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DC170271 DOI: 10.

2118/170271-PA Date: 30-December-15 Stage: Page: 310 Total Pages: 6

Managing Suspension Characteristics of


Lost-Circulation Materials in a Drilling Fluid
Sandeep D. Kulkarni, Dale E. Jamison, Kushabhau D. Teke, and Sharath Savari, Halliburton

Summary pending agents, such as fibers, of specific characteristics can


Lost-circulation materials (LCMs) are often used to mitigate the reduce the settling tendencies of the large LCM particulates. The
loss of drilling fluids into subterranean formations. Well-known reduction of settling tendencies of LCMs (or improved suspend-
LCMs include ground marble, graphitic carbon, and cellulosic ability) can help ensure uniform suspension of LCMs in the pill-
particulates. The carrier fluid’s ability to suspend the LCMs (min- preparation tank and proper suspension of LCMs in a wellbore
imize settling) is critical in high-pressure/high-temperature (HP/ annulus during a lost-circulation control operation.
HT) or inclined wells. This study provides methods to help deter- Rajabian et al. (2005) illustrated that the addition of fibers in
mine and manage suspension characteristics of LCMs in the fluid smaller concentrations (less than 1 vol%) into the fluid does not
with the aid of certain suspending agents (e.g., fibers). significantly alter its fluid rheology. Studies in oilfield literature
A detailed experimental study was conducted to evaluate the (Ahmed and Takach 2008) agree with these findings, where no
suspension of a range of LCMs in various drilling fluids and significant effect on fluid rheology was observed when fibers were
investigate the effects of suspending agents (e.g., fibers) on LCM added in small concentrations (viscosity increase less than 5%).
suspension. On the basis of the experimental data, semiempirical However, the addition of fibers in those small amounts signifi-
models were developed to help predict the influence of fibers on cantly affects the settling tendencies of the particulates (i.e.,
LCM suspension. The design parameters used in these models LCMs in a fluid, as presented in this work).
included fiber concentration, fiber density, number of fibers per Management of suspension properties of the LCMs with the
unit volume, and average fiber length and diameter. The modeling help of carefully engineered suspending agents (i.e., fibers) can
work discussed in this study also provides methods for tailoring provide a significant improvement to LCM technology. This can
the suspending-agent properties necessary for achieving effective minimize corresponding downtime as well as help prevent well-
LCM suspension in the fluid. bore-stability-related issues. This work can also be a part of a dril-
The uniform suspension of LCMs in the carrier treatment or ling-fluid design and help reduce costly and time-consuming trial-
drilling fluid is necessary during LCM pill preparation and during and-error attempts to design LCM treatments.
wellbore applications, such as a hesitation-squeeze operation.
Thus, the use of fibers to manage the suspension characteristics of Theory: Suspendability Modeling
LCMs in carrier fluids can help ensure efficient use of LCMs for Derived from the literature (Chhabra 2007), a suspendability
lost-circulation control. This method is particularly important in index has been defined for measuring the degree of suspension of
severe-loss zones where large-sized LCMs are used, as well as in a lost-circulation-material (LCM) particle (ability to resist set-
HP/HT or inclined wells, where maintaining LCM in suspension tling) in an unsheared (or weakly sheared) viscoplastic drilling
can be challenging. fluid, as shown in Eq. 1:

