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COMPO

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x ME FEATURE
From Materials Evaluation, Vol. 68, No. 8, pp: 880–886.
Copyright © 2010 The American Society for Nondestructive Testing, Inc.

SITES
Compression After Impact
Load Prediction in Graphite
Epoxy Laminates
by Anthony M. Gunasekera

A
s technology evolves, extensive resources are being utilized in the
research and development of new composites to replace metals in
various structures in many industries. Composites have the advan-
tages of better corrosion resistance, better fatigue properties and
higher strength, as well as a higher stiffness-to-weight ratio than most metals.
However, with increasing advantages there are also disadvantages. The
sudden failure of composite structures is one disadvantage that has been crit-
ically analyzed and has become a vastly intricate area of research, as there
are many varying factors that play major roles.
If laminates are to be used as thin outer surfaces or as the skin of an
aircraft, these composites will be subjected to environmental conditions and
other occurrences during flight that can alter their properties. Low energy
impact damage (8 – 20 J), such as small bird strikes, hail, dropping of tools
on a wing section, or runway stones and debris, can cause different modes of
failure, including internal or surface delaminations and matrix cracking within
the composite. Although this damage may be barely visible from the exterior
of the structure, it can cause an extensive reduction in the compressive
performance or residual strength. This type of impact damage is referred to as
barely visible impact damage (BVID), which further weakens materials that are
already much weaker in compression than in tension. In general, composites
are brittle and provide little to no warning before failing. BVID causes compos-
ites to fail or buckle under much lower compressive loadings than usual.
Therefore, implementation of a reliable technique to determine the compres-
sive residual strength of a composite under compression would greatly reduce
the risk of sudden failure in a composite structure while in service (Dion,
2006; Hill et al., 2008; Karl, 2006; Nguyen, 2005; Walker and Hill, 1997).
Identification and monitoring of these structural changes on an aircraft during

AUGUST 2010 • MATERIALS EVALUATION 881


ME FEATURE w
x compression in laminates

A few hits of higher amplitude were visible,


but they were relatively sparse and suspected
to be occurrences of microdelaminations
in-flight conditions is crucial, as it allows designers to Secondly, two backpropagation neural networks
know the limitations of their products. (BPNNs), which weigh the amplitude distributions
Acoustic emission testing (AE) has been success- from AE data to arrive at accurate compressive
fully proven on a broad scale in distinguishing and strength predictions, were constructed and optimized.
classifying failure mechanisms based on the acoustic The first BPNN analyzed data had not been filtered for
signatures of most fiber-matrix composites (ASNT, noise, and were not classified into mechanisms using
2005; Dion, 2006; Hill et al., 2008; Nguyen, 2005). a SOM. The second BPNN analyzed data that the SOM
Although it is challenging to accurately distinguish classified into distinct failure mechanisms and were
between coupled failure modes, failure mechanisms used to eliminate noise. This way, comparisons could
can be distinguished by the acoustic signature emitted be made as to the effectiveness of SOMs in data clas-
during composite failure. Failure mechanisms tend to sification for prediction purposes.
emit sounds in a unique and consistent manner. While A worst case error of 5 to 15% between the
the ultimate failure loads between two different cases predicted load and the actual test coupon failure load
may differ entirely, the acoustic characteristics was desired for this analysis. If these neural networks
maintain similar failure mechanism trends. These could be successfully trained using AE test data, it
trends can be exploited by artificial neural networks could then be possible to use this same technique
(ANNs), computer algorithms that can easily handle during in-flight conditions. AE transducers could be
complex multivariate data sets. ANNs have been mounted on the skin, panels or other structures and
shown to accurately classify failure mechanisms based used to listen and collect discontinuity growth data.
on data trends and to make predictions for compos- These data could then be fed into previously trained
ites after impact residual compressive strength (Dion, neural networks that were trained on test samples and
2006; Hill et al., 2008; Nguyen, 2005). accurately predict the failure modes and final residual
Two investigations regarding ANNs were conducted compression load of the structure. This procedure
by fabricating and impacting graphite/epoxy coupons could be done continuously in-flight and on the
at various energy levels, simulating low velocity impact ground, saving companies money as it would reduce
damage. The plates were then placed in a material maintenance inspections and unnecessary changes in
compression testing machine to test the compressive parts before the actual failure life was reached.
qualities of the specimens. AE transducers were used
to listen and collect discontinuity growth activity data Material and Testing Techniques
from the coupons under compression. Additionally, A graphite bidirectional woven prepreg cloth was used
ambient noise from the testing environment was to fabricate thirty-four 101.6  152.4 mm (4  6 in.)
recorded to properly filter it out of the data set. laminate coupons. The prepreg had a manufacturing
First, a Kohonen self-organizing map (SOM) was discontinuity due to misaligned fibers that were
constructed and optimized to separate the AE data present in the weave. It was thought that this could
into the various failure mechanisms experienced by prove to be a problem, as fibers misaligned in the axis
composite laminates undergoing compression. It was of compression could buckle prematurely, increasing
hoped that by quantifying the failure mechanisms, the variability in the compressive strength of the
more accurate ultimate strength predictions could be coupon. However, since all of the coupons were manu-
made. A Kohonen self-organizing map is an unsuper- factured in the same way with the same discontinuity,
vised, competitive, two-layered artificial neural it became less of a concern. The thickness of prepreg
network (ANN), which is incredibly useful for data clas- tape suggested that a 24 ply lay-up be used to
sification applications. This mapping system is based construct the coupon laminates.
on the human brain, which uses special organization
to classify certain objects or organisms into separate Impact Testing and Imaging
groups. BVID was created using a calibrated impactor. The

