I. WASTEWATER TREATMENT
Primary Treatment of Wastewater 3
Design of Neutralization Contact Basin 11
Design of a Clarifier 15
Design of Upflow Anaerobic Sludge Blanket Reactor 1 27
Design of Upflow Anaerobic Sludge Blanket Reactor 2 37
Design of Trickling Filter 51
Design of Aerated Lagoon 60
II. PIPING SYSTEM
Introduction 70
Codes and Standards 73
Components of a Piping System 74
Factors to be Considered 92
Principles in Piping Design 94
Sample Piping Design 109
III. Instrumentation and Control
Introduction 118
Definitions 119
Types of Controllers 120
Types of Sensors 122
Types of Actuators 126
Sample Design 127
Specific
INTRODUCTION
NEUTRALIZATION
This step is conducted before the main step of wastewater treatment, that is
clarification, to fulfill the overall wastewater treatment objectives.
For Esolite Chemicals Inc., the huge amount of wastewater is generated by the
washing processes in the Nutsche Filters. The manufacturing plant produces 8998.08
kg of wastewater per batch. This wastewater is treated in order to meet the required
effluent characteristic for the discharge in the nearest body of water in Brgy. Bancal,
Carmona, Cavite.
The production of tylose powder from abaca stripping wastes involves chemical
processes which lead to generation of large amount of wastewater. An approximate
amount of 17,996.16 kg of wastewater per day is being generated by the
manufacturing plant due to the washing in the nutsche filters. Its disposal is a major
problem because of its odor, large amount, and harmful contaminants that might
affect the whole plant and the environment.
General Objective:
The main objective is to treat the wastewater generated from the production of
tylose powder from abaca stripping wastes with the following influent characteristics
shown in Table 9.1
Specific Objectives:
1. Collection of Wastewater
The main source of wastewater is the filtrates produced in the nutsche filters.
For every batch, the wastewater produced is 8998.08 kg. The production has two
batches per day, thereby doubling the amount of wastewater. The wastewater
generated will be collected for 6 days before treatment in a flow equalization basin.
Thus, the total amount of influent to be treated is 107,976.96 kg.
2. Neutralization
3. Clarifying
A rectangular concrete clarifier is used to settle the solids from the 111,109.20
kg neutralized wastewater coming from the neutralization contact basin. The influent
contains 931 mg/L of TSS and 1699 mg/L of BOD. The clarifier has an efficiency of
The effluent coming from the clarifier is pumped (5 hp) to the upflow anaerobic
sludge blanket reactor 1. The COD content of the incoming influent is 7692.0016 kg.
Two UASB reactors are used to treat the wastewater using acetic acid-forming bacteria
(acetogens) and methane-forming archaea (methanogens). These microorganisms are
loaded after the UASB reactor is completely filled up. UASB reactors remove 95% of
the COD. Methane is produced due to the anaerobic process treatment. The total
methane produced by the two UASB reactors per month is 18.63 kg. Each reactor has
a residence time of 4 hours. The amount of effluent from the UASB reactor 2 is
103,328.27 kg. The amount of COD still present in the effluent is 17.96 kg.
The effluent from the trickling filter is transferred to the aerated lagoon. The
aerated lagoon is used to reduce the organic matter content of wastewater through
aerated activity of microorganisms which convert it to cell tissues or gases. The TSS,
7. Discharge of Effluent
The discharged effluent amounting to 103,200.92 kg now has 7.0 pH, 17.84
mg/L of BOD, 55.86 mg/L of TSS, and 44.18 mg/L of COD. These properties conform
to the effluent standard of Class C type body of water based from DENR-DAO No. 2016-
08. The final effluent with 4.3m3/h flowrate is discharged to Pasong Pari River. The
total sludge collected from clarifier, UASB reactors 1 and 2, trickling filter, and aerobic
lagoon has a total amount of 7908.28 kg. This will be collected and disposed via third
party treater.
Shown in Table 9.3 is the removal efficiencies for BOD, COD, and TSS of
neutralization contact basin, clarifier, upflow anaerobic sludge blanket reactor,
trickling filter, and aerated lagoon. The equivalent levels of BOD, TSS, and COD of the
influent and effluent is also shown.