Si ¼ f ; . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ð1Þ
Introduction
Addition of lost-circulation materials (LCMs) to drilling fluids is where f signifies LCM properties, including qp ; dp ; sfp , and fluid
the most frequently used method for lost-circulation control. A properties, including q; s0 .
variety of LCMs are used within the industry depending on the
loss rate of the drilling fluid and material availability. Different
LCM Properties. qp is the density of the particle, and dp is parti-
types of LCMs include particles, flakes, cement gunk, and chemi-
cle diameter. The typical nonspherical shapes of the LCMs are
cal sealants. Three prominent aspects that influence the efficiency
accounted for by the shape factor sfp, which is dependent on the
of an LCM application have been studied in literature.
particle aspect ratio. It was considered that the particle con-
LCM properties, or the material properties of LCMs such as
centration was low enough to have no collective influence on the
crush strength or resiliency, have been studied by Kumar et al.
fluid properties.
(2010), Growcock et al. (2012), and Scott et al. (2012).
Formation properties, including fracture-width estimation by
use of formation properties such as Young’s modulus and Pois- Drilling-Fluid Properties. The drilling-fluid density is denoted
son’s ratio, have been studied by Alberty and McLean (2004), van by q. Because temperature and pressure can affect the fluid den-
Oort et al. (2003), Dupriest (2005), and Kumar et al. (2011). sity, the respective effects of thermal expansion and compressibil-
LCM/fluid interaction has been studied for the effect of LCM ity of the drilling fluid on its density were considered when
addition on equivalent circulating density (Whitfill et al. 2006) modeling suspendability. The yield stress of the fluid is denoted
and for the ability of the drilling fluid to suspend LCMs (Kulkarni by s0. The s0 value in Eq. 1 can be obtained for the LCM-carrying
et al. 2014). drilling fluids in various ways:
This study focuses on the LCM/fluid-interaction aspect, and • The 10-second or 10-minute gel strength obtained from a
provides novel methods to address the suspendability challenge viscometer, such as conventional Fann 35
for large LCM particulates that had been demonstrated in previ- • Low shear yield point obtained by applying Bingham plastic
ous literature (Kulkarni et al. 2014). The novel methods presented model to low shear data from the viscometer
in this study involve experiments and modeling to show that sus- • Herschel-Bulkley yield stress obtained by modeling the
shear-stress vs. shear-rate data from the viscometer
Note that the values depend on the temperature and pressure of
Copyright V
C 2015 Society of Petroleum Engineers
the carrier drilling fluid. Therefore, this parameter was also meas-
This paper (SPE 170271) was accepted for presentation at the SPE Deepwater Drilling and ured or adjusted to the desired temperature and pressure condi-
Completions Conference, Galveston, Texas, 10-11 September 2014, and revised for tions. In general, a rheometer may also be used to obtain the
publication. Original manuscript received for review 5 July 2014. Revised manuscript
received for review 19 May 2015. Paper peer approved 22 July 2015. yield-stress property of the drilling fluid.

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Si < 0.5 No suspendability


0.5 ≤ Si < 1 Weak suspendability
Si ≤ 1 Good suspendability

Table 1—Si parameter to determine LCM suspendability in LCM/


LCMT fluid systems.
Aged cell

representative fluid are discussed next. Appendix A (Table A-1)


shows formulation for the water-based drilling fluid. After formula-
tion, the drilling fluid was hot-rolled at 150 F for 16 hours before
performing the suspendability tests with the LCM and fibers.

