Research S p o n s o r e d by t h e W e l d i n g R e s e a r c h C o u n c i l
of t h e E n g i n e e r i n g Foundation
a D e p t h , half length, or half di- fracture toughness (ksi -\/' n -) E/A Energy per unit fracture area meas-
ameter of t h e crack (in.) Kid Dynamic-load plane strain frac- ured in DT test
as, Original crack dimension ture toughness (ksi \/>n.) NDT Nil Ductility Transition tempera-
B Thickness of the plate o r specimen Kx Questionable, invalid values of K ture obtained by DWT or indexed
(in.) due to excessive plastic deforma- by DT test
G Strain energy release r a t e with tion of the crack tip FTE Fracture Transition Elastic
crack extension R Resistance to fracture extension FTP Fracture Transition Plastic
Gc, Gjc Critical values of G for elastic Rr Constant defining resistance to DWT Drop Weight Test
fracture; G!c refers t o t h e plane plastic fracture in terms of DT DT Dynamic Tear Test—all sizes
strain state, while Gc refers t o t h e energy CAT Robertson Crack Arrest Temper-
plane stress state Aa Fracture extension increment ature
K, Ki Stress intensity factor; the sub- a or rj„ Applied stress (psi or ksi) C« Charpy-V test
script / denotes the opening <TyB Yield strength for static (slow) COD Crack Opening Displacement
mode of crack extension (ksi loading (psi or ksi) FAD Fracture Analysis Diagram
VST) o-yd Yield strength for dynamic load- RAD Ratio Analysis Diagram
Kic Slow-load (static) plane strain ing (psi or ksi) Ratio Signifies KT4"V> ° r Kia/<ryd
1940s to present. The dramatic de- and stress for fracture initiation. The termination of this design parameter
velopment of this knowledge is record- early welding engineers had been con- in the laboratory.
ed in large part in the literature of the cerned primarily with procedural as- Examinations of ship failures
SOCIETY. pects of welding and not with welda- provided the first significant informa-
The technological capabilities which bility factors of the steels. In effect, tion as to conditions for the initiation,
have evolved as the result of metallur- everyone relied on past experience propagation, and arrest of fractures.
gical and fracture research are most with riveted and bolted structures, It was noted that the chevron mark-
impressive. Today we can proceed which indicated that the elongation ings pointed back to the exact location
directly to developing new high and reduction-of-area ductility param- of fracture initiation. The initiation
strength steels of desired weldability eters of the tensile test generally sites usually involved minute defects
properties as a systems approach util- ensured ductile performance of the such as weld cracks or arc strikes.
izing a task force comprised of metal- structure. The experience with World Observation that many short cracks
lurgists, fracture specialists and weld- War II welded ships clearly demon- were arrested in regions of steep stress
ing engineers. An elegant description strated that tensile test ductility was gradients, indicated that the specific
of the new systems approach was not a sufficient parameter for the level of the elastic stress field through
provided by Dr. J. Gross in the 1968 characterization of the structural reli- which the moving crack was propagat-
Adams Lecture. ability of steels. ing had a bearing on the fracture
It is my pleasure to chart the course Figure 1 illustrates the effect of problem. In unusual cases it was noted
of this progress and to provide a temperature on the tensile and frac- that arrests were obtained in service
prognosis of continuing advances in ture toughness properties of a typical when the crack entered a new plate in
this dynamic field of research. ship steel. The smooth-body tensile regions which did not feature stress
specimen shows a ductile to brittle gradients. Figure 2 illustrates such an
Origins of the Problem transition over a range of relatively arrest. The important feature to note
and Early Studies low temperatures. In the presence of is that the painted surface has crazed
Prior to 1940 metal structures were cracks, the transition from plastic to at the arrest point, indicating ductile
generally fabricated by riveting and elastic levels of fracture strength is behavior (yielding) of the metal. In
bolting. The failure of a component developed over a range of much high- this case the arrest is clearly due to a
part of such structures is generally an er temperatures. Early studies during plate of higher fracture toughness
isolated event which rarely leads to the period of 1940 to 1943 indicated than the adjoining propagation plate.
total collapse. It was not appreciated that the cracked-body, transition tem- We now recognize two conditions
that the monolithic nature of welded perature range was the critical index which lead to arrests of propagating
structures provides continuity condi- for the loss of fracture strength of cracks:
tions such that fracture initiation in ship structures. It was then deemed 1. Crack entry into a region of very
even a small appendage part can lead essential to evolve notch tests for de- low stress.
to catastrophic consequences. This 2. Crack entry into a plate of high-
fact became appallingly clear with the er fracture toughness.
welded fabrication of World War II AUTHOR'S NOTE: The chronologi- The initiation should be expected to
ships. The initiation of fracture in an cal treatment and separation of the occur at sites of high stresses, in plates
element of the structure, such as a subject matter in the various sec- of low fracture toughness at the serv-
hatch corner, was often followed by tions, suggested a reference system ice temperature.