DESIGN DESCRIPTION
A back and forth long channel contact basin is selected due to easy installation
and lower cost, and provides good contact between the wastewater to be treated and
the chemical added.
DESIGN CONSIDERATIONS
DESIGN REQUIREMENTS
DESIGN CALCULATION
1. HCl Dosing
Chemical Reaction for neutralizing the basic wastewater
107976.96 𝑘𝑔
𝑉𝑜𝑙𝑢𝑚𝑒 𝑜𝑓 𝑊𝑊 𝑤𝑖𝑡ℎ 𝑁𝑎𝑂𝐻 = = 101.9555 𝑚3
𝑘𝑔
1059.06 3
𝑚
354.64 𝑘𝑔 + 315.77 𝑘𝑔
𝑚𝑜𝑙𝑒𝑠 𝑠𝑜𝑙𝑢𝑡𝑒 40 𝑘𝑔/𝑚𝑜𝑙𝑒
𝑀𝑜𝑙𝑎𝑟𝑖𝑡𝑦 𝑜𝑓 𝑁𝑎𝑂𝐻 𝑖𝑛 𝑊𝑊 = =
𝐿 𝑠𝑜𝑙𝑢𝑡𝑖𝑜𝑛 1000 𝐿
(101.9555𝑚3 )( )
1 𝑚3
= 0.0002 𝑀
35.2 𝑘𝑔
𝑚𝑜𝑙𝑒𝑠 𝑠𝑜𝑙𝑢𝑡𝑒 36.46 𝑘𝑔/𝑚𝑜𝑙𝑒
𝑀𝑜𝑙𝑎𝑟𝑖𝑡𝑦 𝑜𝑓 𝐻𝐶𝑙 = = = 0.0097 𝑀
𝐿 𝑠𝑜𝑙𝑢𝑡𝑖𝑜𝑛 100 𝑘𝑔 𝐻20 1000 𝐿
( )( )
𝑘𝑔 1 𝑚3
1000 3
𝑚
1000 𝐿 𝑚𝑜𝑙𝑒𝑠
101.9555𝑚3 ( 3
) 𝑥 0.0002 = 20.3911 𝑚𝑜𝑙𝑒𝑠 𝑁𝑎𝑂𝐻
1𝑚 𝐿
2. Basin Volume
𝑉 = 𝑣𝑜𝑙𝑢𝑚𝑒 𝑜𝑓 𝑤𝑎𝑠𝑡𝑒𝑤𝑎𝑡𝑒𝑟 + 𝑣𝑜𝑙𝑢𝑚𝑒 𝑜𝑓 𝐻𝐶𝑙 𝑎𝑑𝑑𝑒𝑑
𝑉 = 101.9555 𝑚3 + 2.1022 𝑚3 = 104.0577 𝑚3
Applying 20% safety factor:
𝑉 = 104.0577 𝑥 1.20 = 124.8692 𝑚3
𝑼𝒔𝒆 𝟏𝟐𝟓. 𝟎𝟎 𝒎𝟑
3. Surface Area
𝑉 124.8692 𝑚3
𝐴= = = 24.0318 𝑚2
𝐷 4.33 𝑚 𝑥 1.20
𝑼𝒔𝒆 𝟐𝟓. 𝟎𝟎 𝒎𝟐
4. Total Width and Length
𝐴 = 𝐿 𝑥 𝑊 = 20𝑊 𝑥 𝑊 = 21𝑊 2
24.0318𝑚2 = 21𝑊 2
𝑾 = 𝟏. 𝟎𝟔𝟗𝟖 𝒎 = 𝟏. 𝟏𝟎 𝒎
𝑳 = 𝟐𝟏. 𝟑𝟗𝟓𝟏 𝒎 = 𝟐𝟏. 𝟒𝟎 𝒎
5. Channel Width
𝑊𝑇 1.10 𝑚
𝑊𝐶 = = = 0.275 𝑚
4 4
𝑼𝒔𝒆 𝑾𝑪 = 𝟎. 𝟐𝟖 𝒎
𝑼𝒔𝒆 𝑳𝑪 = 𝑳 = 𝟐𝟏. 𝟒𝟎 𝒎
6. Baffle Length
Since Baffle Width is assumed to be 80% of the total basin length,
21.40 𝑚 𝑥 0.80 = 17.12 𝑚
𝑼𝒔𝒆 𝟏𝟕. 𝟐𝟎 𝒎
DESIGN SPECIFICATIONS
NEUTRALIZATION CONTACT BASIN
OPERATING DATA
Number of Units 1
Feed Wastewater from Flow Equalization Tank
Function To neutralize the wastewater to a pH of 7
Material of
Reinforced Concrete
Construction
TECHNICAL DATA
Parameter Proposed
Volume 125 m3
Surface Area 25 m2
Depth 5.20 m
Total Width 1.10 m
Total Length 21.40 m
Channel Width 0.28 m
Channel Length 21.40 m
Baffle Length 17.20 m
SUPPLIER INFORMATION
Company Name Bauer International (Phils) Inc
2nd Floor Regalia Park Tower, 150 P. Tuazon St., Cor.