LCMB LCM Particulates. LCM particles (ground marble) of specific


size ranges were obtained by sieving different grades of ground
marble, as shown in Table 2. The sample was obtained by use of
a sieving process with US mesh standard test sieves. The density
of the selected ground-marble material was observed to be 2.7 g/
cm3, as obtained from a helium ultrapycnometer.
Fig. 1—Snapshot of aged cell (glass liner) after aging for 2
hours at 150 F. Fibers. Polypropylene fibers of various lengths (3, 4, 6, 8, and 12
mm) were used in this study. The diameter of these fibers was 21
Suspendability Index Si. Si is defined as the ability of the LCM mm. The poplypropylene density was 0.9 g/cm3. The fibers were
particulates to resist settling in a drilling fluid. In the earlier work added to the fluid in the amounts of 0.5 to 6 lbm/bbl (ppb).
by Kulkarni et al. (2014), several experimental suspendability
tests (the test method described in the Methodology section in this Experimental Methodology
study) were carried out on various LCM/fluid combinations and
Fann 35 Viscometer Rheology and Mud Weight. The rheology
then the experimental data were incorporated in Eq. 1, to derive
of the hot-rolled drilling fluid was measured at 150 F (Appendix B,
semiempirical models that predict the suspendability of an LCM
Table B-1). It is typically reported in lb/100 ft2. The low shear yield
in a given drilling fluid. The models suggest that the Si parameter,
point was measured as [2(dial reading at 3 rev/min) – (dial reading
calculated for a given LCM/fluid system, is indicative of the LCM
at 6 rev/min)]. The 10-second and 10-minute gel strengths were
suspendability in that fluid. If Si > Sicirt , where Sicirt is the criti-
also measured after leaving the presheared sample under static con-
cal value of the determined Si value from the experimental study,
dition for 10 seconds and 10 minutes, respectively, and then obtain-
the particle will not settle in the suspending viscoplastic drilling
ing the maximum dial reading at a 3-rev/min condition. The mud
fluid. However, if Si < Sicirt , particle settling would begin. The
weight of the fluid was measured by use of a standard mud balance.
value of Sicirt is expected to vary with the method of determining
yield stress. The semiempirical models derived by Kulkarni et al.
(2014) and the criteria shown in Table 1 for the Si parameter can Lost-Circulation Material (LCM)/Fiber Uniform Mixing With
be used to help predict suspendability of an LCM in a given fluid. Fluid. A selected size of the LCM at a specific concentration (40
For several drilling fluids carrying large and/or high-density ppb, or 4–5 vol%) and the polypropylene fibers of a specific size
LCM, weak or no suspendability was observed (i.e., Si < 1). In and concentration were added to the drilling fluid (of given den-
this work, methods/models are provided to help improve suspend- sity and rheology) and the mixture was mixed thoroughly with a
ability in those LCM/fluid systems. When fibers are added to the spatula. The uniform mixture was then poured in a glass liner,
fluid, they act as suspending agents for the LCM. Thus, the for- which was kept in a stainless-steel aging cell.
mula for suspendability index must be modified to take into
account the effect of fiber characteristics: Suspendability Test. The stainless-steel aging cell containing
the LCM/fiber/fluid mixture in a glass liner was placed in the
Si ¼ f ; . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ð2Þ static oven at 150 F and aged for 2 hours (Fig. 1). After aging, the
system was allowed to cool down in a water bath for 10 minutes.
where f is LCM properties, fluid properties, and suspending agents The distribution of the LCM in the static-aged mixture was
such as fiber properties, and the fiber properties are /f ; lf ; investigated by separating the mixture in the glass liner in two
df ; qf ; and sf . The suspendability of the LCM would be influenced equal sections: the top and bottom halves. The fluid in the top half
by various fiber characteristics: vol% fiber concentration (/f), of the liner was slowly poured out to cause minimum disturbance
fiber length (lf), fiber diameter (df), fiber density (qf ), fiber number in the fluid. The LCM quantities in each section were separated
density (nf), and fiber stiffness (sf). The scaling parameters [e.g., from fluid mixture by filtering it through a 50-mesh US standard
fiber-length to LCM-particle-size ratio (lf / dp] and fiber-diameter/ test sieve and washing the LCM/fiber on the sieve with water to
particle-size ratio (df / dp) can also affect fiber contribution to the remove any adhered mud. Usually, the fibers are also washed
LCM suspendability. away with mud during cleaning. The separated LCM particles
were dried in an oven at 220 F and then cooled and weighed.
Experimental Study: Materials The quantities of LCM in the retained top- and bottom-half
sections of the glass liner were indicated as LCMT and LCMB,
Drilling Fluid. Lost-circulation-materials (LCMs) and fibers were
respectively. The degree of LCM suspendability is quantified in
tested by use of several fluids in this study; tests conducted with a
Eq. 3 in terms of percentage of LCM retention in the top-half sec-
tion of the glass liner (percentage of LCMT) obtained after the
Size Sieving Mesh LCM Size dp (µm) aging of the sample:
1 –30 mesh +35 mesh 500–600
2 –18 mesh +20 mesh 850–1000 LCMT
Percentage of LCMT ¼  100: . . . . . . . ð3Þ
3 –12 mesh +14 mesh 1410–1680 LCMT þ LCMB
Table 2—Ground-marble LCM particles of different sizes retained In a situation where there is no (zero) settling of LCM particles
between corresponding sieving meshes. during aging, suspension in the glass liner would remain

