimens
with a uniform cross-section dimension.
X2.12.4 Another problem to be considered is the shape
correction factor in the equation relating to the elastic moduli
to the resonance frequency. It has been recommended that for
rectangular specimens, the ratio of length to either cross-
sectional dimension should not be less than three to one. When
accurate values within 0.1 % are required, the ratio is prefer-
ably not less than six to one. Therefore, it becomes difficult to
determine the elastic moduli of specimens in massive structure.
X2.12.5 The sonic resonance technique has been used for
measurements up to 3000C.
X2.13 Momentary Contact Pressure Coupling Technique
X2.13.1 Measurements of longitudinal and shear-wave ve-
locity from room temperature to beyond 2000C have been
made by the technique developed by Carnevale and Lynnworth
(1).4 In this technique, measurements are made by momentarily
pressure-coupling 1-MHz longitudinal and shear-wave pulses
through a specimen and measuring the transit time (and
amplitudes too, if attenuation is to be determined). Measure-
Copyright ASTM International
Reproduced by IHS under license with ASTM
E 494
ment of longitudinal and shear-wave velocity is accurate to
about 1 %. The test specimen is a cylinder at least five
wavelengths in diameter by several centimetres long. Dimen-
sional requirements are easily met. Accordingly, sample prepa-
ration and moduli determinations are relatively simple. The
momentary-contact method is also applicable to measurement
of thickness of tubing, centerline pipe flaws in billets,
internal temperature and other characteristics of materials at
high temperature, typically 1000C.
X2.14 Notched-Bar and Stepped-Wire Techniques
X2.14.1 These techniques are applicable to bulk specimens
typically 1 to 3 cm in diameter by several centimetres long, or
to slender specimens less than or equal to 3 mm in diameter by
several centimetres long. Specimens are typically tested from
room temperature to the highest temperature of interest.
X2.14.1.1 The bulk specimen is an extension of the buffer
rod, but of smaller diameter. The diameter change creates a first
echo. The free end creates the second echo. With suitable
geometry, a longitudinal wave can be partly mode-converted
within the specimen, yielding both longitudinal and shear wave
echoes, from which both moduli and Poissons ratio are
determined. The upper temperature limit is usually imposed by
heat conduction into the buffer, or by attenuation in the buffer
at the test frequencies normally employed, approximately 1 to
10 MHz.
X2.14.1.2 The slender specimen may be an extension of the
lead-in wire buffer, but more often one uses a given buffer (for
example, tungsten wire, 1 mm in diameter by 1 m long) with
a variety of different specimens. This technique is especially
convenient for fibers of diameter much less than 1 mm, and
also for whiskers of this diameter, and lengths less than 1 cm.
Using a Joule-Wiedemann magnetostrictive search unit, exten-
sional and torsional pulses of approximately 0.1 MHz center
frequency are launched simultaneously and propagate nondis-
persively and without mode conversion down the buffer. But
due to their velocity difference, these modes are clearly
separated by the time they reach the specimen. Therefore one
can readily arrange to determine both velocities and therefore
Youngs and shear moduli and Poissons ratio. At high tem-
perature, the slender buffer produces only a small heat loss.
The specimen itself rapidly follows the furnace temperature. In
some cases, electrical self-heating of the specimen has been
used to determine sound velocity under cyclic conditions, and
at the melting point of refractory wires.
X2.15 Continuous Wave (CW) Phase-Sensitive
Techniques
X2.15.1 A system for measuring phase in a specimen on a
cw basis consists of a lock-in amplifier, an input search unit,
and an output search unit arranged for transmission through the
specimen. The amplifier contains a cw frequency source for the
input search unit. As frequency is varied, the phase meter of the
phase-lock amplifier registers zero (null) for every 180 phase
change. Thus every other zero-crossing is a cycle of phase f.
A plot is made of phase in cycles versus frequency in
