microbes, many operational problems associated with paraffin, reservoir. Out of five reservoirs, A resevoir was identified to
emulsion, scale and corrosion are also significantly reduced. be potential candidates for MEOR application3,4,5.
Bokor field is located in the Baram Delta Area about 40 • Analysis on the crude properties of this reservoir
kilometers offshore Lutong (Miri) at a water depth of indicates low wax, low sulphur, low asphaltene and low
approximately 220 feet below msl (Figure 1). The porosities pour point.
range between 15 and 32% and permeabilities from 50 to 4000
mD. Oil gravities range from 19O to 22O API in the shallower • Biodegradation study indicates complete removal of
reservoirs (1500 - 3000 Ft. ss) to 37O API in the deep normal/branched alkanes and partial removal of
reservoirs (6300 Ft. ss). The reservoirs in the Bokor field can aromatics due to in-reservoir alteration.
be divided into two main groups i.e. the Main Reservoirs (A -
F) and the Deep Reservoirs (H - L). This study is focused on A • Core study: The product (MEOR) used is non-
reservoir which is the shallowest reservoir for the field. damaging to Bokor sandstone formation.
The application of MEOR seems to be attractive for Bokor • Rheology study: There is a slight viscosity reduction in
field mainly due to: - sample inoculated with microbes.
• Low recovery factor in major reservoirs (19 % - 27%)
• Emulsion breakout test: Samples collected for this
• Viscous oil (2 cp - 10 cp) produce from shallow study are found to have emulsion problem. These
reservoir emulsion are very stable at room condition The result
• Bokor data conform to the basic screening criteria of indicate that the product is capable of breaking-up the
MEOR application (Table 1) emulsion within 24 hours of inoculation for most
• In line with Petronas Initiative in promoting samples.
IOR/EOR technology application in Malaysia
• Geochemical Test: After inoculation, there is an
S creening C riteria
increase in the solubility of high molecular weight
component as a result of biosurfactant activity.
O il G ravity (°A P I) 10 to 50
Based on the above results, it can be concluded that there is
potential application of MEOR technology to improve oil
Tem perature (°F) < 270 recovery in A reservoir. In order to further investigate and
W ater S alinity (ppm C l-) < 100,000 evaluate the technology, pilot project was proposed for
P arafin w ax (% ) >=3 seleceted candidate wells.
pH 5 to 8
P revious biodegration Little or none Pilot Project Objective
A vg. P erm eability (m d) > = 20 m d
The pilot test was recommended to extend the laboratory the
P orosity (% ) > = 10
feasibility study to the field study. In July 2000, the pilot
O il viscosity (cp) 5 to 50
project was successfully carried out on three strings namely,
H 2 S (ppm ) < 10,000
B-1, B-2 and B-3. The locations of the strings on reservoir and
P ressure G radient (psi/ft) > 0.10
production performance status are shown in Figure 3.
W ater cut (% ) 10 to 50
A dedicated team was formed for the pilot project
Table 1 : Screening criteria and Bokor data implementation. The team comprises members from various
As shown in Figure 2, the process of the project has been disciplines. The specific objectives of the pilot project are : -
categorized into three main stages i.e. 1) feasibility study, 2)
pilot project implementation and 3) full field scale • To demonstrate the feasibility of microbial application in
implementation. This paper only discusses until the the Bokor field.
completion of the pilot project results implementation. • To assess the impact on oil production (incremental oil
gain and sustainability) during 5 - 6 months monitoring
Feasibility Study period.
The feasibility studies of MEOR technology application in • To justify the potential of future full field scale
Bokor field was carried out and completed in April 2000. implementation.
During the feasibility studies, the focus was on the Main
Reservoirs with priority on the shallowest reservoirs i.e. A
SPE 72125 MICROBIAL ENHANCED OIL RECOVERY (MEOR) TECHNOLOGY IN BOKOR FIELD, SARAWAK 3
• To gain experience and application knowledge in carried out as part of the other planned acidizing campaign.
microbial stimulation through planning, monitoring and Due to limited space on the platform, all equipment such as
evaluating the pilot. pumps, tanks and microbes products were placed on a barge.