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T T
LCM Size dp (µm) LCM After Aging (%) Si Fiber Length and Concentration LCM After Aging (%) Si
500–600 4 8. 5 1. 6 4 mm, 0.5 ppb 7.2 0.63
850–1000 45 1 8 m m , 0 .5 p p b 1 8 .7 0 .8
1410–1680 7 0. 57 12 mm, 0.5 ppb 43 1 .1
T
Table 3—Percentage of LCM retention in top-half section of glass Table 4—Experimentally retained percentage of LCM and Si for
liner (percentage of LCMT) and Si for suspension of different sizes of addition of different-length fibers to the LCM/fluid system of ground-
LCM in the selected drilling fluid (17 lbm/gal and low shear yield marble LCM (1410–1680 mm) and selected drilling fluid (17 lbm/gal
point 5 5). and low shear yield point 5 5).

completely uniform (i.e., LCMT  LCMB, or percentage of Effect of Fiber Length on LCM Suspendability. Table 4 illus-
LCMT  50%). On the contrary, when all the LCM particles sink trates that when the concentration of the polypropylene fibers in
to the bottom during aging, LCMT  0 or percentage of the fluid was maintained (0.5 ppb), the length of the fibers signifi-
LCMT  0%. If some partial settling occurs during the aging pro- cantly influenced suspendability of the LCM particulates. With 4-
cess, then 0% < percentage of LCMT < 50% (considering no mm-long fibers, the ground-marble particles (1410–1680 mm)
upward motion of LCM in the fluid, because LCM is generally exhibited effectively no improvement to suspendability (percent-
considered to be heavier than the fluid). For the LCM distribution age of LCMT  7%). On the contrary, suspendability increased to
after aging, it was considered that a condition of 40% < percentage of LCMT 18.7% when 8-mm-long fibers were used
percentage of LCMT  50% indicates a good-suspendability con- at the same concentration. The suspendability was further im-
dition. Conversely, 5% < percentage of LCMT  40% was con- proved drastically—percentage of LCMT  43%, or good sus-
sidered to be a weak-suspendability condition and percentage of pendability—when 12-mm-long fibers were used (at the same
LCMT  5% indicated no-suspendability condition. The same concentration). Thus, fiber length has significant influence on the
tests were repeated for different sizes/concentrations of the fibers suspendability of LCM particulates.
added along with the LCM particulates to the drilling fluids. The Table 4 also shows values of the suspendability index Si by
repeatability of the test results was checked and the observed use of Eq. 2, where the experimental data were used to develop
standard deviation for the experimental error while measuring the correlations to accommodate the effect of fiber characteristics.
percentage of LCMT was 6 2%. The correlations successfully demonstrate the effect of fiber
length on LCM suspendability. Si only slightly increases (0.57 to
Results and Discussion 0.63) with the addition of 4-mm fibers (0.5 ppb) to the given
Lost-Circulation-Material (LCM) Suspension in the Drilling LCM/fluid system. However, with 8-mm-long fibers, Si increases
Fluid (No Fibers Added). First, the ground-marble LCM par- further (Si  0.80), which is consistent with the corresponding
ticles were tested for suspendability in the selected drilling fluid. increase in experimentally obtained percentages of LCMT. The
Table 3 shows experimentally obtained percentages of LCMT for correlations are further verified where the Si calculations indicated
the three different-sized ground marbles added to the drilling fluid good suspendability (Si  1) upon the addition of 12-mm fibers of
in the amount of 40 ppb. Consistent with the qualitative observa- the same concentration.
tions, small-sized 500- to 600-mm particles and medium-sized
850- to 1000-mm particles demonstrated good suspendability