882 MATERIALS EVALUATION • AUGUST 2010


impactor was configured with a blunt 12.7 mm (0.5
in.) hemispherical tup. The tup simulated a low 101.6 mm
velocity impact such as a tool dropping on the (4 in.)
coupon. The impactor was set to impact at energies Compression fixture 50.8 mm
(2 in.)
ranging between 8 and 20 J. An ultrasonic C-scan and 150 kHz Resonant AE
X-ray image were also performed to analyze the effects transducer

of the impact damage on the coupon.


38.1 mm
Compression Testing and Acoustic Emission (1.5 in.)

A material compression testing machine was used to


Graphite/epoxy test coupons
compress the specimens. Compression after impact
152.4 mm
testing (CAI) is an ASTM standard test that is used to (6 in.)
test the compressive strength of aerospace materials Impact damage

after they have been impacted with low or high energy


impacts. The CAI test fixture was used to secure the 38.1 mm
coupons for compression (Figure 1). After securing the (1.5 in.)

coupon in the compression after impact fixture, the


specimen was placed in the compression machine
and the coupons were compressed at a constant rate
of 296.548 N/s (66.667 lbf/s). Upon failure, the
applied force dropped from the maximum load to zero
and the machine was stopped. Acoustic emission data Figure 1. Compression test setup.
were recorded during the compression test using an
acoustic emission analyzer. This handheld device
employs two 150 kHz transducers to collect acoustic
emission data. The transducers were hot-melt glued being hot-melt glued to the laminates, but with no
(used in the industry to mount transducers) to the compressive loads applied and the compression
specimens on the centerline from the top and bottom machine crosshead stationary. The compression
edges of the coupon. The transducers were also taped machine was turned on and recordings were
to the compression fixture to avoid damage in case conducted for approximately the same duration as a
buckling failure caused them to violently separate from typical compression test, ranging from 180 to 300 s.
the coupon. The acoustic emission analyzer also Once this noise signature was separately analyzed, it
allowed for a parametric input of the load from the was clearly seen in acoustic emission data taken from
compression machine so the final compressive load a specimen test. Figure 2 shows this low amplitude
could be obtained. This was also used to visualize the noise with specimen data in a hits versus amplitude
compressive life of the coupon and analyze how load graph.
changes with failure mechanisms.

