Tensile tests were carried out at room temperature on 6061-aluminium alloy reinforced with SiC
and AI203 particulates. Although a significant increase in strength could be achieved by
introducing ceramic reinforcements into the aluminium alloy matrix, it is associated with
a substantial decrease in fracture strain. In order to understand the reason for the inferior ductility
of such composites, analytical solutions were obtained using a simple composite model. SEM
studies were carried out on the side surfaces of the fractured specimens to verify the proposed
failure behaviour. Failure modes observed to operate in such composites under uniaxial tension
are described.
TABLE I T6 heat-treatment condition used in the present study (7,0(00,0) = - (7osin20/2 (lb)
(7o0(0% 0) = (7o(1 - cos20)/2 (lc)
SiCp/A1 composite (AI203)p/A1 composite
The Airy stress function, q), for this case can be given
Solution treatment 530~ 70 min 560 ~ 60 min
as a linear combination of function of polar coordin-
RT ageing 24 ~ 48 h 24 ~ 65 h
Artificial ageing 200 ~ 10 h" 170 ~ 14 h b ates r and 0. Matrix part of this function, qbm', is
(7 0
a Overaged condition. ~ml(r,O) = ~-r2(1 -- cos20)
b Peak-aged condition.
Ca4(COS 20"~]
Material Direction" E(GPa) %s(MPa) r e~(%)
+ \ ,.2 }/ (2)
SiCp/A1 T - 269.5 323.0 2.8 where A, B, and C are constants, and superscript ml
L - 302.0 368.6 5.3 denotes matrix under applied uniaxial loading. One
(A1203)p/AI T 80.6 b 285,0 345.2 2.5 can notice that the first term in Equation 2 describes
L 79.9 b 301.5 364.5 9.0
the undisturbed field (when there is no inclusion in the
6061 AI 68.0 b 265.5 310.5 20.0
matrix), and the last three terms describe the local
a T, transverse direction; L, Longitudinal direction. disturbance due to the discontinuity (i.e. inclusion) in
b Values measured by sonic resonance method. the elastic medium. However, according to Saint
5454
Figure ] (a) Scanning electron micrograph showing crack development in a tensile specimen of SiCp/Al composite (etched with HCl to reveal
the subsurface region). (b) Interfacial debonding and particulate cracking. Note the crack propagation into the matrix in front of the
particulate crack. (c) Joining of particulate crack and debonded interface.
5455
U~nl = (O'0/S].tm)[ - 2r - B ( K m -- 1)a2/r
+ 2Ca4/r 3] sin20 (4e)
o~ = (Cro/2)(D -- E cos20) (4f)
il
at0 = (Cro/2)(E + 3FrZ/a 2) sin20 (4g)
it
~oo = (%/2)[D + (E + 6FrZ/a2)cos20] (4h)
u~' = (Oo/8g i) {D(K i -- 1)r
- [2Er - F(K i -- 3)r3/a 2] cos20} (4i)
u~ 1 = (Oo/8p i) [ 2 E r + f ( ~ i + 3)r3/a 2] sin20 (4j)
[F(~c i - 1) + 2] (6a)
B = 2(F - 1)/(F + ~:m) (6b)
C = (1 -- F)/(I ~ -I- Ic m ) (6c)
F = 0 (6f)
where F = g m / f
++lf++
,1r
r162162162162162
1o) %
% %
++++++ ++++++
+<mi.tm
~
x k'
AT &r
+
@
r 4, z
r162162162162162
r162162162162
if0 (TO
(b)
Figure 4 (a) Two-dimensional composite model; a large thin plate having a circular inclusion with different elastic constants, (~c,Ix), and
thermal expansion coefficients, c(, subjected to uniaxial tension, c%, where la is the shear modulus, c( is the thermal expansion coefficient,
l~ = (3 - 4v) for plane strain, • = (3 - v)/(1 + v) for plane stress. (b) Schematics drawings of the superposition of stresses caused by external
loading and thermal expansion coefficient mismatch.
5457
where superscripts m 2 and i 2 represent matrix and Normatizedstress, ~x/%
inclusion parts under inelastic contribution due to 1.6-
thermal expansion coefficient mismatch.
Hence, from the results in Sections 4.1 and 4.2, the
total stress and displacement should be the sum of the 1.2-
elastic and the inelastic terms
~ ...........
13.1j
=
i1 i2
(~ij -JF (~ij, ~M =
rn~ m2
i~ij + {~ij
(9a)
/
I i1 i2 m s m2
0.8-
it
ui = ui + ui, u~ = ui + ui 9 (9b) iJ
3.8
5. Analysis and discussion
5.1. Stress concentration and load transfer
When a discontinuity is present in a body, local stress 0.4
disturbances will be developed near the discontinuity.