nearly instantaneous fracture of the of bibliographic type. These pri-
mary references, which are ar- The separation of ship plates into
entire ship. the categories of initiation, propaga-
ranged chronologically and by
The problem was compounded by subject matter at the end of Part tion, and arrest types provided for
the lack of reliable information on 11 of this lecture, have been se- calibration of the significance of the
metallurgical factors which deter- lected to lead the reader into de- only standardized notch tests of the
mined the specific fracture sensitivity tails of studies for the various time—the Charpy-Keyhole (Ck) and
of steels. Thus, the metallurgist could time periods. The titles of the text- the Charpy-V (Cv) tests. Both tests
not proceed directly to develop steels books generally identify the con- were evolved about 1905 and had
of improved fracture properties which tents. This treatment provides for been used for qualitative assessments
the broadest possible reference sys-
could be used to solve the problem. tem without complications of mul- of the transition temperature range of
The designer had no basis for analysis tiple cross references. steels. There was no rational basis for
of the relationship between flaw size using these tests in predicting struc-
92-s I M A R C H 1971
STRUCTURAL MILD STEEL
STRENGTH AND DUCTILITY
TRUE STRESS TRANSITIONS
AT FRACTURE
150
A
N. LOWER YIELD
v7^
\_J f \
^ —-_
~~-^_^___^
FULL
DUCTILITY
b
/~\ ^C,??-''.-^-.'.-"'-;,- 1 -'.; SMOOTH BODY A'7f CRACKED BODY
FRACTURE ,'TS? FRACTURE
D INITIATION fy7'lf
DUE TO S M A L L / v V : ' *
TRANSITION
50
- n •
FLAW \ /i$V?f
/SfABLEf
,
1 i I i i i
# 2 3 ; - $ '"f^cUSir
I I 1
LIMIT
1 1
-400 -350 -300 -250 -200 -150 -IOO -50 50 100 150 200 (°F)
L I _l I I
-250 -200 -150 -IOO -50 50 IOO C O
TEMPERATURE
Fig. 1—Comparison of t r a n s i t i o n t e m p e r a t u r e ranges d e f i n e d by t e n s i l e a n d d y n a m i c f r a c t u r e tests for a t y p i c a l struc-
t u r a l m i l d steel. T h e highest possible t r a n s i t i o n t e m p e r a t u r e range is e s t a b l i s h e d by increases in d y n a m i c f r a c t u r e
t o u g h n e s s w h i c h p r e c l u d e t h e d e v e l o p m e n t of u n s t a b l e f r a c t u r e . All t r a n s i t i o n s related to f l a w size a n d l o a d i n g rate
aspects m u s t be b e l o w t h i s l i m i t i n g t r a n s i t i o n t e m p e r a t u r e range
tural performance. Additionally, it significantly in excess of 20 ft-lb re- demonstrated that the critical transi-
was not known if measurements of sulted in "yielding" arrests (see Fig. tion temperature references moved to
fracture energy or some other crite- 2). higher positions on the Cv energy
rion should be preferred for the cali- These statistics indicated that serv- curve (higher Cv energy indices) for
bration of these tests. It should be ice temperatures below the 10 ft-lb many steels which differed from the
noted that the Cv energy transition transition temperature index would original ship fracture type. This
curves parallel the course of the frac- provide for fracture initiation due to finding was catastrophic to the con-
ture appearance and the notch-root the presence of small cracks. Service cept of an invariant reference to the
contraction (ductility) transition temperatures below the 20 ft-lb tran- Cv energy transition curve. Clearly
curves. The energy curve provides for sition temperature index would the C„ test requires specific calibra-
the most direct definition of the tran- provide for propagation, except in ar- tions for different steels and, as such,
sition features, and no advantage is eas of abnormally low stress. Service poses unacceptable complications for
gained by reference to other measure- temperatures in excess of the 20 ft-lb general engineering use across broad
ments. transition temperature index would families of steels.
By 1945 the Ck test was recognized assure arrests, due to metal ductility,
to be totally inadequate for definition as the fracture extended into a plate Evolution of Natural Crack Tests
of the true transition temperature of such characteristics. As the result A wide variety of new fracture tests
range experienced in service. Because of these studies, it became conven- were evolved from 1940 to 1950.
of its excessively blunt notch, it indi- tional to reference the transition tem- These tests can be separated into two
cated a transition from ductile to brit- perature range quality of the steels in basic types:
tle fracture at temperatures which terms of the 15 ft-lb transition tem- 1. Tests which utilized small labora-
were much lower than experienced by perature index which represented a tory specimens featuring machined
the ships. The Cv test offered better conservative definition of the highest notches and tensile loading.
promise for calibration since its transi- temperature for fracture initiation. 2. Structural prototype tests of very
tion region includes the temperatures By 1952 the 15 ft-lb C„ transition large dimensions featuring machined
of ship fractures. Attention was then temperature was accepted as the notches and/or the presence of welds.
directed to studies of the ship failure definitive criterion for purposes of de- The interest in large structural pro-
steels solely by the use of the Cv test. sign and as guidance for metallurgical totype tests resulted from the inability
By 1950 correlations were evolved studies. The effects of alloy elements, to reproduce ship failure conditions at
which disclosed that the fracture initi- grain size, normalizing heat treat- service temperatures by any of the
ation, propagation, and arrest plates ments, deoxidation practices, etc. small test specimens. Irrespective of
featured distinctly different maximum were investigated in terms of the the acuity of the machined notches
values of Cv energy at the tempera- effect on shifting the 15 ft-lb transi- and the notch depth, stresses over
ture which corresponded to the serv- tion temperature. Unfortunately, yielding were always required for ini-
ice fracture. The results were as fol- there was a basic error in the assump- tiation of the fractures for the labora-
lows: initiation plates—maximum 10 tion that the 10 to 20 ft-lb Cv energy tory tests. In contrast, the initiation of
ft-lb; propagation plates—maximum range had the same significance for failures in service was always obtained
20 ft-lb; arrest plates—energy values these modified steels. By 1953 it was at elastic stress levels. Increasing the
Fig. 2—Crack arrest in ship structure which developed as the frac- Fig. 3—Features of Explosion Crack Starter Tests of ship
ture entered a plate of higher-than-average fracture toughness. plate steels. The steel illustrated features a 15 ft-lb Cv
The intense craze pattern of the painted surface indicates plastic transition of approximately 30° F (0° C) and is representa-
deformation of the underlying metal tive of best quality. Ship plates of relatively poor quality
develop similar transition features at higher temperatures
size of the test plates did not modify 2. The slow loading rate favored The results of typical ship plate test
this behavior. Again the service failure the development of extensive yielding series conducted over a range of tem-
conditions could not be reproduced. prior to initiating cleavage. peratures are illustrated in Fig. 3. The
Obviously a fresh approach was re- The highest temperature range for test series present a clear panorama of
quired—slow loading of specimens the initiation of cleavage fracture at the effects of temperature on the initi-
featuring machined notches did not elastic stress levels must be deter- ation and propagation features of the
correspond to the service conditions mined by laboratory tests involving steel in the service temperature range
of fracture initiation. In view of the cracks of ultimate sharpness and the of the ships.* At 20° F ( - 8 ° C) a flat
impasse which existed in 1950, investi- application of dynamic loading. The break is obtained (elastic fracture),
gations were redirected to fracture test specimen size can be reduced to while at 40° F (5° C) and higher
studies involving natural cracks. The very small dimensions if these condi- temperatures, increasing bulging
basic premise which guided this new tions are met. These conditions are (plastic overload) indicates increased
approach was the recognition of the essential to ensure that the cleavage of resistance to the initiation of fracture.