(40% < percentage of LCMT  50%) in the given fluid. The Effect of Fiber Concentration on LCM Suspendability. Table 5
large-sized 1180- to 1400-mm particles showed weak suspendabil- shows that the concentration of the fibers significantly influences
ity (percentange of LCMT  7%). the suspendability of the LCM particulates. The experimental data
Table 3 also shows values of the suspendability index Si by showed that the suspendability of ground-marble particles
use of Eq. 1 and dependent on the properties of the ground marble (1410–1680 mm) increased from percentages of LCMT  7.9% to
(density and size/shape) and the selected drilling fluid (yield stress 47% when the concentration of the 6-mm-long fibers increased
and mud weight) used for the previously discussed experiments. It from 0.5 to 2 ppb. Similarly, the suspendability of the LCM was
was evident that Si  1 for smaller- and moderately sized LCM observed to increase from percentages of LCMT  20% to 48%
showed good suspendability, whereas the suspendability index when the concentration of the 3-mm-long fibers increased from 3
was much smaller (Si  0.57) for the larger-sized LCM that to 6 ppb.
showed weak suspendability. This analysis confirms correlations Table 5 also shows values of the suspendability index Si by use
developed in the previous work (Kulkarni et al. 2014). of Eq. 2, where the experimental data were used to develop correla-
To improve the suspendability of the large ground-marble par- tions to accommodate the effect of fiber characteristics. The corre-
ticles (1410–1680 mm) in the selected drilling fluid, addition of lations successfully demonstrated the effect of fiber concentration
fibers was attempted. Several experiments were conducted with on the LCM suspendability. The Si calculations showed Si < 1
various sizes and concentrations of polypropylene fibers to inves- where addition of fibers with lower concentrations did not improve
tigate the ability of fibers to improve LCM suspendability. The the LCM suspendability significantly (percentage of LCMT 
experimental data were analyzed to develop correlations (by use 40%). In addition, the Si calculations indicated good suspendability
of Eq. 2), which could be used to predict LCM suspendability in (Si  1) where the addition of fibers in sufficient concentrations led
the presence of fibers on the basis of fiber characteristics, such as to percentage of LCMT > 40%. Note that the change in rheology
fiber length/concentration. attributed to the addition of fibers in the discussed amounts was
less than 10%, as demonstrated in Appendix B.
The discussed work shows that LCM suspendability is influ-
Fiber Length and Concentration
T
LCM After Aging (%) Si enced by both the length and concentration (ppb or vol%) of
added fibers. The higher the fiber length (up to 12 mm), the lower
6 mm, 1 ppb 7 .9 % 0 .7 5 the amount of fibers (ppb or vol%) required to achieve good LCM
6 mm, 2 ppb 4 7% 1.1 suspendability. This behavior is captured in modeling by correlat-
3 mm, 3 ppb 2 0% 0.8 ing Si with characteristic dimensionless concentration of the fibers
3 mm, 6 ppb 4 8% 1 defined as nf  l3f , where nf is fiber number density and lf is fiber
length. Fig. 2 shows model predictions for how polypropylene
Table 5—Experimentally obtained percentage of LCMT and Si for fibers can be used to achieve good LCM suspendability for 1410-
addition of different amounts of fibers to the LCM/fluid system of to 1680-mm ground-marble particles in the selected drilling fluid.
ground-marble LCM (1410–1680 mm) and selected drilling fluid (17 Fig. 2 shows that, if the fiber length is 5 mm, a concentration of 2
lbm/gal and low shear yield point 5 5). ppb of these fibers is required to achieve good suspendability of