However, the extent and shape of stress disturbance
near the discontinuity depend on the geometry of the /•D
t}}{r
(el Normalized distance
5458
acting on the matrix near the pole of the inclusion is Norrnotized stress, ~y/%
calculated ~to be about 1.5 times that of the applied 1.0
tensile stress. This stress reaches a maximum value in
the matrix at a point slightly away from the pole along
the direction of the applied stress, and finally de- 0.6
creases to the level of applied tensile stress at regions C
away from the pole. Such a stress distribution at the
pole region of the inclusion, along the direction of the 8 0
tensile stress, appears to be responsible for some of the Normalizedciisto'nce'
matrix material to be adherent to the particulate rein-
forcement, as has been observed occasionally at the
debonded interfaces (Fig. 3b). This stress distribution
is illustrated in Fig. 7. -0"61
(el -1.0
,JA TABLE III Selected material properties for SiC and AlzO 3 1-28]
Material
6061 AI
E(GPa)
68.0
p(GPa)
29.3
v
0.33
:z (10 -6 ~
28.0
1)
5459
O"0
tftttt
the matrix. This is due to the fact that the axial stress,
Oxx, at the interface decreases and that in the matrix
increases abruptly as can be seen in Fig. 5.
Tensile loading also gives rise to stress concentra-
tion within SiCp, causing particulate cracking. From
Equations 4 and 10, the stress exerted on SiCp is
o
z B calculated to be about 1.5 times that of the applied
tensile stress. Although, this calculated stress is
smaller than the fracture strength of SiC, its failure can
occur even under a small stress value, because most
-4.5 -0'.9 -0'.3 0'.3 0'.9 '
1.5 ceramic particles have flaws, grain boundaries, and
sharp points where higher stress is concentrated.
(b) Normatized stress~ (~x/O'o
From Fig. 3, which illustrated typical particulate
2.0 cracking under tension, one can notice that particulate
cracking precedes matrix failure, although severe plas-
1.8- tic deformation could be observed in the matrix near
the region of cracked SiCp. Once SiCp has cracked, the
= 1,6- constraint on the plastic deformation of the matrix
._m will disappear. Then matrix near SiCp can easily
undergo plastic deformation. Such a situation can be
"~ 1.4-
o
considered to be similar to the matrix alloy with
E
o
a crack in it, providing a higher stress concentration at
z 1.2-
the crack tip. Under such conditions, the matrix fails
easily, and the ductility of the composite will decrease
1.0 t , , significantly.
1.0 111 1.2 1.3 1.4
(c) NormO.izedstres% O'x/Oo
Figure 7 (a) Schematic illustration of the loading configuration and 5.3. Effect of thermal residual stress on the
the trajectory along which stress distributions are drawn. (b) Nor- failure mode
malized stress (ox/o0) distribution from the pole of SiCp along
the line AB (tensile direction). (c) Detailed stress distribution
In this specific case, the pressure acting on the
pattern within the enclosed rectangle. The shaded quarter-circle in matrix/inclusion interface ( - P in Equation 7) is com-
(b) indicates the location of the particulate. puted to be about - 800 M P a for the temperature
5460
drop from the composite fabrication temperature to
room temperature (AT,~600~ However, upon )~ T~
cooling from the fabrication temperature, most of this
inelastic stress will be relieved by the plastic deforma-
0
tion of the matrix near SiCp (i.e. generation of disloca-
tion around SiCp) and only a small portion of about
- 30 MPa, as estimated by Arsenault and Taya [31],
will remain in the form of residual stress at the inter-
face. These inelastic stresses acting on SiCp and the
0
matrix will not change the state of stress significantly, ,ol $
because values are small compared to those of the
applied stress. Consequently, there should be no sub-
stantial changes in the mode of particulate cracking
and interfacial debonding as a result of the thermal
residual stress.
6. Conclusions
Stress concentration in the matrix near the pole of the
particulate, and stress concentration within the partic-
ulate, appear to result in interfacial debonding and
particulate cracking, respectively. Increase in applied
stress causes such microcracks to open. New cracks
develop in the matrix at the tip of the opened-up (f)
crack, propagate into the matrix and join with nearby
cracks, and form a large void. Based on the micro- Figure 9 Schematicdrawings of the failuremechanism of the partic-
scopic examinations and analytical study, interfacial ulate-reinforced aluminium alloy composites. (a) Loading config-
debonding and particulate cracking together were uration. (b) Formation of particulate cracking and interfacial
debonding. (c) Opening-up of cracked plane and debonded inter-
considered to be responsible for the substantial de- face due to plastic flow of the aluminium matrix. (d) Crack propa-
crease in the ductility of the particulate-reinforced gation into the aluminium matrix due to stress concentration
aluminium alloy composites. build-up at the crack tip. (e) Joining of cracks. (f) ~oid formation.