role of cleavage microfracture proc- the first grains is developed under the The term Nil Ductility Transition
esses, which are inherent to metallur- most adverse (worst case) conditions (NDT) temperature was applied to
gical considerations of the problem. for suppression of microfracture duc- the flat break temperature. In other
This information had been evolved by tility. The highest temperatures at words, with descending temperature a
basic research investigators, primarily which a steel structure can be expect- critical transition point is reached such
at universities and most notably by ed to fail is controlled by such worst that elastic fracture initiation (nil duc-
Gensamer, Low, Cohen, and Stout. case conditions. By enforcing the tility) is possible in the presence of a
Such considerations had matured to worst case in laboratory tests, an ex- dynamically loaded small flaw.
suggesting that the cleavage fracture act match can be found to the highest It should be noted that the resist-
instability is first developed in embrit- temperatures of possible service fail- ance to propagation of the fractures
tled metal adjacent to the weld i.e., in ure at purely elastic load stresses. increases markedly with increasing
the heat-affected zone. Once the temperature. Between 60 and 80° F
These analyses led to the develop-
cleavage instability is developed within (15 and 25° C) the fractures no
ment of the Explosion Crack Starter
relatively few grains in the embrittled longer run through the elastically
Test which featured a short, brittle
heat-affected zone region, the base loaded edge regions; however, contin-
weld bead (hard surfacing type) de-
metal grains in line are then subjected ued propagation is obtained through
posited on the plate surface. The 1 in.
to the dynamic extension of an ul- the plastically loaded center regions.
thick plates (14 X 14 in.) were placed
trasharp natural crack. As a conse- This temperature point was defined as
over a circular die and loaded by
quence, the mechanical behavior of the Fracture Transition Elastic
offset explosion. The intent was to
the structure as a whole is equivalent (FTE) and signifies the highest pos-
observe the effects of increasing tem-
to that which should be expected for sible temperature for unstable frac-
perature on the propagation of the
dynamic loading. ture propagation through elastic stress
fractures. The function of the brittle
fields. Ultimately, a higher temperature
There were two problems with the weld bead was to introduce a small
is reached at which only ductile tear-
long-sought goal of attempting to ini- crack of natural sharpness, similar to
ing is possible. Because of the high
tiate fracture at elastic levels in the the weld defect cracks or arc strikes
resistance to propagation of ductile
presence of a machined notch loaded of the service failures. The function of
fracture, the explosion loading re-
at slow rates: the offset explosion loading was to
sulted in a helmet-type bulge at 120°
1. The metal grains at the notch ensure dynamic conditions for the ini-
F (50° C) and higher temperatures.
root are not subjected to the same tiation phase and to maintain soft-
high degree of triaxial constraint to spring (continued) loading on the "Temperature conversions will be ap-
plastic flow provided by the ultrasharp plate while the fracture was propa- proximated to the degree of accuracy im-
plied—in general, to nearest 5° F signi-
natural cracks. gated from the center to the edges. ficance.
94-s ] M A R C H 1971
The 160° F (70° C) bulge resulted range for the improved ship steels. weight. In practice, the DWT is con-
from the use of a much larger ex- The failure of the C,. test to ducted by loading the specimen as a
plosive charge than was applied for provide an invariant method for char- simple edge-supported beam with a
the remainder of the test series and acterization of the true transition tem- stop placed under the center position.
serves to illustrate the high degree of perature range features of steels em- The stop restricts the deformation to a
ductility. The temperature point of phasized the need for evolving a sim- very small amount; thus, the deforma-
fully ductile tearing is defined as the ple type of natural crack test for tion is kept constant for steels of
Fracture Transition Plastic ( F T P ) . routine laboratory use. This led by different yield strengths.
The fracture panorama presented 1953 to the invention and validation Figure 4 (top) presents a typical
by many test series of this type clearly of the Drop Weight Test ( D W T ) . The test series which defines the NDT
illustrated why ship fractures only oc- DWT was designed specifically for the temperature as the highest tempera-
curred at winter temperatures. The determination of the NDT tempera- ture of nil ductility break. The flat
significance of initiation, propagation, ture because of the critical importance break signifies that fracture initiation
and arrest features also becomes of this index to fracture-safe design. due to the small flaw occurred prior to
clear. The controlling temperature for Figure 4 illustrates the general the deveopment of significant plastic
fracture initiation due to small flaws is features of the DWT specimen and deformation. Figure 4 (bottom) illus-
obviously the NDT temperature. the effect of temperature on its frac- trates tests conducted without the
Fractures due to small flaws could not ture characteristics. The specimen stop. At NDT + 20° F (NDT + 10°
be expected to initiate in ship struc- features the brittle weld of the ex- C) and N D T + 30° F (NDT + 17°
tures above the N D T temperature be- plosion test. A saw cut across the weld C) the specimen can be deformed
cause gross plastic overloads are re- localizes the fracture of the weld bead plastically without causing fracture.
quired. to a single crack at the exact center of This performance clearly indicates
Excellent correlations were ob- the specimen. The weld crack pro- that a sharp increase in dynamic frac-
tained between the fracture per- vides the equivalent of a small thumb- ture toughness is developed above the
formance in the explosion test and the nail-size flaw with an ultrasharp tip. NDT temperature. Extensive use of
Cv energy transition curve for ship The brittle weld bead is fractured as the DWT has shown that the N D T
fracture steels. N D T fracture initia- near-yield-stress levels are attained as reproducibility is within ± 10° F
tion features are obtained as the ex- a consequence of dynamic loading of ( ± 3° C ) . This degree of reproducibil-
plosion test temperature falls below the specimen provided by a dropping ity should not be surprising in view of
the 10 ft-lb Cv transition temperature.
The FTE arrest transition is de-
veloped close to the 20 ft-lb transition
temperature index. The temperature
at which the Cr curve attains shelf
values corresponds to the FTP or full
ductility temperature. Thus, the initia-
tion, propagation, and arrest relation-
ships of ship fractures to the Cv curve 30°F
were clearly reproduced by the ex-
plosion test series.
