2 DETRMINACION DE TRAZAS
3 12/6/2013
Analito: Acido Peracetico, Acido Acetico y Peroxido de Hidrogeno
4
5 Curva de Calibracion
6 Contenido/Potencia/Valoración
26 1 3 0.0803
27 2 5 0.5530
28 3 10 1.2500
29 4 15 3.8557
30 5 30 8.1800
31
32 RESULTADOS
33 N 15
34 Coeficiente de Correlacion 0.9992
35 Pendiente b1 0.2790
36 Ordenada en el origen b0 -0.2289
37 Intervalo de confianza (IC(b1)) 0.239032551-0.318870131
38 CRITERIOS DE ACEPTACION
39 Coeficiente de Detrminacion (r2)= ³0.98 Laboratorios Sydenham S.A de C.V.
40 Intervalo de confianza (IC(b1))= No incluye el cero
Calle de la Rosa No. 38 B Col.10 de mayo
41 C.P 72270 Puebla. Pué.
42 T. + (52) (222) 2 34 70 28 / 2 34 69 27
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46 1 de 6
A B C D E F G
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49 GRAFICO:
C o n d u ct v id ad (m S)
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54 Curva de Calibracion
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55 8
f(x) = 0.2789513407x - 0.2288744799
6 R² = 0.9992148003
56 4
2
0
0 5 10 15 20 25 30 35
57
Concentración (ppm)
58
59 FORMULAS:
61 CALCULOS:
62 x y x2 y2 xy
63 1 0.06 1 0.0034 0.058
64 1 0.09 1 0.0076 0.087
65 1 0.10 1 0.0092 0.096
66 3 0.55 9 0.3036 1.653
67 3 0.51 9 0.2621 1.536
68 3 0.60 9 0.3552 1.788
69 5 1.23 25 1.5228 6.17
70 5 1.27 25 1.6205 6.365
71 5 1.24 25 1.5450 6.215
72 15 3.71 225 13.7864 55.695
73 15 3.91 225 15.2959 58.665
74 15 3.94 225 15.5472 59.145
75 30 8.20 900 67.1580 245.85
76 30 8.20 900 67.2400 246
77 30 8.15 900 66.3410 244.35
78 Sumatorias 162 41.76 3480 250.9980 933.673
79 26244 2 de 6
A B C D E F G
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81 b1 = 0.2790
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83 b0 = -0.2289
84
85 t0.975, n-2 = 2.365
86
87 Sy/x = 0.0902 260.4493 -9.5571 0.1058 0.00813919 0.0902174735
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89 Sb1 = 0.01688 -22764 -1517.6 -0.000658935 0.01687898
90
91 IC(b1) = 0.2390325506 0.3188701308
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125 3 de 6
Laboratorios Sydenham S.A de C.V.
A
VALVULA UBICADA LA LAMPARA ULTRAVIOLETA 2
2
VM12 (1) 84.39 0.741 83.65
VM12 (2) 85.43 0.741 84.69
PUNTOS DE USO UBICADOS LOOP
VPU1 (1) 85.66 0.741 84.92
VPU1 (2) 85.69 0.741 84.95
VPU2 (1) 84.89 0.741 84.15
VPU2 (2) 85.26 0.741 84.52
VPU3 (1) 85.43 0.741 84.69
VPU3 (2) 85.74 0.741 85.00
VPU4 (1) 85.16 0.741 84.42
VPU4 (2) 85.69 0.741 84.95
CALCULOS
Donde:
y= Conductividad Especifica de la Muestra
m= 0.279
x= Incognita
b= -0.2289
VM12 (1) X= 83.65-(0.2289)/0.279= 300.638 ppm
VM12 (2) X= 84.69-(0.2289)/0.279= 304.365 ppm
VPU1 (1) X= 84.92-(0.2289)/0.279= 305.190 ppm
VPU1 (2) X= 84.95-(0.2289)/0.279= 305.297 ppm
VPU2 (1) X= 84.15-(0.2289)/0.279= 303.756 ppm
VPU2 (2) X= 84.52-(0.2289)/0.279= 303.756 ppm
VPU3 (1) X= 84.69-(0.2289)/0.279= 304.365 ppm
VPU3 (2) X= 85.00-(0.2289)/0.279= 305.476 ppm
VPU4 (1) X= 84.42-(0.2289)/0.279= 303.397 ppm
VPU4 (2) X= 84.95-(0.2289)/0.279= 305.297 ppm
A
VALVULA UBICADA LA LAMPARA ULTRAVIOLETA 2
2
VM12 (1) 2.165 0.741 1.424
CALCULOS
Donde:
y= Conductividad Especifica de la Muestra
m= 0.279
x= Incognita
b= -0.2289
VM12 (1) X= 1.165-(0.2289)/0.279= 5.924 ppm
VM12 (2) X= 1.187-(0.2289)/0.279= 6.003 ppm
VPU1 (1) X= 1.171-(0.2289)/0.279= 5.946 ppm
VPU1 (2) X= 1.198-(0.2289)/0.279= 6.043 ppm
VPU2 (1) X= 1.140-(0.2289)/0.279= 6.032 ppm
VPU2 (2) X= 1.195-(0.2289)/0.279= 6.032 ppm
VPU3 (1) X= 1.197-(0.2289)/0.279= 6.039 ppm
VPU3 (2) X= 1.169-(0.2289)/0.279= 5.939 ppm
VPU4 (1) X= 1.151-(0.2289)/0.279= 5.874 ppm
VPU4 (2) X= 1.159-(0.2289)/0.279= 5.903 ppm
A
VALVULA UBICADA LA LAMPARA ULTRAVIOLETA 2
2
VM12 (1) 1.365 0.741 0.624
VM12 (2) 1.387 0.741 0.646
PUNTOS DE USO UBICADOS LOOP
VPU1 (1) 1.312 0.741 0.571
VPU1 (2) 1.398 0.741 0.657
VPU2 (1) 1.340 0.741 0.599
VPU2 (2) 1.395 0.741 0.654
VPU3 (1) 1.397 0.741 0.656
VPU3 (2) 1.410 0.741 0.669
VPU4 (1) 1.441 0.741 0.700
VPU4 (2) 1.419 0.741 0.678
CALCULOS
Donde:
y= Conductividad Especifica de la Muestra
m= 0.279
x= Incognita
b= -0.2289
VM12 (1) X= 1.365-(0.2289)/0.2790= 3.057 ppm
VM12 (2) X= 1.387-(0.2289)/0.2790= 3.136 ppm
VPU1 (1) X= 1.312-(0.2289)/0.2790= 2.867 ppm
VPU1 (2) X= 1.398-(0.2289)/0.2790= 3.175 ppm
VPU2 (1) X= 1.340-(0.2289)/0.2790= 3.165 ppm
VPU2 (2) X= 1.395-(0.2289)/0.2790= 3.165 ppm
VPU3 (1) X= 1.397-(0.2289)/0.2790= 3.172 ppm
VPU3 (2) X= 1.410-(0.2289)/0.2790= 3.218 ppm
VPU4 (1) X= 1.441-(0.2289)/0.2790= 3.329 ppm
VPU4 (2) X= 1.419-(0.2289)/0.2790= 3.251 ppm