5461
Because particulate cracking and interracial debond- 16. D . L . M c D A N E L S , Met. Trans. 16A (1985) 1105.
ing were observed to always precede the matrix 17. R.J. ARSENAULTandS. B. WU,Mater. Sci. Engng96(1987)
77.
failure, such phenomena appear to be more respon-
18, A . K . VASUDEVAN, O. R I C H M O N D , F. Z O K and J. D.
sible for the failure than a mechanism based on the E M B U R G , ibid. A107 (1989) 63.
matrix failure 19. H. O H T S U , "Design and manufacturing of advanced com-
posites" (ASM, Detroit, 1989) p. 187.
20. D. J. LLOYD, H. LAGACE, A. M c L E O D and P. L.
References MORRIS, Mater. Sci. Engng A107 (1989) 73.
21. S.R. N U T T and J. M. DUVA, Scripta Metall. 20 (1986) 1055.
1. N. T S A N G A R A K I S , B. O. A N D R E W S and C. CAVAL-
22. S.R. N U T T and A. N E E D L E M A N , ibid. 21 (1987) 705.
LARO, J. Compos. Mater. 21 (1987) 481.
23. J . J . L O W A N D O W S K I , C. LIU and W. H. H U N T , Mater.
2. T . G . NIEH and D. J. C H E L L M A N , Scripta Metall. 18 (1984)
Sci. Engng 107A (1989) 241.
925.
24. C. P. YOU, A. W. T H O M P S O N and I. M. BERNSTEIN,
3. R . J . A R S E N A U L T and S. B. WU, ibid. 22 (1988) 767.
Scripta Metall. 21 (1987) 181.
4. R . J . A R S E N A U L T , Mater. Sei. Engng 64 (1981) 171.
25. T. CHR1STMAN, A. N E E D L E M A N , S. N U T T and
5. Y. F L O M and R. J. A R S E N A U L T , J. Metals 38 (1986) 31.
S. SURESH, Mater. Sci. Engng 107A (1989) 49.
6. V.C. N A R D O N E , Scripta Metall. 21 (1987) 1313.
26. G . M . J A N O W S K I and B. J. P L E T A K A , ibid. A129 (1990) 65.
7. R . H . JONES, C. A. L A V E N D E R and M. T. SMITH, ibid. 21
27. N. I. M U S K H E L I S H V I L I , "Some basic problems of the
(1987) 1565.
mathematical theory of elasticity" (Noordhoff, Groningen,
8. W . A . L O N G S D O N and P. K. LIAW, Engng Fract. Mech. 24
Holland, 1953) pp. 215-16.
(1986) 737.
28. Y. S. T O U L O U K I A N (ed.) "Thermophysical properties of
9. T. C H R I S T M A N and S. SURESH, Mater. Sci. Engng 102
high temperature solid materials, Vol. 6, part I (Thermophysi-
(1988) 211.
cal properties research center, Purdue University, 1967).
10. J . K . SHANG, W. YU and R. O. RITCHIE, ibid. 102 (1988)
29. Y. F L O M and R. J. A R S E N A U L T , Mater. Sei. Engng 77
818.
(1986) 191.
11. F . M . H O S K I N G , F. F. P O R T I L L O , R. W U N D E R L I N and
30. T. ISEKI, T. K A M E D A and T. M A R U Y A M A , J. Mater. Sci.
R. M E H R A B I A N , J. Mater. Sci. 17 (1982) 477.
19 (1984) 1692.
12. F. A. G I R O T , J. M. Q U E N I S S E T and R. NASLAIN,
31. R.J. ARSENAULTandM.TAYA,ActaMetall. 35(1987)651.
Compos. Sci. Technot. 30 (1987) 155.
13. V. C. N A R D O N E and J. R. STRIFE, Metall. Trans. 18A
(1987) 109.
14. K . S . R A V I C H A N D R A N , J. Metals 39 (1987) 28.
Received 17 June
15. J.J. STEPHENS, J.P. LUCASandF. M. HOSKING, Scripta
Metall. 22 (1988) 1307. and accepted 16 December 1991
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