Microbes products were sampled taken and tested prior to
mixing operation6. The microbes were mixed with water to
Performance Monitoring/Analysis Strategy for Pilot acquire the required concentration and subsequently injected
Project (bullheaded) into the wells
This section discusses the monitoring strategy that was Upon completion of injection, the wells were shut-in. The
developed for the project. Performance monitoring/analysis shut-in period has been extended from one week to five (5)
strategy was developed to effectively measure or assess the weeks to coincide with shutdown for maintenance works. The
performance of the project. advantages of this opportunity are zero production deferment
The following parameters were being monitored/tested: - during treatment and maximize the time for microbes’s
Wellhead Sample/Lab Monitoring/testing reaction in the reservoir.
• Compositional analysis Pilot Project Results
• Dynamic viscosity
This section discusses the production performance and
• Emulsion Stability (@ reservoir temp.)
wellhead sample results over the five (5) months period after
• API gravity
the MEOR treatment.
• Asphaltene, wax, Sulphur, pour point
• Formation water analysis & Bacteria (SRB) analysis 1) Production Performance Results
• Emulsion stability (on-site @ room temp.)
Production Performance Monitoring/Testing Production Baseline - Pre-MEOR production trends for
the three wells were generated to forecast the well
• Production well test (oil, watercut, FGOR, gaslift
performance without MEOR treatment. This is required in
injection rates)
order to assess the well production impact after the treatment.
• Tubing and Casing head pressures. The trends were generated by performing a decline/incline
• Sand production. curve analysis over the available historical production data
• BHP surveys (permeability, skin, productivity index). (10–15 years) for oil, watercut or GOR. In order to minimize
the effect of gaslift variation on production, the injection rate
Appropriate responsibilities were assigned to team members was closely monitored and controlled to its pre MEOR rates
to ensure smooth monitoring/analysis processes. The 5 – 6 (0.2 - 0.3 MMscf/d).
months monitoring plan was also generated and most B-1 Post MEOR Results - The well test results for the the
importantly the Key Performance Indicators for each data first two weeks indicate that the gross production has
were identified to measure the project performance. increased from 600 b/d (baseline) to 1500 b/d. Historical data
confirms the gross production for the string could only reach
Wellhead Sampling maximum 600 - 800 b/d eventhough after long shut in period.
Wellhead samples were collected at specified frequency This indicates that the sudden high gross production could be
through out the project monitoring stage. During the sampling due to the MEOR treatment. However, two weeks after the
exercise, a dedicated personnel was appointed to take the treatment, the gross production has dropped and maintained at
samples as well as to conduct the on-site analyses to ensure its baseline. Formation GOR and wellhead pressures were also
consistency of the results. To enable a reliable comparison of monitored and no change observed for these performances.
the MEOR treatment performances and effectiveness, pre Based on the above production test data and daily watercut
MEOR samples were also included in samples collection as a performance, the monthly average net oil production data was
baseline information. estimated. The production data for net oil and watercut
performance was then plotted as shown in Figure 4. Over the
Two type of samples were taken i) the crude oil and ii) the past 5 months (post MEOR), the average oil production
formation water samples. The samples were taken manually increased from 152 b/d to 334 b/d. The increase in oil
from the wellhead sampling port of each string. The crude production was mainly due to the drop in watercut
samples were labelled and the formation water samples were performance from 75% (pre MEOR) to average of 45%
preserved according to the test requirement. The preserved (watercut performance post MEOR fluctuated between 30% to
samples were sent to lab for detailed analyses. 82%). The average oil gains of B-1 for 5 months is 182 b/d
(equivalent to 120% oil incremental).