megahertz. The slope of this curve is the group delay t g in
microseconds from which the group velocity is found by the
formula:
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v g 5 L/tg
X2.15.2 To study materials with this system, the ideal
specimen is either an unbounded plate tested through its
thickness, or a thin wire (diameter of d) tested along its length.
In the first case, sidewall effects are nonexistent. In the second
case, sidewall effects give rise to the first longitudinal mode
only, and it is nondispersive as long as l is much greater than
d. With specimens of aspect ratio nearer unity (for a cube, this
ratio is exactly unity), the multiplicity of modes in the structure
can obscure the material parameters. Then the measurement
becomes merely qualitative. Comparative measurements on
specimens of identical shape and size could be made, however.
X2.15.3 The method is very useful in highly attenuating
specimens in which echoes cannot be observed, that is, for a
material loss of 20 dB or higher in one pass through the
specimen. Then the phase is monotonic in frequency, offering
unambiguous readings. Both dispersive and nondispersive
materials can be tested. Nondispersive materials show no
variation of tg with frequency (that is, f is a straight line versus
frequency), and then the group velocity is equal to the phase
velocity.
X2.16 Alternative Method for Measuring Velocities of
Materials
X2.16.1 An alternative method to that used in this recom-
mended practice, but in which provisions have been made to
(1) eliminate errors due to parallax, (2) minimize errors due to
imperfect sweep linearity, and (3) use one mode velocity in the
reference block as the known velocity for all measurements, is
included as a useful technique for measuring ultrasonic veloc-
ity in materials.
X2.16.2 Velocity is distance traveled per unit of time;
therefore, time (which is displayed on the ultrasonic pulse echo
instrument screen as horizontal displacement) equals distance
divided by velocity. Calibrating time with multiple reflections
of a piece of T thick material (distance or length ultrasonic, L)
of known longitudinal velocity (Vl) gives distance divided by
velocity:
Lu/Vl 5 time
Setting an equal time in another material whose t thickness
can be measured, we can drop the reference to time. This
permits us to measure velocity by the ratio of distance to
velocity:
Lu/Vl 5 L m/Vx or Vx/Vl 5 L m/Lu.
Since these are ratios, we can state velocities in centimetres
per second and lengths in inches or other units as long as we
keep both velocities in the same units and both lengths in the
same units. The equation can be simplified to:
Vx 5 V l Lm/Lu
where:
Vx = velocity in a measured sample (longitudinal or shear
depending on which search unit is used on the
measured sample),
Vl = known longitudinal velocity in the reference block (a
straight beam longitudinal wave search unit is used to
standardize time),
Copyright ASTM International
Reproduced by IHS under license with ASTM
E 494
Lm = measured length of physical path through the mea-
sured sample, and
Lu = ultrasonic length of equal time path through the
reference block.
Restated in the general terms of the figure, the velocity is:
Vx 5 V l @nt/~NT 1 reading!#
where:
n = number of measured sample back reflections,
t = thickness of the measured sample,
N = number of standardization back reflections before the n
back reflections, and
T = thickness of the reference block reading in direct
standardized distance units from the Nth indication to
the nth indication.
This measurement may be accomplished in the following
steps:
X2.16.2.1 Measure thickness T of the reference sample and
thickness t of the sample to be measured using a micrometer or
caliper with capability to accurately read 60.0025 mm (0.0001
in.).
X2.16.2.2 Rub a pencil on the fine scale (for example, 1 mm
or 1/32-in. divisions) on an engraved scale (such as the steel
scale in a combination square set). Lift the standardization
from the scale with a strip of transparent tape. Attach to the
display of the instrument as shown in Fig. X2.1. Attach a
second scale tape to the screen cover. (Superimposing the two
scales eliminates errors in reading caused by misalignment of