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7 Conclusions

Fiber Concentration (ppb)


6 • The experimental work demonstrated that lost-circulation-mate-
5
rial (LCM) particles can settle severely in typical drilling fluids
in several cases. Therefore, determination and control of LCM
4 suspendability is important.
3 • LCM suspendability (or settling resistance) in the fluid can be
2
improved by use of suspending agents, such as fibers, of spe-
cific characteristics.
1 • Both length and concentration of added fibers influence LCM
0 suspendability.
3 4 5 8 10 12 • The suspendability-index models were modified to account for
Fiber Length (mm) the effect of fiber characteristics on LCM suspendability, and
the model predictions are in excellent agreement with the ex-
Fig. 2—Length/concentration chart for the amount of polypro- perimental data.
pylene fibers required to achieve good suspendability for 1410-
to 1680-lm ground-marble particles in the selected drilling fluid
• Evaluation of LCM suspension properties and, accordingly,
(17 lbm/gal and low shear yield point 5 5). mitigation of the LCM-settling challenges by use of the dis-
cussed methods/models can help ensure effective lost-circula-
tion control, particularly for high-pressure/high-temperature
and inclined wells.
the LCM. However, if the fiber length is 10 mm, then only 0.75 ppb
of these fibers are sufficient to achieve the same suspension effect.
The correlation can be further extended for application on a Nomenclature
mixture of fibers of different lengths added to the fluid to achieve df ¼ fiber diameter (mm)
LCM suspendability. dp ¼ particle diameter (mm)
lf ¼ fiber length (mm)
Field Application LCM ¼ lost-circulation materials
This refers to a case study at a well drilled through highly frac- LCMB ¼ quantity of LCM retained in the bottom section of the
tured carbonate formations (Mississippi lime formation) in north- glass liner (g)
ern central Oklahoma, USA, where lost-circulation occurrence is LCMT ¼ quantity of LCM retained in the top section of the glass
very common. In this geographical area, during the past 2 years, liner (g)
an average nonproductive time associated with lost circulation nf ¼ fiber number density (mm3)
was as high as 60%. On this particular well, the lost-circulation ppb ¼ pounds per barrel
treatment involved application of several large-sized-particulate sf ¼ fiber stiffness (N/m2)
lost-circulation materials (LCMs) added at high concentrations sfp ¼ particle shape factor
to the fluid to make LCM pills; however, the losses were never Si ¼ suspendability index
cured completely. Si–crit ¼ critical value of the determined value based on the ex-
One possible reason for the LCM pill to be ineffective was perimental study
considered to be the settling of large LCM particulates in the pill, T0 ¼ drilling fluid yield-stress (lbm/100 ft2)
which hinders the right-sized LCMs reaching to the fractures. qp ¼ density of the particle (g/cm3)
Fibers (12-mm length, 1-ppb concentration) were added to the q ¼ drilling fluid density (lbm/gal)
LCM pills expecting that they would prevent LCM settling, /f ¼ fiber concentration (g/cm3)
improving suspendability and LCM effectiveness. qf ¼ fiber density (g/cm3)
The laboratory experimental tests and the previously discussed
derived models confirmed that the addition of fibers to this LCM
pill helped suspension of the LCM particulates (minimized set-
tling); in turn, this also improved the LCM performance on the Acknowledgments
industry-accepted standard laboratory particulate-plugging appa- The authors thank the management of Halliburton for permission
ratus (PPA) test, as shown in Table 6. The slotted disk in the PPA to present this work.
simulates the fractures in the wellbore and the slot-plugging test
is widely used in the industry to test the plugging efficiency of
LCM particulates. It is expected that fibers not only help to mini- References
mize settling of the large LCMs, but also contribute to form a Ahmed, R. M. and Takach, N. E. 2008. Fiber Sweeps for Hole Cleaning.
good plug. Presented at the SPE/ICoTA Coiled Tubing and Well Intervention
The solution of LCM with fibers was applied to the wellbore. Conference and Exhibition, The Woodlands, Texas, 1–2 April. SPE-
A 40-bbl LCM pill comprising engineered composite of 120 ppb 113746-MS. http://dx.doi.org/10.2118/113746-MS.
of large-sized LCM along with the fibers (12-mm size, 1-ppb con- Alberty, M. W. and McLean, M. R. 2004. A Physical Model for Stress
centration) was mixed with the fluid and pumped downhole. The Cages. Presented at the SPE Annual Technical Conference and Exhibi-
LCM pill was spotted and shut down the well for 2 hours. After tion, Houston, 26–29 September. SPE-90493-MS. http://dx.doi.org/
this time, mud was circulated and full returns were observed. 10.2118/90493-MS.
Thus, the lost circulation was successfully cured and the same so- Chhabra, R. P. 2007. Bubbles, Drops and Particles in Non-Newtonian Flu-
lution was used in the area on several wells. ids. New York: Taylor & Francis.

Particulate Comb inations PPA Test Result


120-ppb large-sized-particulate LCM Slot remains unplugged, total fluid
loss
120-ppb large-sized-particulate LCM + fibers Slot plugged, minimal fluid loss
(12 mm, 1 ppb)

Table 6— PPA test results (on 2-mm slotted disk at 4,000-psi differential) on particulate combinations
with and without fibers.