Pilot Project Execution
The project was successfully completed with a total project
costs of US $ 0.4 Million and a head of original planned
schedule. To minimise the operation cost, the project was
4 M. GHAZALI ABD. KARIM, MAT ALI HJ SALIM, ZAHIDAH MD. ZAIN, NOOR NAZRI TALIB SPE 72125
B-2 Post MEOR Results – Initially, the gross production Test on “as received’ wellhead sample for B-1 (Figure 9) at
for post MEOR was slightly higher. The gross production was the reservoir temperature of 48oC are in a small range of 21 to
declines and approaches the baseline. Formation GOR and 22 cP and 18 to 22.5 cP, respectively. As the temperature
wellhead pressures were also monitored and no change lower, the viscosity differences are significant. This can be
observed for these performances. The watercut (Figure 5) explained in a way that, at higher temperature, the emulsion
declines from 30% to 20% before increases to the baseline. tends to break up resulted in a viscosity close to the oil
The average oil gain for B-2 for 5 months is 41 b/d (equivalent viscosity. As the temperature lower, the emulsion starts to
to 15% oil incremental). form and therefore larger viscosity differences can be
observed, depending on the nature and severity of the
B-3 Post MEOR Results - The gross production for post
emulsified samples.
MEOR was higher than its baseline. Figure 6 shows the net oil
and watercut performance. For 5 months post MEOR, no Hydrocarbon Compositional Analysis
change observed in watercut but due to higher gross
production average oil gain of 41 b/d (equivalent to 36% oil The objevtive of the analysis is to detect any changes in the
incremental) was realized. properties of the crude oils. The bulk properties of the oils that
were used to monitor the effect of MEOR process on the
Overall Production Performance – As shown in Figure Bokor oils are API gravity, bulk composition, pour point
7, the average total oil gains from the three strings are 274 b/d temperatures, and wax, sulphur and asphaltene contents.
(equivalent to 47 % oil incremental). This is beyond the
expectation of the project which was estimated about 20% oil The API gravities show that the Bokor oils are considered to
gains. The higher oil incremental is mainly contributed from be heavy with values ranging from 17 to 20 °API. The low
the high watercut well, B-1. API gravities of the oils as supported by whole oil gas
chromatography, is due to the complete absence of normal and
Downhole Pressure Buildup Survey Results - Table branched alkanes removed during in-reservoir biodegradation
2 shows the downhole pressures buildup survey for the strings. by indigenous microbes and/or water washing taking place in
No permeability change observed . However, there was a the reservoir after accumulation.
slight improvement in skin and PI for the low permeability
wells, B-2 and B-3. This could be one of the causes that The API gravity of the samples show that there is not much
contributed the higher gross oil production as mentioned variation in the API values in samples collected after 6 hours,
above. 3 days, 2 weeks and 2 months compared to the pre-treatment
samples. This indicates that there is hardly any change in the
Table 2 : Pre and Post FBUS Results bulk properties of the oils with soaking time. The results, as
expected, are consistent with those reported in the feasibility
Pre Treatment Post Treatment studies. This finding is supported by other bulk property data
such as wax (1.0 to 2.8 wt %), asphaltene (0.03 to 0.13 wt%)
Well Permeability Skin Productivity Permeability Skin Productivity and sulphur (0.12 to 0.15 wt%) contents which do not show
(mD) Index (mD) Index
(stb/d/psi) (stb/d/psi) any significant change in the values with soaking time. The
very little or no variation in the bulk property values may be
B-1 1926 25 4 1901 27 4.6 explained by the fact that the Bokor oils accumulated in these
B-2 557 29 1.7 525 23 1.9 shallow A reservoirs have been biodegraded.
