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1.

Pembuatan Kurva Standar Konsentrasi vs Konduktansi Kurva Standar Asam Aseta


Larutan Konduktansi, S/m
0 3.00E-05
0.05 3.70E-04 K
0.04 3.30E-04 4.00E-04
0.03 2.90E-04 f(x) = 0.006344709
3.50E-04 R = 0.9229120266
0.02 2.40E-04 3.00E-04
0.01 1.90E-04

Konsentrasi, N
2.50E-04
0.005 1.00E-04
2.00E-04
1.50E-04
2. Peneraan Debit Aliran
1.00E-04
Waktu = 30 detik
No
Tinggi float pada flowmeter,
Volume
cm tertampung, mL 5.00E-05

1 20 30 0.00E+00
0.00050 0.01050 0.0
30
K
29
2 40 41
42 Konsentrasi Asam Asetat
41
Waktu,
3. Adsorpsi Asam Asetat menit
ID kolom 1.7 cm 0
H act. Ca 30.3 cm 3
Waktu, Q = 20 cm3/menit Q = 40 cm3/menit 6
menit Volume, mL Konduktansi, S/m Volume, mL Konduktansi, S/m 9
0 0 2.20E-04 0 2.20E-04 12
3 88 1.60E-04 195 3.30E-04 15
6 140 3.00E-04 345 3.20E-04 18
9 221 3.20E-04 493 3.20E-04 21
12 311 3.40E-04 638 3.20E-04 24
15 394 3.40E-04 782 3.20E-04 27
18 474 3.50E-04 929 3.20E-04 30
21 559 3.50E-04 1075 3.20E-04
24 644 3.50E-04 1232 3.10E-04 Kurva Breakthrough
27 732 3.50E-04 1385 3.20E-04
30 816 3.50E-04 1536 3.10E-04 Waktu,
menit
0
3
6
9
12
15
18
21
24
27
30

Peneraan Debit Alir

20

40

Data Nilai ln(C0/Ct-1) vs w

Kurva BDST untuk Q = 20 cm3/menit Waktu,


menit
35
0
30
3
25 6
Waktu, menit

20 9
f(x) = - 8.0077588698x + 5.8800217287
R = 0.6504554517 15 12
15
10
18
5
21
0 24
-2.0000 -1.5000 -1.0000 -0.5000 0.0000 0.5000 1.0000 1.5000
27
ln[(Co/Ct)-1] 30

Menghitung No

Kurva BDST untuk Q = 40 cm3/menit slope


intercept
35

30
20
25
Waktu, menit

20
f(x) = - 7.8830290868x + 7.1135038503 15
R = 0.1196372241
10

0
-1.6000-1.4000-1.2000-1.0000-0.8000-0.6000-0.4000-0.20000.0000 0.2000 0.4000
40
ln[(Co/Ct)-1]
Kurva Standar Asam Asetat

Kurva Standar Asam Asetat


4.00E-04
f(x) = 0.0063447099x + 8.09385665529011E-05
3.50E-04 R = 0.9229120266
3.00E-04
2.50E-04
2.00E-04 Col umn B
Li near (Col umn B)
1.50E-04
1.00E-04
5.00E-05
0.00E+00
0.00050 0.01050 0.02050 0.03050 0.04050 0.05050 0.06050
Konduktivitas, S/m

Konsentrasi Asam Asetat Keluar Kolom Pada Berbagai Waktu

Q = 20 cm3/menit Q = 40 cm3/menit
Konduktansi, S/m Konsentrasi, N Konduktansi, S/m Konsentrasi, N
2.20E-04 0.0215 2.20E-04 0.0215
1.60E-04 0.0116 3.30E-04 0.0396
3.00E-04 0.0346 3.20E-04 0.0379
3.20E-04 0.0379 3.20E-04 0.0379
3.40E-04 0.0412 3.20E-04 0.0379
3.40E-04 0.0412 3.20E-04 0.0379
3.50E-04 0.0429 3.20E-04 0.0379
3.50E-04 0.0429 3.20E-04 0.0379
3.50E-04 0.0429 3.10E-04 0.0363
3.50E-04 0.0429 3.20E-04 0.0379
3.50E-04 0.0429 3.10E-04 0.0363

Kurva Breakthrough

Q = 20 cm3/menit Q = 40 cm3/menit Kurva B


Volume, mL C/Co Volume, mL C/Co
1.0000
0 0.0000 0 0.0000
0.9000
88 0.2322 195 0.7914
0.8000
140 0.6927 435 0.7585
0.7000
221 0.7585 493 0.7585 0.6000
311 0.8243 638 0.7585
C/Co

0.5000
394 0.8243 782 0.7585 0.4000
474 0.8571 929 0.7585 0.3000
559 0.8571 1075 0.7585 0.2000
644 0.8571 1232 0.7256 0.1000
732 0.8571 1385 0.7585 0.0000
0 5 10 15 2
Waktu, men
0.3000
0.2000
0.1000
0.0000
0 5 10 15 2
816 0.8571 1536 0.7256
Waktu, men

Peneraan Debit Alir

Vol tertampung rt2 = 29.67 mL Kurva


Debit aliran = 59.33 mL/menit 1.0000
Vol tertampung rt2 = 41.3333333333 mL 0.9000
0.8000
Debit aliran = 82.6666666667 mL/menit
0.7000
0.6000
Data Nilai ln(C0/Ct-1) vs waktu

C/Co
0.5000
0.4000
Q = 20 cm3/menit Q = 40 cm3/menit 0.3000
Ct, N ln(Co/Ct - 1) Ct, N ln(Co/Ct - 1) 0.2000
0.0215 0.2836 0.0215 0.2836 0.1000
0.0116 1.1957 0.0396 -1.3332 0.0000
0 200 400 600 800 10
0.0346 -0.8128 0.0379 -1.1444 Volume, cm
0.0379 -1.1444 0.0379 -1.1444
0.0412 -1.5455 0.0379 -1.1444
0.0412 -1.5455 0.0379 -1.1444
0.0429 -1.7918 0.0379 -1.1444
0.0429 -1.7918 0.0379 -1.1444
0.0429 -1.7918 0.0363 -0.9724
0.0429 -1.7918 0.0379 -1.1444
0.0429 -1.7918 0.0363 -0.9724

Menghitung No

1/(k.Co)
No.z/(Co.u)

y=-9.8141x-0.9542
intercept = 0.9542
slope = -9.8141
u= 8.8158155731 cm/menit
k= -2.0378842686 L/gram/menit
No = 0.0138812726 N/menit

y=-7.5047x-0.1513
intercept = -0.1513
slope = -7.5047
u= 17.6316311463 cm/menit
k= -2.6649966021 L/gram/menit
No = -0.0044020888 N/menit
Kurva Breakthrough
00
00
00
00
00
00 Q = 20 cm3/meni t
Q = 40 cm3/meni t
00
00
00
00
00
0 5 10 15 20 25 30 35
Waktu, menit
00
00
00
00
0 5 10 15 20 25 30 35
Waktu, menit

Kurva Breakthrough
000
000
000
000
000
000 Q = 20 cm3/meni t
Q = 40 cm3/meni t
000
000
000
000
000
0 200 400 600 800 10001200140016001800
Volume, cm3