The success of the explosion test in
providing a direct correspondence to 20°F
the service performance of the ship
steels suggested its utilization on a
broad front in studies of fracture initi-
ation, propagation, and arrest !0°F (NDT)
features. This was required in particu-
lar for the wide variety of steels for
which there was no detailed documen-
tation of service failure history. These
studies were also directed to investigat- 0°F
ing whether the Cv curve predictions
of the initiation and arrest transition
temperatures would hold for im-
proved ship plate steels. Unfortunate-
ly, these and other types of steels
indicated correlations which were in-
dexed to much higher C„ fracture NDT+3Q°F
energies and, therefore, higher relative
positions on the Cv curve. These ob-
servations were of crucial importance
because they negated the then gener- NDT+20°F
ally accepted conclusion that the 10
and 20 ft-lb Cv transition temperature
indices would provide for invariant
assessment of the service fracture
characteristics of steels. At the time NDT
there was additional distress over the
fact that the Cr test had provided an Fig. 4—Typical DWT series (top) which define an NDT temperature of 10° F
(—12° C). The sharp increase in dynamic fracture toughness of the metal
overoptimistic indication of the de-
above the NDT temperature is illustrated (bottom) by the tolerance for
crease in the transition temperature plastic deformation for tests conducted in the absence of a stop
LOAD
ymffttWrwrnm/T
3 FT
LIQUID NITROGEN 40 r
APPLIED
~ 30
;cr*^:
IMPACT' 2FT
SAW CUT cn 2 0 -
WELD
Fig. 7—Summary of tests for a wide variety of steels which indicate that These findings were of major conse-
the temperature range location of the CAT curve may be established by quence because they disclosed the spe-
temperature increment (At) reference to the NDT temperature. The points cific relationship between initiation
represent CAT or FTE determinations for different steels and arrest aspects of unstable frac-
96-s | M A R C H 1971
TENSILE
ULTIMATE FAD
STRESS STRESS LEVEL
FOR FRACTURE INITIATION
FOR SPECTRUM OF
FLAW SIZES
YIELD / / / / «• TltLU b I K t b b II
STRESS
I"
£YS
2
i»
STRESS LIMITATION
Fig. 8—Fracture Analysis Diagram (FAD) .Note that the stress level for plastic (over yield) fracture is not indexed because of
the lack of analytical procedures for its definition. Ultimate stress signifies only that maximum load and strain tolerance is
attained at FTP for specificflaw size cited. It obviously does not indicate the equivalent of the tensile test specimen maximum
load or maximum strain limits
ture. These relationships are evident ing flaw size, from the small-size flaw carefully catalogued with respect
from the temperature dependence of curve position to the CAT-curve posi- to the fracture initiation flaw size, the
two curves plotted in Fig. 7. The tion as a limit. From these consider- NDT temperature, the service failure
upper curve plots the rise in the level ations it became apparent that the temperature, and the stress level
of stress required for dynamic frac- corridor between small-flaw and CAT which had applied to the flaw region
ture initiation due to a small flaw. It is curves should encompass a family of of the structure. In addition, data
important to note that the rise of this curves of similar form, but related to became available for the effect of
curve represents a transition from a spectrum of flaw sizes. increasing flaw sizes (below NDT) for
elastic to plastic levels of fracture ship plate steels as the result of large-
initiation stress. The N D T indexes the Fracture Analysis Diagram (FAD) scale tests conducted by Battelle
temperature of the initial rise of this The coupling of flaw size consider- Memorial Institute investigators.
curve to above-yield-stress levels. The ations with transition temperature These various data provided the in-
sharp rise of the CAT curve also starts concepts evolved at the time that the formation required for assigning flaw
at the N D T temperature. Both curves engineering significance of fracture size values for the curves of the di-
evolve a simultaneous rise above the mechanics definitions of stress intensi- agram shown in Fig. 8, which was
N D T temperature because the dynam- ty factors began to be appreciated. evolved about 1960 and was defined
ic fracture toughness of the metal For a brittle metal the stress required as the Fracture Analysis Diagram
develops a strong temperature depend- for initiation should decrease in pro- (FAD).
ence starting at this reference tem- portion to the increase in the square The FAD provides a generalized
perature. Both curves are controlled root of the flaw size. Thus, very large definition of the flaw size, relative
by the same basic microfracture fac- increases in flaw sizes should be re- stress, temperatre relationships by a
tor, i.e., the increase in dynamic quired for fracture initiation, with de- "At" or "temperature increment"
cleavage fracture ductility of the met- crease of stress from yield magnitude reference to the N D T temperature.
al grains. to levels of low nominal load stresses. The location of the generalized di-
Since the CAT curve defines the The spectrum of flaw sizes that should agram to specific positions in the tem-
course of the stress-temperature rela- lie between the small flaw and CAT perature scale requires the experimen-
tionship for arrest, it follows that it limit curves was qualitatively predicta- tal determination of a single parame-
should also define the limiting stress- ble on this basis. Unfortunately, there ter—the N D T temperature. Thus, by
temperature relationship for the initia- were no experimenal data of fracture the simple procedure of conducting a
tion of unstable fracture. Fracture mechanics parameters required for DWT the other factors are made evi-
initiation could be expected only for calculating these flaw sizes at the dent by reference to the FAD.
conditions which provide for propaga- NDT temperature, or for establishing
Extensive international use of F A D
tion, i.e., in the region which lies to the temperature dependence of the
during the past decade has provided
the left of the CAT curve. Thus, the stress level above the N D T tempera-
positive documentation of its engi-
effects of increasing flaw size should ture.
neering practicality. All known cases
be restricted to lowering the stress The desirable integration of these of structural failures by unstable frac-
level for fracture initiation from plas- concepts directed the attention of ture have been analyzed to conform
tic levels to the limit elastic stress NRL investigators to failure analysis to the limits predicted by the FAD. In
level defined by the CAT curve. This as a means for defining the spectrum addition, continuing research of the
effect may be viewed as a shift of the of flaw size curves. Extensive studies transition temperature fracture prob-
fracture initiation curve with increas- of service failures were conducted and lem has evolved added scientific ra-
-s | M A R C H 1971
by successive 30° F (17° C) tempera- Fig. 10. Accordingly, one should not feet per second at the toe of the
ture increments above the NDT, re- use a design criterion in excess of real transition because the fracture process
duces the problem of fracture-safe requirements because this results in entails elastic-stress-induced cleavage.