B-3 664 33 1.8 663 11 2.5
Bulk composition of the oils shows that the content of the
aromatics (45 to 60 %) is relatively very high in all the
2) Wellhead Sample Analyses Results samples at the expense of the saturates (34 to 49 %). This
Dynamic Viscosity classifies the Bokor oils as napthenic-aromatic oils. The shift
in the property of the oils from paraffinic to napthenic-
Dynamic viscosity tests were conducted for crude oil aromatic resulted from the removal of paraffins during in-
viscosity and ‘as received’ wellhead samples to measure the reservoir biodegradation. The high aromatic fraction in the oils
viscosity profile(viscosity vs temparature) of the samples relative to the saturates could be one of the reasons for the
before and after microbes injection (after 6 hours, 3 days, 2 high tendency of the Bokor oils to form emulsion. This is
weeks and 1 months of microbes treatment). because the aromatic compounds are more polar and therefore
Analyses on crude oil viscosity for B-1 (Figure 8), B-2 and relatively more soluble in water compared to the less polar
B-3 shows insignificant changes after MEOR treatment. This saturated hydrocarbon compounds.
is consistence with the findings during feasibility studies Whole oil gas chromatographic (GC) traces of all the Bokor
whereby whole oil gas chromatography traces suggest that oils indeed indicate that the normal and branched alkanes have
Bokor oil has been biodegraded to the extend that the normal been totally removed due to in-reservoir alteration or
and branched alkanes have been totally removed due to in- biodegradation. In order to see more clearly the changes in the
reservoir alteration leaving cyclic alkanes and aromatics. geochemical properties of the oils with soaking time (pre-
SPE 72125 MICROBIAL ENHANCED OIL RECOVERY (MEOR) TECHNOLOGY IN BOKOR FIELD, SARAWAK 5
treatment, 6 hours, 3 days, 2 weeks and 2 months), histograms settling time. Only high water cut well show some degree of
were plotted to reflect the distribution of the hydrocarbons reduction on the water cut level, whereas for the other two
contained in the oil. Results show that there is a slight wells no significant improvement on the water cut level.
difference between oils treated with demulsifier and those However the analysis is only based on a grab sample at that
without. particular time and not really representing the actual
performance of the water cut.
The analysis of oil treated with demulsifier show that there
is an increase in the lower molecular weight components at the Under controlled condition in laboratory, the samples were
expense of the higher molecular components with soaking allowed to settle for 7 days at both room and reservoir
time (Figures 10). This shows that there is a breakdown of temperature (48°C). The volume of emulsion, oil and water
higher molecular weight compounds to lower ones, which was monitored.
could result in a slight increase in the quality of the oils. This
The observation (Figure 12) for all samples at reservoir
slight increase in oil quality may not be detected or noted in
temperature (48°C), indicates emulsified crude breakout
the bulk property data as the bulk property analyses are less
completely into oil and water less than a week of laboratory
sensitive to changes as compared to whole oil GC or GCMS
time. This will slightly help the fluid to flow faster because the
which are very sensitive.
viscosity of the oil and water will be lower compare to
In the case of oils not treated with demulsifier, the viscosity of emulsion.
histograms of the hydrocarbon distribution show that there is
The trend of emulsion vs. time obtained for all three wells
an increase in the higher molecular weight components
clearly described the effectiveness of the microbial products in
relative to the lower ones in samples of up to two weeks
reducing emulsion stability. The effectiveness of the microbes
soaking time. One possible explanation for this is the increase
in breaking the emulsion decreases as the production time
in the solubility of the higher molecular weight components as
increases when most of oil near the wellbore is being
a result of biosurfactant activity of the microbes in dissolving
produced.
the insoluble hydrocarbons found in higher abundance in
biodegraded oils. These results, however, are just the opposite
of the samples treated with demulsifier. The actual reason for Formation Water sample analysis
this observation is still unknown but needs further laboratory The composition of the formation water before and after the
investigation to understand the behaviour of emulsions and the treatments has no significant change7. Based on the lab
chemistry of demulsifier. However, for sample with two analysis the composition analysis of the three wells showed a
months soaking time, there seems to be a decrease in the high typical value for a production wells in Baram Delta Area. The
molecular weight components compared to the two weeks sulfide level of the formation water is significantly low and no
sample. This suggests possible breakdown of high molecular significant change after the treatments (Figure 13).
weight components as seen in samples treated with
demulsifier.