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Dupriest, F. E. 2005. Fracture Closure Stress (FCS) and Lost Returns tation of paper AADE-11-NTCE-19 given at the AADE National
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dam, 23–25 February. SPE-92192-MS. http://dx.doi.org/10.2118/ Rajabian, M., Dubois, C. and Grmela, M. 2005. Suspensions of Semiflexi-
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Lost Circulation Materials in a Drilling Fluid. Oral presentation of pa- March. SPE-151227-MS. http://dx.doi.org/10.2118/151227-MS.
per AADE-14-FTCE-24 given at the AADE Fluids Technical Confer- van Oort, E., Gradishar, J., Ugueto, G., et al. 2003. Accessing Deep Reser-
ence and Exhibition, Houston, 15–16 April. voirs by Drilling Severely Depleted Formations. Presented at the SPE/
Kumar, A., Savari, S., Whitfill, D., et al. 2010. Wellbore Strengthening: IADC Drilling Conference, Amsterdam, 19–21 February. SPE-79861-
The Less-Studied Properties of Lost-Circulation Materials. Presented MS. http://dx.doi.org/10.2118/79861-MS.
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Appendix A—Formulation of the Base


Drilling Fluid
After formulation, the drilling fluids were hot-rolled at 150 F for
16 hours before performing the suspendability tests with the LCM
particulates.

Additives Concentration (p pb) Mixing Time (minutes)


NaCl brine (2 40, 000 ppm) A s r eq ui re d –
Viscosifier I 0.65 10
Viscosifier II 1 10
Filtration control agent 2.0 10
Barite As required 10
Citric acid/pH adjustment 0.15 5
Mud weight 17 lbm/gal
pH range 9±0.3
Hot roll temperature (16 hours) 150°F

Table A-1—Formulation of base drilling fluid.

Appendix B—Rheology Data for the Formulated


Base Drilling Fluid and With Addition of Fibers to
the Fluid

Base Drilling Fluid + Fibers


Base Drilling Fluid Dial (3 mm, 6 ppb) Dial Reading
2
Reading (lbm/100 ft ) (lbm/100 ft2)
600 rev/min 127 129
300 rev/min 84 85
200 rev/min 67 67
100 rev/min 46 46
6 rev/min 9 10
3 rev/min 7 8
10-second gel 7 8
10-minute gel 9 10
Plastic viscosity ( c p) 43 44
2
Yield point (lbm/100 ft ) 41 41
Low shear yield point (lbm/100 ft2) 5 6
º
Table B-1—Fann 35 rheology data (at 150 F).

314 December 2015 SPE Drilling & Completion

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DC170271 DOI: 10.2118/170271-PA Date: 30-December-15 Stage: Page: 315 Total Pages: 6

Sandeep D. Kulkarni is a principal technical professional with Kushabhau D. Teke was formerly a senior scientist with Hallibur-
Halliburton. He has been working for Halliburton Baroid for ton; he was with Halliburton for 6 years, until 2013. Teke’s
approximately 5 years. Kulkarni’s areas of interest include dril- research interests include shale inhibition, barite sag, and lost
ling-fluid rheology and hydraulics, lost circulation, cuttings circulation of drilling fluids. He has authored or coauthored
transport, barite sag, and particle-size measurements. He more than 10 technical papers and holds three patents. Teke
holds five granted patents in the area of drilling fluids and has holds a master’s degree in chemistry from the University of
presented 19 technical papers in various SPE and American Pune, India.
Association of Drilling Engineers conferences. Kulkarni holds a
Sharath Savari is global technical adviser with Halliburton and
PhD degree in chemical engineering from City University of
New York. has 8 years of experience in the oil and gas industry, all with
Halliburton. He is the subject-matter expert for Halliburton on
Dale E. Jamison is a technology fellow with Halliburton for lost-circulation prevention, lost-circulation-material solutions,
Baroid, with more than 39 years of industry experience. His pres- and field applications. During his career, Savari has authored
ent research interests and areas include lost circulation, tran- or coauthored approximately 25 presentations in various SPE,
sient rheology, non-Newtonian hydraulics simulations, and real- American Association of Drilling Engineers, and International
time fluid-testing hardware. Jamison successfully pioneered Association of Drilling Contractors conferences. He holds five
the drilling-fluid hydraulics software at Baroid approximately 20 patents. Savari has served in a variety of professional capaci-
years ago. He holds 37 patents and has authored or contrib- ties at SPE, including as a steering committee and program
uted to more than 30 technical papers. Jamison holds a me- committee member at six SPE conferences and workshops. He
chanical engineering degree from the University of Houston. holds a master’s degree in chemical engineering.

December 2015 SPE Drilling & Completion 315

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