Company Address
EDSA, Cubao, Quezon City
Phone Number +632 912 4503
Contact Details
Email Address Bauer.international@yahoo.com
DESIGN CONFIGURATION
DESIGN CONFIGURATION OF NEUTRALIZATION CONTACT BASIN
CLARIFIER
Factors to be considered in Designing a Clarifier
1. Detention time
2. Surface loading rates
3. Scour velocity
1. Given the influent data (mass and density), solve for the influent volumetric
flow rate of the wastewater. This will be used in the calculation of the volume
requirements for the clarifier.
2. Calculate the capacity of the clarifier using the influent volumetric flowrate.
Apply the safety factor. This shall be used in the calculation of the
dimensions.
3. Calculate the dimensions of the clarifier using the computed capacity.
4. Solve for the detention time using the volume of the wastewater and the
capacity of the clarifier.
5. Compute the removed and retained total suspended solids.
6. Compute the removed and retained BOD.
7. Calculate the total volume of effluent.
Clarifier Design
DESIGN PROBLEM
DESIGN DESCRIPTION
DESIGN SELECTION
A rectangular clarifier will be used for the design. Rectangular shaped is chosen
over circular because rectangular clarifiers can be built shallower but can achieve the
same effluent quality and subsequently result in cost savings. Also, flow is usually more
even and often requires less head loss in rectangular clarifiers. The even flow
distribution configuration for rectangular clarifiers requires simpler and less expensive
pipe work layout and pumping requirement as compared to circular clarifiers where
the pipes require a more complicated layout pattern and perhaps a separate pumping
station, as well.
FUNCTION
1 Inlet The entry point of the wastewater to the clarifier
2 Sludge Trough The scraped sludge goes here before exiting the clarifier
3 Drive Unit Moves the flight and chain system
DESIGN ASSUMPTIONS
DESIGN CONSIDERATIONS
2. The safety factor is 20% (Perry, R.H. and Green, D.W. Perry’s Chemical
Engineering Handbook 7th edition)
5. The typical design value of detention time is 2.00 - 3.00 hours (Clarifier
Calculations by Michigan Department of Environmental Quality Operator
Training and Certification Unit).
6. The typical design value of surface overflow rate is 400-800 gal/d/ft2 (Clarifier
Calculations by Michigan Department of Environmental Quality Operator
Training and Certification Unit). The assumed surface overflow rate is 600
gal/d/ft2 (24.54 m3/d/m2).