design to a temperature reference sys- specifications of lower NDT and, The propagation rates fall off rapidly
tem of utmost simplicity. therefore, increased costs. with increasing temperature in the
The choice of steel is dictated by NDT to FTE interval because time-
the following factors: Shelf Considerations dependent deformation must then be
1. The lowest service temperature. The transition to a shelf level of developed for each grain prior to at-
2. The design reference point cri- fracture toughness marks the attain- taining cleavage fracture strains
terion chosen, i.e., NDT, N D T to FTE ment of a fully ductile mechanical (strain-induced cleavage).
midrange, FTE, or FTP. state which is both temperature and The metallurgical factors which de-
In order to make an appropriate strain-rate independent—that is, in- termine the specific temperature range
choice of steel, information is required creasing temperature or strain rate of the lower half of the transition are
as to the expected NDT frequency does not affect the high ductility different from those that determine
distribution. Figure 10 presents typi- which is inherent to the shelf level of the ductility level attained at the shelf.
cal frequency curve data for a variety low strength steels. The temperature transition range is
of conventional steels. This figure il- The shelf condition is entered grad- controlled by microcrack incubation
lustrates the wide range of choice that ually as the microfracture mode of the processes, i.e., the genesis and en-
is available. It also emphasizes that individual grains attains conditions of largement of grain-size-scale cracks.
metallurgical control of steel quality is high cleavage fracture ductility and The microcracks represent cleavage
an essential aspect of fracture-safe then fully ductile rupture. The ductile sites of individual crystals which crack
design. rupture process evolves by the open- preferentially, or the cracking of brit-
In general, the spread of NDT tem- ing up of small voids between grains, tle metallic phases such as carbides.
perature is in the order of 60° F (30° and particularly at sites of nonmetallic Grain size, the size and distribution of
C ) , with a high concentration in a 30° inclusions. The metal bridges between carbide phases, grain embrittling
F (17° C) span. If the yield strength these sites are elongated as tiny tensile effects of solute elements such as P,
and thickness are specified, informa- specimens which finally rupture in a N a , Oo, etc. have potent influence on
tion as to the average or the highest progressive (slow) ductile mode. Be- microcrack formation. These effects
expected N D T temperature can be ob- cause of these features the fracture are well known to the metallurgist and
tained from steel producers. Obvious- process is defined as void coalescence are used to suppress microcleavage
ly, there is a correspondence of rela- (void growth), i.e., the development and to favor slip processes. The transi-
tive cost to lower NDT temperature. and enlargement of microscopic tion temperature range is thus shifted
For example, as steels of progressively voids. to lower temperatures.
lower N D T are specified, a require- The propagation rates of brittle The level of shelf ductility is highly
ment for normalizing, fine-grain prac- fractures can be very rapid because sensitive to the relative cleanliness of
tice, alloy additions, and ultimately the cleavage of individual grains is a the steel. The presence of many sites
quenched and tempered (Q&T) heat high-speed process. These rates attain of void nucleation due to nonmetallic
treatment will ensue, as indicated in limiting velocities of several thousand inclusions promotes easy rupturing
THICK SECTIONS
CONVENTIONAL
C-Mn MILD STEELS
FREQUENCY
CURVE
35-40 kSI
NDT DATA Y.S. 22-28 KG/MM2
RANGE
-60 -40
-40
HIGH STRENGTH METALLURGICALLY OPTIMIZED STEELS
OPTIMUM ALLOY INCREASED
FOR THICKNESS PLUS •ALLOYS SMALL ADDITIONS
PLUS Q-T Q-T . PLUS A-C OF ALLOYS PLUS N
Y.S. Y.S.
80- 130 KSI , 50- - 6 0 KSI
KG/MM' KG /MM 2
I
-200 -180 -160 -140 -120 80
1 L
-120 -100 80 -60 -40 20 20
TEMPERATURE
Fig. 10—Representative NDT frequency distributions of commercial structural steels. The figure notations relate to
alloy contents and heat treatment factors as follows: < C / M n , decreased C to Mn ratio; A-R as-rolled, N, normalized;
A-C, accelerated cooling; and Q-T, quenched and tempered
T^\
h* 16
DIMENSIONS IN INCHES
100-s I M A R C H 19 7 1
TEMPERATURE -
Fig. 13—Significance of DT test transition features for steels Fig. 14—DT test transitions to various levels of shelf fracture
which develop high-shelf-level fracture toughness. The rise toughness. Note that with a decrease in shelf level fracture energy
in fracture energy and change in fracture appearance docu- there is a corresponding change from fractures with large lateral
ment a transition from plane strain (elastic) to high-duc- contraction to flat fractures with nil contraction features. The
tility plane stress (plastic) fracture. The transition curve decrease in shelf energy marks a transition from plastic (plane
represents a C-Mn steel plate of 1 in. thickness stress) to elastic (plane strain) fracture conditions
Fe-Ti alloy. The narrow weld is frac- gy curve traces the temperature characterize high strength steels in this
tured easily in loading and thus pro- course of the CAT curve from N D T frame of reference, as will be ex-
vides a reproducible sharp crack. It has to FTE. plained. The condition of low-shelf
now been establised that equivalent The D T specimen provides an inex- fracture toughness requires special
results may be obtained by the use of pensive method for determining the consideration for these steels because
a deep sharp crack produced by fa- full course of the transition tempera- increasing temperature does not
tigue or by slitting, and then sharpen- ture range from NDT to FTP. If the provide a solution for fracture-safe
ing a deep notch by a pressed knife design, as for the case of low strength
temperature transition rises only to
edge. DT specimens featuring a deep steels. The procedures by which con-
intermediate or low levels of shelf
flaw produced by any of these meth- siderations relating to fracture-safe
fracture toughness, the D T energy
ods are tested over a range of temper- design may be made for the shelf
curve also provides direct evidence of
atures using the pendulum-type ma- (strength) transition will be described
this characteristic. Figure 14 provides in detail. At this point it should be
chines shown in Fig. 12. The upswing schematic illustrations of DT energy
of the pendulum following the frac- recognized that the DT test specimen
transition curves featuring the same provides for independent assessment
ture defines the energy absorbed in the NDT temperature but different shelf
fracture of a standardized test section. of the transition temperature range
quality characteristics. The curves and shelf level characteristics of a
Figure 13 illustrates typical rela- which show high- and intermediate- steel; as such, it is a highly versatile
tionships of the DT test energy transi- shelf features, represent typical test test procedure.