the indication scale and your eye.)
X2.16.2.3 Attach a straight beam search unit to the instru-
ment. The search unit wave mode determines what velocity
will be measured. For example, a g cut quartz, whose major
motion is face shift parallel to the contact surface, will produce
a straight beam shear wave. Couple the search unit to the
sample to be measured with oil or glycerin (the more viscous
liquid, isopolybutene, provides improved coupling for shear
wave measurement). Adjust instrument controls to provide the
largest number of clear back reflections with the reject (clip-
ping, threshold) control adjusted to provide maximum ampli-
tudes. Measurements should not be attempted on less than two
back reflections and it is rarely necessary to use more than ten
back reflections. Five back reflections provide good accuracy
for velocity measurement. Mark the sweep line at the left edge
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
of the nth indication with a grease pencil (5t) to dark indication
if the sweep is adjusted as shown on the top screen in Fig.
X2.2.
X2.16.2.4 Read the number (N) of back reflections between
the initial pulse and the grease pencil mark. Delay the Nth back
reflection to position its left edge at the first whole inch mark
on the scale. Sweep control adjust the N + 1 back reflection to
position its left edge at a distance equal to the thickness (T) of
the standardized sample from the N back reflection. (Delay and
sweep must be readjusted two or three times to attain N
position at the first even inch mark on the scale and T spacing
on the scale between N and N + 1 back reflections.) Mark
amplitudes of N and N + 1 on the screen with a grease pencil
and connect the two points with a straight line.
X2.16.2.5 Couple the search unit to the sample to be
measured. Adjust sensitivity (gain) to set the amplitude of back
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FIG. X2.2 Instrument Setup for Reading
reflection n on the N to N + 1 amplitude line. Read distance
from the first even inch mark to the sweep line point at the left
edge of back reflection n; this is the reading.
X2.17 Through TransmissionPulse Echo
X2.17.1 The through-transmission technique is suitable for
usage in situations involving specimen surfaces that are not
ideally flat and parallel and also materials that are highly
attenuating. This technique, which utilizes more than one
search unit, does not require back reflections on a linear time
axis.
X2.17.2 In the through-transmission method, if one can
receive the pulse from the transmitting search unit, then a
velocity measurement is possible provided the thickness can be
determined.
X2.17.3 By adding an oscilloscope, one can measure more
accurate time readout. The method here is to view the output
pulses on the expanded r-f component of the pulse which can
be used as a reference point to locate the pulse on the time axis
which has been appropriately standardized by a reference
standard.
X2.18 Velocimetry Methods Independent of Thickness
X2.18.1 Most ultrasonic velocimetry methods are based on
an equation of the form:
V 5 x/t
where:
V = velocity,
--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
Copyright ASTM International
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x = ultrasonic path length (that is, x = thickness, for
through-transmission, or x = twice the thickness, for
pulse-echo), and
t = transit time.
In contrast to these methods, there are several other methods
for measuring V without requiring knowledge of x. Thus, they
may be appropriate when it is not convenient to determine x;
for example, when only one surface is accessible.
X2.18.2 Critical Angle ReflectivityThis method is based
on Snells law. It involves measuring one of several critical
angles, depending on which wave type (longitudinal, shear,
Rayleigh, etc.) is of interest. Denoting the velocity of interest
as V2, Snells law gives V2 in terms of the velocity V 1 and the
measured initial angle of incidence u1c in an adjacent medium
(usually water) as follows:
V2 5 V1/sin u1c
This method has been described in greater detail by Rollins
(2) and by Becker (3).
X2.18.3 Differential Path or Differential Angle:
X2.18.3.1 This method, of limited use (4), is also based on
Snells law, and may be considered when it is not convenient
to measure x or u1c. It may be understood by applying Snells
law twice, for two different angles of incidence. Let the
incident angles be denoted u 1a and u 1b. Consider the two
refracted rays of like mode in Medium 2, which will travel
along different paths at refracted angles u 2a and u2b. They will
be reflected after traveling in Medium 2 for intervals tp and tq,
respectively (tp and tq are transit time one way). Again denoting
the velocity in Medium 1 as V 1, if we define A |Cc sin u1a/V1
and B |Cc sin u1b/V1, it may be shown that, for isotropic media,
1 2 ~tp/tq!2
V2 5
B 2 A 2 ~tp/t q!2
2
As a special simplifying case, we may let u1a = 0 (normal
incidence). Then A = 0 and
V2 5 ~1/B!=1 2 ~t p/tq!2
X2.18.3.2 The practical difficulty stems from trying to
measure tq directly. Of perhaps academic interest, one might
determine tq by timing the modulation of a laser beam by the
echoes, where the laser in effect monitors at least one surface
of the specimen. This would, of course, be limited to wedges or
specimens, or both, that were optically transparent, and would
be a relatively complicated measurement in any event.
X2.18.3.3 In principle, one can also determine V2 in terms
of the transit time tp measured at normal incidence, and the
distance 2W along the specimen surface between a pair of
symmetrical pitch-and-catch wedge search units, when the
distance between these search units is adjusted for the maxi-
mum echo amplitude. It may be shown that
Vs 2 W
5 t sin u
= V12 2 V 22 sin2u1 b p 1b
Now, if the wedges are such that u1b = 45, this simplifies to
V22 W
5t
= 2V12 2 V2 2 p
For a specific wedge velocity V 1, and measurements of W
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 E 494
and tp, the unknown V2 may be estimated by an iterative V2 5 ~Z1/r2!~1 1 R!/~1 2 R!
calculation, or by interpolation from graphical or tabular data
X2.18.5 Velocity Ratios In some instances, it may be
such as is shown in Table X2.1. The accuracy of this method
useful to determine the ratio of two velocities over a common
generally is not nearly as good as more conventional veloci-
path (6). This is sometimes easier to do than to determine just
metry methods. It is seen to depend on the relative values of V1
and V2, as well as on the angle of incidence. The errors stem in one velocity, when the path length x is known (7). The velocity
part from the uncertainty in determining W. ratio for longitudinal and shear waves is simply the reciprocal
X2.18.4 Reflection CoeffcientIn this method, V2 is de- of the corresponding transit time ratio as follows:
rived in terms of the sound pressure reflection coefficient R (5). VT tL
One can measure R at normal incidence, at the interface VL 5 t T
between a first medium (liquid or solid) of known character-
X2.18.5.1 Poissons ratio s may be written in terms of these
istic impedance Z 1 and the second medium. That is, one
ratios as follows:
measures R = Ecoupled/Efree, where the Es are the echo
amplitudes observed when the two media are coupled and then 1 2 2~VT/VL!2
s5
uncoupled, respectively, for a wave in Medium 1 impinging on 2 2 2~VT/VL!2
Medium 2. Provided the density r 2 in Medium 2 is known or
measurable, the velocity V2 may be determined as follows: X2.18.5.2 Conversely, the velocity ratio may be expressed
in terms of s as follows:
TABLE X2.1 Calculated Values of W/tp for Incident Angle of 45
W/tp, m/s
VT
VL 5 122s
2~1 2 s!
V2, m/s V1 = 5000 7500 10 000 X2.18.5.3 In the case of specimens such as round wires or
2500 m/s m/s m/s m/s
thin rods whose diameter is small compared to wavelengths,
0 0 0 0 0 such that, instead of the propagation of longitudinal waves,
1000 0.295 0.143 0.0947 0.0709
2000 1.37 0.59 0.384 0.286 extensional waves propagate at a velocity of VE = =E/r,
3000 4.81 0.764 0.885 0.651 where E = Youngs modulus and r = density, and torsional
4000
5000
...
...
2.74
5.00
1.63
2.67
1.18
1.89
waves propagate at VT = =G/r, where G = shear modulus,
6000 ... 9.62 4.12 2.81 the thin rod velocity ratio is as follows (8):
7000 ... 49.00 6.15 3.99
VT
VE 5 1 = 1 1 s
8000 ... ... 9.19 5.49
9000 ... ... 14.43 7.43
10 000 ... ... 28.3 10.00