Data Filtering and Noise Analysis


A software code was created to eliminate erroneous 300
data points and filter the data efficiently. Hits that Low amplitude noise (30 – 36 dB)
250
recorded values of zero (extremely weak hits) for
energy, duration or rise time were all removed first. 200
Long duration hits greater than 9800 µs were also Specimen amplitude distribution
Hits

150
removed (these being thought to be rubbing noise band (34 – 100 dB)
from the sides of the compression fixture). 100
Additionally, due to the wide variety of random noise 50
signals that occur during the progression of any type
of testing, a proper noise analysis was important. In 0
30 40 50 60 70 80 90 100
order to truly understand the acoustic signature of
ambient noise and thus remove it, five recordings of Amplitude (dB)
the quiescent testing environment were taken. All of
these recordings were captured using the pocket Figure 2. Hits versus amplitude plot showing the difference between noise and
acoustic emission transducer, with the transducers specimen data.

AUGUST 2010 • MATERIALS EVALUATION 883


ME FEATURE w
x compression in laminates

Figure 3. Laminate with 15 J BVID, displayed using C-scan and X-ray imaging.

Results and Discussion how the coupons were affected by the varying impact
energies. It can clearly be seen that as impact energy
Effects of Impact Testing increases, the residual CAI failure load of the
Figure 3 shows a laminate coupon that was impacted laminates is affected in a parabolic fashion. A signifi-
at 15 J. To the naked eye, it is difficult to see any cant amount of variability is observable, but this is to
damage. However, when an ultrasonic C-scan and X- be expected, given the nature of composite materials
ray image are taken of the same coupon, the damage and the manner of fabrication. The parabolic nature of
is visible. Longitudinal and transverse cracking is the compressive failure load was expected, because
clearly seen at the site of impact along the weave of as impact energy increases, the type of impact
the composite. damage changes from barely visible to a high velocity
impact that penetrates the surface. This penetration
Effects of the Compression and Noise Analysis creates a circular indentation that is thought to inhibit
Once testing was completed and all of the failure slip between plies. This effect would then increase,
loads were acquired, Figure 4 was plotted to visualize rather than decrease, the compressive strength. The
latter line is the tolerance interval, the B-basis
allowable for the composite coupons.
30 000
The first graph obtained from acoustic emission
28 000
Standard data data to be discussed will be amplitude versus time, as
Compressive failure load (lbf)

26 000 Best fit parabola shown in Figure 5 for Coupon 23A. The time scale is
24 000
B-basis allowables from the start of the test all the way to failure. Note
22 000
that in the first half of the test, the vast majority of the
hits occur in a range thought to be consistent with
20 000
matrix cracking. A few hits of higher amplitude were
18 000
visible, but they were relatively sparse and suspected
16 000 to be occurrences of microdelaminations. Matrix
14 000
cracking, as this range is assumed to be, occurs evenly
across the time scale. At the beginning of the second
12 000
half of the test, hits in the range consistent with
10 000
8 9 10 11 12 13 14 15 16 17 18 19 20
delaminations become more frequent. Additionally,
Impact energy (J) hits in the range consistent with fiber breaks also
begin to occur, becoming more prevalent as the test
proceeded to failure.
Figure 4. Failure load versus impact energy plot showing parabolic relationship.

884 MATERIALS EVALUATION • AUGUST 2010


Failure Mechanism Classification through Kohonen
Self-Organizing Maps
100
Macro delaminations
After considerable trial and error, it was determined micro/macro fiber breaks (70 – 100 dB)
that the SOM would best classify the various failure 90
Micro delaminations (55 – 72 dB)
mechanism signals using the amplitude and average 80

Amplitude (dB)
frequency parameters. Alternative analyses were
70
conducted using amplitude, energy and duration, but
the best results were produced using the former 60
combination. Using amplitude, average frequency,
50
energy and other separate parameters during testing
resulted in the same type of plots acquired from the 40
Matrix cracking (34 – 62 dB)
network tested on very few parameters. Values from
30
each of the 34 samples were then used to make indi- Start of test failure
vidual testing files, which revealed slightly varying Time (µs)
outputs for each coupon. As for the number of
Kohonen layer processing elements, training iterations
were performed with as few as two and as many as Figure 5. Amplitude versus time graph showing when certain mechanisms are
experienced.
twenty processing elements. The number of processing
elements approximate how many groups or clusters
the data will be divided. Graphs were created for every
300
variation of processing elements in the network. Noise
The number of Kohonen layer processing elements Matrix cracking Mech1
250
will equal (2n + 1)  (the number of choices [or Mech 2
Mech 3–4
clusters of data the network is given for classification]). 200
This SOM was configured to assign X and Y coordi-
Hits