tion curve to the NDT, FTE, nd FTP results for strong and weak directions
temperatures for a low strength steel of intermediate strength steels. The The D T test and the analytical
of high-shelf fracture toughness. At procedures for its interpretation have
curves which show intermediate- and
the N D T temperature the fracture is been evolved since 1964, and most
low-shelf characteristics are typical of
brittle and shows a flat, featureless notably in the period 1967-1969. The
steels featuring relatively high yield
surface devoid of shear lips—exactly need for such a test was paced by the
strengths. The low-shelf curve which
similar to the DWT fracture at NDT. rapid increase in the engineering utili-
shows no significant transition temper- zation of high strength steels, titani-
A sharp increase in the fracture energy ature effects is typical of ultrahigh
reading is recorded above the NDT um, and aluminum alloys. The analyti-
strength steels for both weak or strong cal interpretations are derived in part
temperature as increased ductility is directions, i.e., differences due to di-
developed by the metal grains prior to from principles of fracture mechanics
rection are of small magnitude. The theory which matured to technologi-
cleavage. The fracture surfaces de- notations of elastic and plastic frac- cal utilization during the late 1960's.
velop visible shear lips as the N D T ture emphasize the common mechani- Accordingly, an introduction to frac-
temperature is exceeded, and these cal features of the "temperature" and ture mechanics concepts are required
then become progressively thicker as "shelf" transitions, a change from before proceeding with discussions of
the temperature is increased to FTE elastic to plastic levels of fracture shelf (strength) transition aspects.
levels. As the shelf temperature is toughness.
entered the fracture no longer shows
signs of cleavage but becomes totally A shelf transition from high frac- Fracture Mechanics Tests
of the ductile, void growth type. The ture ductility to the brittle state which Fracture mechanics plane strain
FTE is located at the midpoint of the evolves as a consequence of an in- tests are designed for the measure-
DT energy transition curve and in- crease in strength level has been ment of very fine differences in frac-
dexes the transition from elastic to defined as a "strength transition." Be- ture toughness, at levels which relate
plastic stress-induced fracture. In cause of the strong influence of in- to the relatively brittle state. The tests
effect, the lower half of the D T ener- creasing yield strength on shelf frac- are not applicable to measurement of
ture toughness, it is informative to the full span of fracture toughness
STRESS FIELD
INTENSITY
cr.NOMINAL
CLIP GAGE
Fig. 15—Relationships of elastic and plastic stress fields to the plastic Fig. 16—General features of bend-type Krc test speci-
zone at crack tips for the case of plane strain constraint. As plastic mens. The stress level for fracture initiation (insta-
relaxation is developed (large plastic zone and crack tip blunting), bility) is defined by a plot of load vs. clip gage crack
the elastic stress fields are replaced by plastic strain fields. Elastic opening displacement. The failure stress (07) and
stress field " K " definitions are not possible for these conditions crack depth (a) provide for calculation of KTc by the
following generalized formula, Ku = Ci af\/ira, where
Ci is a constant specific to the crack geometry
from brittle to plastic levels.
Fracture mechanics test procedures
define fracture instability conditions in process of extension. visualized by considering the degree of
terms of the elastic stress field acting 3. A secant-offset instability which is through-thickness lateral contraction
ahead of the crack tip plastic zone. indicated by a deviation from elastic which is developed in the course of
Figure 15 provides a schematic illus- response of the COD gage, plus other fracturing edge-cracked specimens of
tration of a sharp crack with a small confirming evidence (such as ultrason- the K,e and DT types. Plane strain
plastic zone and the associated elastic ic detector) that the crack tip has signifies that the lateral (through-
stress field. The intensity of the stress moved slightly without becoming un- thickness) contraction parallel to the
field, which is represented by the stable. crack front is of very small (nil)
steepness of rise of the stress on ap- values. Plane stress signifies that
proach to the plastic zone, is defined All of these instabilities are consid- through-section yielding occurs with
by the parameter K,. Linear elastic ered acceptable in the determination notch blunting (plastic COD). In oth-
analyses have been evolved which of KIr values according to ASTM er words, for the plane stress case the
relate crack depth, crack geometry, recommended practices. In addition, crack is not effective in constraining
and nominal section stress to KT. The there are nonstandard definitions of the flow of the metal to a small plastic
Kr value at instability is defined as KIr values which are ASTM nonval- zone.
K,,„ i.e., the critical value of Kr. id, but are nevertheless widely used
with this qualification. The important The features of plane stress frac-
A typical fracture mechanics test point is that the K value signifies a ures are illustrated in Fig. 17. The
specimen is illustrated in Fig. 16. The measurement of the "first event" (i.e., small plastic zone of the plane strain
specimen features a deep fatigue the beginnings of separation of metal case is now replaced by a large plastic
crack carefully prepared to ensure grains at the crack tip) and does not enclave and features a surface dimple
maximum acuity. A clip gage is describe following events unless other which represents the equivalent of the
mounted at the notch opening to mon- information is provided, such as: neck region for a tensile specimen.
itor the crack opening displacement popin K,c, rising load Klc, secant- The high energy absorption of ductile
(COD). For a valid KIr determina- offset KIr, nonvalid Klc etc. (plane stress) fractures derives from
tion it is necessary to document that the requirement for continuously form-
"instability" is developed at nominal From an engineering point of view ing a plastic enclave region ahead of
elastic stress levels and that the clip it may be argued that a minute insta- the propagating tear. The large
gage COD trace is recording in the bility that is followed by increasing amount of plastic deformation in-
elastic range. In general, "instability" resistance to further extension of the volved requires the application of
signifies a detectable (by the COD crack is not of consequence to the plastic load stresses.
