05O2 (LNCA) cathode material is successfully synthesized with the precursor
of Ni0.8Co0.15Al0.05(OH)2 (NCA) prepared by co-precipitation method. This method is considered simple and results high homogenities solution. LiOH was added to this precursor with a molar ratio of Li:M = 1.05:1. This experimental purposed is to find out influence of adding NaCl. The effect salt added in the precursor on the NCA characteristic was deeply investigated. We adding NaCl 1%, 3%, 5%, and 10% to LNCA. Optimum condition at 700oC for 10 h exhibits the high degree of crystal. The crystal parameter were examined using X-Ray Diffraction Characterization. LNCA with NaCl 3% added show the higher peak ratio and shows the same XRD pattern with NCA commercial preferences.