nates to input vectors with similar amplitudes and 150


average frequencies. The number of Kohonen
processing elements determined the number of 100
distinct amplitude and average frequency ranges to Micro delaminations
which an input vector could be classified. In a complex 50 Macro delaminations
Low amplitude micro/macro fiber breaks
classification problem such as composite failure mech- noise
0
anisms, a SOM by itself cannot determine the ideal 30 40 50 60 70 80 90 100
failure mechanism distributions; rather, it provides
Amplitude (dB)
ranges of similar data, which must be interpreted to
determine plausible mechanism distributions.
For this research, the best results were obtained Figure 6. Amplitude histogram of data classified by a SOM.
using 14 Kohonen layer processing elements (or data
ranges), then combining the output into four distinct
groups: low amplitude noise, matrix cracking, microde-
100
laminations, and a combination of macrodelamina-
Macro delaminations
tions and fiber breaks. These results are shown in a 90
micro/macro fiber breaks
hits versus amplitude and an amplitude versus
80
average frequency graph for the coupon tested in
Amplitude (dB)

Figures 6 and 7. All this was after an iterative process 70


Micro delaminations Noise
in which the 14 separate ranges were combined into
60 Mech 1
four plausible failure mechanisms. Specifically, the Mech 2
humps thought to be external noise, microdelamina- 50 Mech 3–4
tions, and the combination of macrodelaminations
and fiber breaks were left unchanged – they are 40
Matrix cracking
possibly unique ranges that were output by the SOM. 30
The other 11 ranges of data were combined to 0 50 100 150 200
Low amplitude noise
produce the dominant hump denoted as matrix Average frequency (kHz)
cracking. This suggests that within the mechanism of
matrix cracking, there may be 11 different modes of Figure 7. Amplitude versus average frequency graph of data classified by a SOM.

AUGUST 2010 • MATERIALS EVALUATION 885


ME FEATURE w
x compression in laminates

cracking or possibly 11 different specimen reso- the sole output processing element was the predicted
nances, each emitting slightly differing acoustic signa- failure load. After the optimization process was
tures. It could also be possible that, as the processing completed for each configuration, the lowest
elements were increased, the SOM itself found unique maximum prediction error was found to be 15.89% for
characteristics in the data of low amplitude noise, the unclassified data. On the other hand, for the clas-
microdelaminations, and the combination of macrode- sified data with the noise removed, the lowest
laminations and fiber breaks, and could only further maximum error was reduced to –11.65%. After
divide the data considered to be matrix cracking into approximately 65 more iterations attempting to
clusters. optimize the minor parameters for the second configu-
ration, the maximum error was ultimately reduced to
After-Impact Load Prediction Using Backpropagation –11.53%.
Neural Networks
In order to predict the CAI failure load in the coupons, Conclusion
BPNNs were constructed and optimized using the In conclusion, using AE and ANNs to classify failure
same software as for the SOM. In the training phase, mechanisms and predict compressive failure loads for
the networks were trained by normalizing 24 of the this research proved highly successful. The combina-
coupons’ amplitude distributions (containing data up tion of these techniques could be used on aircraft to
to 50% of the failure load) as the inputs. The known predict the failure loads associated with impact
failure load for each of these coupons was also damaged parts without knowing a priori the level of
entered into the network. The network then updated impact damage. Moreover, these predictions could be
the weights between the processing elements until the made in-service using AE. w x
output failure load came within a certain percent error
of the actual failure load, at which point the ANN was AUTHOR
considered to be trained. Aerospace Engineering Department, Embry-Riddle Aeronau-
tical University, 600 South Clyde Morris Road, Daytona
In the testing phase, the networks were tested Beach, FL 32114.
using the amplitude histograms from the other ten
samples, with the corresponding failure loads being ACKNOWLEDGEMENTS
predicted. Two general BPNN architectures were used, The author would like to thank Michael W. Langdon, William
and various network parameters were optimized for D. Rice and Eric v.K. Hill for their assistance in the research,
writing and editing of this paper.
each configuration until the most accurate predictions
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