gage) forward extension of the crack structure. It is an event which occurs Plane stress fracture may be of
tip which may be of minute dimen- at the crack border while the crack tip low- or high-shelf characteristics. The
sions. It does not imply necessarily is blunted to some degree and, there- energy absorbed is related to the de-
that the instability results in fracture fore, leads to increased resistance to gree of through-thickness contraction
of the specimen. crack movement. which controls the size of the plastic
There are three types of instabili- The fracture mechanics nomencla- enclave. The degree of through-
ties: ture of plane strain is applied to brittle thickness contraction is controlled in
1. A nonarrestable "popin" instabili- fracture conditions which are mathe- turn by the critical strain which can
ty which leads to total fracture. matically definable by the Klc stress be endured by the metal grains prior
2. A momentary "popin" instability field parameter. The nomenclature for to rupture. The metallurgical quality
which is arrested and then requires plastic fracture is plane stress. The factors which represent the basic con-
increased load for further extension basic difference between plane strain trol mechanism of the total process
because the crack tip is blunted in the and plane stress fractures may be are best expressed at the microscale
102-s I M A R C H 1971
level. A steel with combined features
of high cleanliness (low void site
density) and high grain structure duc-
tility resists the incubation and en-
largement of microvoids. The inherent
microfracture ductility thereby forces
the development of large macroscopic
contraction and associated large plas-
tic enclave. Conversely, a steel of high
void site density combined with low
grain structure ductility will suffer
PLASTIC \
early enlargement and rupture of the STRESS ^
microvoid bridges. As a consequence,
low critical strain and small (or nil)
lateral contraction will result.
The plane strain condition is at-
tained when the lateral contraction CRITICAL
and enclave features are reduced to PLASTIC STRAIN
1 FOR RUPTURE
nil values. Since little flow is de-
I* 5 i » l
veloped in the through-thickness di- 1
J
rection, the Poisson-related flow in the
crack opening direction is minimized
and the deformation is limited to a
s **=!
-/ ' \
L0W-
V0ID-SITE
HIGH-
IID-SITE
VOID-SITE /*»p
narrow zone. The plane stress case DENSITY DENSITY
ENSITY \ |
/% S
starts with the beginning of through- LOW
thickness yielding, i.e., loss of con- \J 1 , HIGH
CRITICAL CRITICAL
STRAIN STRAIN
straint at the crack tip. Measurements
of plane strain fracture toughness may
be considered in terms of a "vernier
scale" measurement of crack tip duc- Fig. 17—Features of h i g h - d u c t i l i t y p l a n e stress f r a c t u r e as i l l u s t r a t e d by
tility, i.e., very fine differences. By t h r o u g h - t h i c k n e s s c o n t r a c t i o n a n d t h e d e v e l o p m e n t of plastic enclave
d i m p l i n g . T h e i n t r i n s i c v o i d site d e n s i t y q u a l i t y of t h e steel d e t e r m i n e s t h e
comparison, measurements of plane
critical plastic s t r a i n for r u p t u r e . A c c o r d i n g l y , m e t a l l u r g i c a l q u a l i t y con-
stress fracture for ductile metals re- t r o l s t h e degree of c o n t r a c t i o n , t h e d i m p l e size, a n d t h e m e a s u r e d level of
quire only gross scale definitions be- fracture toughness
LARGE
SECTION SIZE
OO . 11'
/ ,,|N HIGH-DUCTILITY
SMALL / PLASTIC FRACTURE
SECTION ;
SIZE /
/ ,
JL
'"2.0 CORRELATIONS
WITH A S T M - E 2 4 VALID K lc
WITH PLASTICITY
CORRECTED K K VALUES
RATIO
******** SELF-INDEXED
PLASTIC FRACTURE
MARGINAL
METALLURGICAL DUCTILITY HIGHLY DUCTILE
(CONSTRAINT CONTROLS)
_L_J L_J_ I I I I I I I I I I I I i i i
•V
DYNAMIC TEAR TEST ENERGY
Fig. 18—Schematic relationships of DT energy values to Ku and KIC/<jyB ratio values. The DT energy values are
indexable to these plane strain parameters for highly brittle and marginal conditions of metallurgical ductility,
i.e., for conditions such that the plane strain state is possible. The codes indicate the limits of experimental cor-
relations and the types of Kic measurements involved. For conditions of plane stress fracture, the DT test is self
indexing, i.e., it defines if the plane stress ductility is of low, intermediate, or high levels—see discussion of R
curve factors
1 ( KT \ Klc.
• FATIGUE c
CRACK \
\
\ K
Ty- jy 4.0 2.0
\KC
INTERIOR
s \
\ K \ \ ^ Klc
PLANE STRAIN 1.6 \ c W 1.3
2^ — \
1
\
SURFACE 1.0
\ W
W
Klc 1.0
PLANE STRESS »KC
0.4- - m- K
Ic
0.6
i i i I
2.5 10
THICKNESS (IN.)
cause both the absolute values and the limitations. These values have been Klc-DT relationship due to entry
differences are very large. shown to agree reasonably well with into the plane stress state is of major
At its present state of development ASTM-valid Klc data. However, it significance because it indicates a
fracture mechanics is restricted to should be noted that ASTM-valid Klc transition from elastic to plastic stress
measurement of the fine differences in values in excess of the 1.0 ratio are levels of fracture toughness. As such,
plane strain fracture toughness, i.e., generally of the secant-offset type, the it is of considerable importance to
differences in degrees of brittleness. engineering significance of which is fracture-safe design considerations.