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X3. ACOUSTIC VELOCITY IN ENGINEERING MATERIALS

TABLE X3.1 Acoustic Velocity in Engineering Materials

Longitudinal Velocity Shear Velocity
Material Density kg/m3
(m/s) 310 (in./s)
3
(m/s) 3103(in./s)
Aluminum 2700 6300 250 3130 124
Beryllium 1850 12 400 488 8650 340
Bismuth 9800 2180 85 1100 43
Brass 8100 4370 173 2100 83
Bronze 8860 3530 139 2230 88
Cadmium 8600 2780 109 1500 59
Columbium 8580 4950 194 2180 85
Copper 8900 4700 185 2260 88
Gold 19 300 3240 127 1200 47
Hafnium 11 300 3860 152 2180 82
Inconel 8250 5720 225 3020 119
Iron, electrolytic 7900 5960 235 3220 128
Iron, cast 7200 3500 to 5600 138 to 222 2200 to 3200 87 to 131
Lead 11 400 2160 85 700 27
Lead antimony 10 900 2160 85 810 32
Magnesium 1740 5740 227 3080 122
Monel 8830 6020 237 2720 107
Nickel 8800 5630 222 2960 118
Plastic (acrylic resin) 1180 2670 105 1120 44
Platinum 21 450 3960 155 1670 65
Fused quartz 2200 5930 233 3750 148
Silver 10 500 3600 141 1590 62
Silver nickel 8750 4620 182 2320 91
Stainless steel (347) 7910 5790 226 3100 122
Stainless steel (410) 7670 5900 232 3300 130
Steel 7700 5900 232 3230 127
Tin 7300 3320 130 1670 65
Titanium 4540 6240 245 3215 126
Tungsten 19 100 5460 214 2620 103
Uranium 18 700 3370 133 1930 76
Zinc 7100 4170 164 2410 94
Zirconium 6490 4310 169 1960 77

X3.1 The values given in this appendix have been gathered and processing as well as the conditions of test. They are, in
from a number of sources. The values should not be taken as general, sufficiently accurate for most practical applications.
exact values because of the effects of variations in composition
TABLE X3.2 Densities and Ultrasonic Velocities of Some Ceramic Materials
Longitudinal Velocity Transverse Velocity
Density %Theo-
Material Condition Frequency Frequency
(kg/m3) retical (m/s) (m/s)
(MHz) (MHz)
Alpha silicon carbide Sintered 3190 99+ 12 180 20 7680 20
3100 11 182 7510
3000
2900 90 11 020 6950
Aluminum oxide Sintered 3660 92 9850 50 5900 20
Extruded & sintered 3700 10 200A 5890A
3700 9970B 5930B,C
3700 9970B 5910B,D
Zirconium oxide Sintered 5700 98 7040 30 3720 10
Thermally aged 5680 7050 3760
Silicon nitride HIP 3200 99+ 10 800 50 6010 20
Reinforced silicon nitride 30 vol % SIC whiskers 3200 99+ 10 800 50 6250 20
Reinforced silicon nitride 25 vol % SIC fibers 2490 77 7600E 5 4700E,F 5
4300E,G
YBa2Cu3O7-x(superconductor) Single phase untextured 5940 93 5120 20 3040 5
A
Propagation parallel to extrusion axis.
B
Propagation perpendicular to extrusion axis.
C
Polarization parallel to extrusion axis.
D
Polarization perpendicular to extrusion axis.
E
Propagation perpendicular to fiber axis.
F
Polarization parallel to fiber axis.
G
Polarization perpendicular to fiber axis.