Bacteria analysis
From the test conducted on-site8,9,10,11, the SRB activity in
Emulsion stability the three wells is very minimal, in other words the SRB is not
It is anticipated that the treatment will reduce the stability of detected by the SRB rapid Check kits (below detection level).
the crude oil emulsion. The stability of the emulsion is very Based on the experienced in other nearby fields, the SRB
important to be studied because it will provide information on Rapid Check method, cannot detect all the SRB present in the
net oil content (water cut), time to reach stable emulsion, water. However, theoretically high sulfide level in the
percentage of stable emulsion, effect of temperature and formation water will also an indicative of SRB activity in the
effectiveness of MEOR treatment. wells, and by analyzing at the trend of the sulfide and sulfate
levels in the formation water analysis, the level of sulfide
Based on the analysis done for all samples on site, it is detected was significantly low compare to the some higher
observed that the degree of emulsion stability has reduced value in other field in Baram Delta Area. It was observed that
significantly. Prior to the treatment, the emulsion separation there is a slightly increased of sulfide level in the formation
tested using gravity settling without demulsifier method, water immediately after the well opened up. The effect could
showed a very low rate. After the treatment, the emulsion be due to accumulation of Hydrogen Sulfide during the close
become less stable. For example, the rate of separation based in. However, the level is reduced to it baseline after continuos
on the 1, 4 and 24 hr settling, all the three wells showed a production. Hence it does confirm that, no significant SRB
similar trend or curves. Immediately after the open up of the activity in the three wells before or after the treatments.
well, the rate of emulsion separation increase to more than However for a future test, an alternative method such as
90%. However these effect only observed temporarily, after 2 prepared SRB media (SRB conventional test) can be
weeks opened up, the rate decreased and continuously reverted considered to analyze the present of SRB in the systems.
to it initial stages. Figure 11 shows the summary of emulsion
separation rate for each strings based on 1 hr, 4 hr. and 24 hr.
6 M. GHAZALI ABD. KARIM, MAT ALI HJ SALIM, ZAHIDAH MD. ZAIN, NOOR NAZRI TALIB SPE 72125
FAIR LE Y
BARAM
TO BSP
TO E11
BARONIA
BARAM
BAKAU
BETTY
WEST
LUTONG
BRUNEI
TUKAU
MCOT
BOKOR
SIWA
SARAWAK
OIL PIP
PIPELINE
ELINE
GAS PIPELINE
Figure 2 : Flowchart of the systematic approach for MEOR project in Bokor field
S u r v e illanc e
Product C rude and
Recomm endation C h aracterizations M o n itoring
Geochemical
A n a ly s i s D e s ig n Field Scale
Res ervoirs/ Pilot of Job
S a m p lin g O b jectiv es Execution
Implementation
w ells Pilot
Screening
R h e o lo g y
Study
Figure 3 : Location of the well and production Figure 4 : B-1 Net oil/watercut Post-MEOR Performance
performance status
B -1