The DT test specimen provides for not clear. In summary, the DT test There is no need for engineers to
measurement of the full span of frac- provides excellent correlations and become highly versed in fracture
ture toughness states from plane strain may be used to index Klc values mechanics theory for routine utiliza-
to high-ductility plane stress. The gen- reliably irrespective of whether these tion of the subject. The engineering
eral relationships which have been es- are obtained by ASTM-valid or by aspects may be expressed by simple
tablished experimentally between D T correction procedures. analysis charts with instruction as to
and Klc test values are illustrated in With an increase in metallurgical their use in fracture-safe design. The
Fig. 18. The general features of the ductility and DT test values, the plane discussions will now be aimed directly
correlations with ASTM-valid Kjc strain limit is exceeded (noted as infin- at achieving this degree of utilitarian
data are represented by the solid part ity (co) ratio) and the plane strain familiarization.
of the curve which extends to Kjc/crys fracture mode no longer applies. No Section size is an important consid-
ratios of approximately 1.0. The Klc further correlations can then be made eration in KIc testing and in the engi-
value relationship rises essentially between Klc and DT test energy. The neering application of fracture
linearly with the DT test energy and DT test energy values which rise to a mechanics principles. Section size es-
then develops a slight curvature. very high value (dashed part of the tablishes the flaw size that can be
Above the 1.0 ratio the available Klc curve) are self indexing and represent placed within a section with retention
data have been of the plasticity- levels of plane stress fracture tough- of plane strain conditions. Constraint
corrected type due to specimen size ness. The point of departure for the to metal flow at crack tips is increased
with increase in flaw size, provided
sufficient metal remains surrounding
the flaw to contain the plane strain
elastic stress fields. If plane strain
conditions are to apply, a significant
part of the flaw tip region must reside
in the equivalent of a semi-infinite
medium which does not provide for
mechanical "sensing" of free surfaces.
This aspect is best understood by
reference to the Klc specimen size
requirements for measurements of
valid KIc. Figure 19 illustrates sche-
matically that edge-cracked specimens
have KIc measurement capacities
which increase with increasing section
thickness. As the intrinsic metallurgi-
cal ductility of the metal is increased,
Fig. 20—Schematic i l l u s t r a t i o n of t h e physical s i g n i f i c a n c e of plane s t r a i n the plane strain fracture toughness
c o n s t r a i n t r e q u i r e m e n t s expressed in t e r m s of section t h i c k n e s s B a n d value and the section size of the speci-
surface flaw sizes men used for its measurement must
*
STUBBY FLAW i z i l - 3 ^ _
8.0
7.0 -
=
- 6.0
in
UJ
X
o
z - Q/
=• 5 . 0 —
X
W
S:
h- —
D- Q/
hJ -1 &l Q //
Q
4.0 — ty/ •V
• #
1 - $
_i
-J 3 . 0
<J
— 7
o —
-
i-
-
/ o>y
v y
° 2.0 TN /
-
1 / /
1.0
/
1/ / ^
- /
0 ^^\ i i i 1 V_
0:5 1.0 1.5 2.0 0.5
r
RATIO ^ RATIO
Ys ^Ys
Fig. 21—Relationship of flaw size and stress requirements for the initiation of plane strain fracture as a function of increase
Kic/o-ys ratios. The section size requirements are indicated by the B scale. The basis for calculating the graphical plots for
semielliptical surface flaws in tension is provided by the flaw size-stress relationship: Ku = —'-= o-y/wa where a = crack depth,
VQ
<r = nominal stress (P/A), and Q = flaw geometry parameter obtained from tables
increase also. If the intrinsic plane toughness is indicated by the following ments, as well as to section size. The
strain fracture toughness of the metal expression, as recommended by the two sets of curves relate to limit
is greater than can be measured for ASTM E-24 Committee: conditions of flaw geometries—stubby
the section size that is involved, say a and thin. The long thin flaw is more
fixed plate thickness, then the behav- severe than the stubby flaw because it
ior of the metal will be characterized S(in.) & 2 features greater constraint for the
by plane stress for reasons of inade- same nominal depth. The ratio 2.0
quate mechanical constraint. represents the limit of plane strain
It is important to note that the Klc For a KI<s/<r7B ratio of 1.0 a mini- fracture toughness. The value of plane
value is not a sufficient index of frac- mum plate thickness of 2.5 in. is strain fracture toughness in excess of
ture toughness—it must be referenced required; for ratios of 0.5 and 2.0 the the ratio 2.0 will be defined as an
to the yield strength. Low Kh. values respective minimum thicknesses are infinity ratio (°°), i.e., unattainable,
may relate to high plane strain frac- 0.6 and 10 in. irrespecitve of section and flaw size.
ture toughness for metals of low yield The general relationships of low In simple terms, the metal ductility
strength. These same values may sig- and high ratios to the size of the Klc becomes too high to permit the plane
nify low plane strain fracture tough- test specimen and to the relative size strain state and plane stress conditions
ness for a metal of high yield strength. of surface flaws is indicated schemati- apply.
In all cases it is essential to "think" cally by Fig. 20. Small section size and The determination of K l c values
ratio rather than in terms of the K,c small flaws suffice for plane strain for the transition temperature range is
value per se. The relationship of fracture initiation of low-ratio metals. in fact a measure of the mechanical
Kh./o-ys is basic to any definition of Conversely, large section size and state which applies to the cleavage of
plane strain fracture toughness be- large flaws are required for high-ratio the first few grains when the load is
cause it relates to the plastic zone size metals. The mathematical relation- applied slowly. The fracture of the
developed at crack tips. The test spec- ships are best expressed graphically as Klr test specimen is controlled by
imen thickness B required for meas- shown in Fig. 21 which relates ratio dynamic (KId) fracture toughness
urement of plane strain fracture values to flaw size and stress require- properties after the initial instability is
106-S | M A R C H 1971
inferred that all steels of thick section 1,000,000
should be mechanically brittle irre- PLASTIC SHELF
spective of metallurgical consider- FRACTURE ESTIMATE
ations. These postulates were unac- 12-IN. A 5 3 3 - B PLATE
ceptable to those who held the metal-
lurgical point of view that fracture 800,000
toughness was inherently controlled at 9
microscale. If true, the fracture PARTIAL
FRACTURE
mechanics postulate would have ne-
gated all of the carefully evolved m
physical metallurgy principles which 600,000 V
had guided the evolution of improved
steels by control of microstructure. STATIC PLANE
STRAIN LIMIT o
The basic issues were settled in cc
160 uj
1969 by investigations of thick-section
400,000
(6 and 12 in. thick plates) reactor-
grade steel of the A533-B type. West- 120
inghouse Research Laboratories
studies by Wessel involved K!(. tests to II
12 in. size. NRL studies involved DT 80
tests ranging from 5 / 8 to 12 in. size. 200,000
Large-scale KId tests of the same
steel were completed in 1970. 40
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