--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---

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X4. VARIATION OF THE ACOUSTIC VELOCITY IN WATER WITH TEMPERATURE

TABLE X4.1 Variation of the Acoustic Velocity in Water with

Temperature
Temperature, Velocity Temperature, Velocity
C (m/s) 3103(in./s) C (m/s) 3103(in./s)
15.0 1470.6 57.89 20.2 1483.6 58.40
15.2 1471.1 57.91 20.4 1484.1 58.42
15.4 1471.6 57.93 20.6 1484.6 58.44
15.6 1472.1 57.95 20.8 1485.1 58.46
15.8 1472.6 57.97 21.0 1485.6 58.48
16.0 1473.1 57.99 21.2 1486.1 58.50
16.2 1473.6 58.01 21.4 1486.6 58.52
16.4 1474.1 58.03 21.6 1487.1 58.54
16.6 1474.6 58.05 21.8 1487.6 58.56
16.8 1475.1 58.07 22.0 1488.1 58.58
17.0 1475.6 58.09 22.2 1488.6 58.60
17.2 1476.1 58.11 22.4 1489.1 58.62
17.4 1476.6 58.13 22.6 1489.6 58.64
17.6 1477.1 58.15 22.8 1490.1 58.66

--`,,,````,,````,``,,```,,`,-`-`,,`,,`,`,,`---
17.8 1477.6 58.17 23.0 1490.6 58.68
18.0 1478.1 58.19 23.2 1491.1 58.70
18.2 1478.6 58.21 23.4 1491.6 58.72
18.4 1479.1 58.23 23.6 1492.1 58.74
18.6 1479.6 58.25 23.8 1492.6 58.76
18.8 1480.1 58.27 24.0 1493.1 58.78
19.0 1480.6 58.29 24.2 1493.6 58.80
19.2 1481.1 58.31 24.4 1494.1 58.82
19.4 1481.6 58.33 24.6 1494.6 58.84
19.6 1482.1 58.35 24.8 1495.1 58.86
19.8 1482.6 58.37 25.0 1495.6 58.88
20.0 1483.1 58.38

REFERENCES

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Measurement of Elastic Moduli at Elevated Temperatures, Using
Momentary Contact, Journal of the Acoustical Society of America,
Vol 36, No. 9, September 1964, pp. 16781684.
(2) Rollins, F. R., Jr., Critical Ultrasonic ReflectivityA Neglected Tool
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1969, pp. 127145.
(3) Becker, F. L., and Richardson, R. L., Ultrasonic Critical Angle
Reflectivity, Research Techniques in Nondestructive Testing, Aca-
demic Press, New York, NY 1970, pp. 91131.
(4) Lynnworth, L. C., et al, Final Report, NAS3-26931, June 1972.
(5) Lynnworth, L. C., et al. Attenuation Measurements Using the
Pulse-Echo AB Method, Without Multiple Echo Reverberations in
Specimen, Materials Evaluation, Vol 31, No. 1, January 1973, pp.
616.
(6) Mason, W. P., Piezoelectric Crystals and Their Application to Ultra-
sonics, Van Nostrand, Inc., Princeton, NJ 1950, pp 390437.
(7) Lynnworth, L. C., and Carnevale, E. H., Proceedings of the 5th
International Conference of Nondestructive Testing, Montreal, May
1967, pp. 300307.
(8) Tzannes, N. S., IEEE Transactions on Sonics and Ultrasonics, SU-13,
Vol 2, July 1966, pp. 3341.
(9) Bell, J. F. W., The Propagation of Sound in Metals at High
Temperatures, British Journal of Nondestructive Testing, September
1968.
(10) Chick, B., Ultrasonic Attenuation Unit and Its Use in Measuring
Attenuation in Alkali Halides, Journal of the Acoustical Society of
America, Vol 32, No. 2, February 1960, pp. 186193.
(11) Frederick, J. R., Journal of the Acoustical Society of America, Vol 20,
1948, pp. 586(A).
(12) Levitt, A. P., and Martin, A. G., Nondestructive Testing, Vol 18, 1960,
pp. 333336.
(13) Lynnworth, L. C., Papadakis, E. P., and Fowler, K. A., International
Journal of Nondestructive Testing (1972), Proceedings 1971 ARPA/
AMMRC Symposium, June 1971.
(14) May, J. E., Jr., Precise Measurement of Time Delay, IRE National
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 E 494
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