MEOR begins
400
A Reservoir Net Oil
300
PD oil (bbl/d)
B-2 B-1 Post-
200 Historical data MEOR
B-3
203L Pre
100 ME
OR
215L
fault tren
d
0
Oct-95 Mar-97 Jul-98 Dec-99 Apr-01 Sep-02
Typical top structural map Time MEOR begins
100
well oil watercut GOR liftgas Reserves Watercut
rate (%) (scf/stb) (scf/stb)(MMstb) 80
(stb/d)
watercut(%)
B-1 160 75 180 0.3 0.2 60
B-2 290 30 150 0.3 0.3
B-3 150 50 150 0.3 0.4 40
Total 600 0.9 0.9
20 Reduction
in watercut
0
Mar-97 Jul-98 Dec-99 Apr-01 Sep-02
Time
Figure 5 : B-2 Net oil/watercut Post-MEOR Performance Figure 6 : B-3 Net oil/watercut Post-MEOR Performance
B -2 B -3
MEOR begins
MEOR begins 600
600 Net Oil
Net Oil 500
500
Post-
PD oil (bbl/d)
PD oil (bbl/d)
400 MEOR
400
300 300
200 200
Post- Historical data
100 MEOR 100
P re M E O
R tr e n d
0 0
Mar-97 Jul-98 Dec-99 Apr-01 Sep-02 Jul-98 Dec-99 Apr-01 Sep-02
Time
MEOR begins Time
100
MEOR begins
100
80 Watercut
Watercut
watercut (%)
80
60
watercut( %)
60
Figure 40
4 : B-1 Net oil/watercut Post-MEOR Performance
Figure 4 : B-1 Net oil/watercut Post-MEOR Performance 40
Figure 20
4 : B-1 Net oil/watercut Post-MEOR Performance 20
0
0
Oct-95 Mar-97 Jul-98 Dec-99 Apr-01 Sep-02 Jul-98 Dec-99 Apr-01
Time Time
10 M. GHAZALI ABD. KARIM, MAT ALI HJ SALIM, ZAHIDAH MD. ZAIN, NOOR NAZRI TALIB SPE 72125
VISCOSITY [cP]
600 3rd. post treatment = 21 cP
100
4th. post treatment = 22 cP
400
80
200
0 60
Sep 00 Nov 00 Jan 01 40
Oct 00 Dec 00 Avg
20
Sep 00 Oct 00 Nov 00 Dec 00 Jan 01 Avg 0
Pre MEOR 595 587 580 570 564 579 20 25 30 35 40 45 50
940 790 880 813 845 854
Post MEOR
TEMP [C]
Gains 345 203 300 243 281 274 1st. post-treatment2nd. post-treatment3rd. post-treatment4th.post-treatment
12 Breakdown of high
Crude oil Sample for B-1 mwt. to low mwt.
100 10 hydrocarbon
Viscosity at 48 C
pre- treatment = 19 cP
Abundance (Normalised %)
C11
C10
C12
C13
C16
C17
C18
C33
C14
C15
C34
C19+C20
C21+C22
C25+C26
C27+C28
C29+C30
C31+C32
C23+C24
TEMP [C]
pre-treatment 2nd. post treatment 4th. post treatment
1st. post treatment 3rd. post treatment Carbon Number
Pre-Treatment 1st.post (6 Hours) 2nd. post (3 Days) 3rd. post (2 Weeks) 4th. post (2 Months)
SPE 72125 MICROBIAL ENHANCED OIL RECOVERY (MEOR) TECHNOLOGY IN BOKOR FIELD, SARAWAK 11
Figure 11 : Emulsion stability results – Onsite measurement Figure 13 : Formation water analysis results
60 100
% Volume
Oil
mg/l
Emulsion 50 10
Water 40 1
30 0.1
20
0.01
10
0.001
0 Na Mg Fe K Cl S2- Cond TDS
1st Hr 4th Hr 1st Hr 4th Hr 1st Hr 4th Hr 1st Hr 4th Hr 1st Hr 4th Hr
2nd Hr 24th Hr 2nd Hr 24th Hr 2nd Hr 24th Hr 2nd Hr 24th Hr 2nd Hr 24th Hr Ca Ba St CaCo3 SO4 pH SG
Settling Time Sample Description
80
EMULSION (CC)
60
6 HRS
3 DAYS
40
2 WEEKS
20
2 MONTHS
Figure 14 : Mechanism of Emulsion stability reduction Figure 15 : Possible mechanism of watercut reduction
Pre MEOR
Coalescence of oil droplets discontinuos Kro Post MEOR Krw
phase
droplets
Kro Sor ..???
Microbes Krw
Coalesced Kro ..???
discontinuos
phase Krwpre
point of coalescence Kropost Krwpost
during wetting of
bacterial surface
Kropre
WATER
0 Sw Sw pre 1
OIL Ref: Cairns et.
all