7. The typical efficiency of clarifiers for BOD and TSS are 30% and 70%,
respectively (Handbook of Water and Wastewater Treatment Plant Operations,
Frank R. Spellman)
DESIGN REQUIREMENTS
1. Volume of Wastewater
2. Clarifier Dimensions
3. Detention Time
4. Suspended Solids
5. BOD
DESIGN CALCULATIONS
1. Volume of Wastewater
V = 87.1595 m3/day
2. Clarifier Dimensions
𝑣𝑜𝑙𝑢𝑚𝑒 𝑜𝑓 𝑤𝑎𝑠𝑡𝑒𝑤𝑎𝑡𝑒𝑟
𝐴𝑟𝑒𝑎 =
𝑜𝑣𝑒𝑟𝑓𝑙𝑜𝑤 𝑟𝑎𝑡𝑒
104.5914 𝑚3
𝐴𝑟𝑒𝑎 = = 4.2621𝑚2
24.54 𝑚3 /𝑚2
4.2621 𝑚2 = 4𝑊 2
W = 1.0322 m
H=3m
3. Detention Time
Use 4 hours
4. Suspended Solids
The typical efficiency of clarifiers for TSS is 70% according to the Handbook of Water
and Wastewater Treatment Plant Operations, Frank R. Spellman, page 565
Based from the test results of Mach Union Water Lab., the TSS of the wastewater
sample is,
5. BOD
The typical efficiency of clarifiers for BOD is 30% according to the Handbook of Water
and Wastewater Treatment Plant Operations, Frank R. Spellman, page 565
𝑘𝑔𝑠𝑜𝑙𝑖𝑑
𝑆𝑜𝑙𝑖𝑑𝑠 𝑟𝑒𝑚𝑜𝑣𝑒𝑑 = 44.4252 𝑘𝑔𝐵𝑂𝐷 × 1.7 = 75.5228 𝑘𝑔
𝑘𝑔𝐵𝑂𝐷
Mass effluent = Mass influent – Mass TSS removed - Mass Solids removed
110,976.8753 𝑘𝑔
𝑉=
1274.78 𝑘𝑔/𝑚3
V = 87.0557 m3
DESIGN SPECIFICATIONS
CLARIFIER
OPERATING DATA
Number of Units 1
DESIGN CONFIGURATION
CLARIFIER
1. Upflow velocity
2. Sludge Production
3. Methane Production
4. Effluent Characteristics
1. Given the influent data (mass and density), solve for the influent volumetric flow
rate of the wastewater. This will be used in the calculation of the volume
requirements for the UASB reactor.
2. Calculate the capacity of the UASB reactor using the influent volumetric
flowrate. Apply the safety factor. This shall be used in the calculation of the
dimensions.
3. Calculate the dimensions of the UASB reactor using the computed capacity.
4. Calculate for the volume of the sludge recovered from the reactor.
5. Calculate the amount of methane gas produced in the reactor per day.
6. Compute the removed and retained COD.
7. Calculate the total volume of effluent.
DESIGN PROBLEM
DESIGN DESCRIPTION
DESIGN SELECTION
The UASB Reactor was selected to lower the COD of the wastewater. It was
chosen because of allows the use of high volumetric COD loadings compared to other
anaerobic process.
PARTS FUNCTION
Primary Clarifier Removal/entrapment of (non)biodegradable suspended
solids from the influent
Biological reactors Removal of biodegradable organic compounds by
converting them into methane. (main UASB reactor)
Secondary clarifier Clarifying the treated effluent in the settler zone at the top
part of the UASB reactor
Sludge digester Stabilisation (digestion) and improving the dewatering
characteristics of the retained influent primary sludge
DESIGN ASSUMPTIONS
DESIGN CONSIDERATIONS
1. Dimensions of the reactor or the Main UASB tank, shape of tank is rectangular
for large scale.
4. The maximum amount of methane that the UASB can produce can be estimated
by multiplying BOD by the maximum methane producing capacity of the
wastewater (B0). The default B0 value for wastewater is 0.6 kg CH4/kg BOD,
6. The slope of the settler bottom (1.e. the inclined wall of the gas collector) should
be between 45-60°
7. The surface area of the apertures between the gas collectors should be 15-20%
of the reactor surface area.
8. The height of the gas collector should be between 1.5-2m at reactor heights of
5-7m.
9. To facilitate the release and collection of gas bubbles and to combat scum layer
formation, a liquid-gas interface should be maintained in the gas collector.
10. To avoid up-flowing gas bubbles to enter the settle compartment, the overlap
of the baffles installed beneath the apertures should be 10-20cm.
11. Generally, scum layer baffles should be installed at the effluent weirs.
12. The diameter of the gas exhaust pipes should be sufficient to guarantee the
easy removal of the biogas from the gas collection cap, particularly in case
foaming.
13. In the upper part of the gas cap, anti-foam spray nozzles should be installed in
the case of the treatment of the waste water is accompanied by heavy foaming.
14. The removal efficiency for COD of UASB reactor is 95% (Metcalf & Eddy, 4th ed,
pg 1007).
15. The soluble COD accounts for over 80% of the total COD (Eremektar et. Al,
2005).
DESIGN REQUIREMENTS
1. Reactor Volume
4. Volume of Sludge
DESIGN CALCULATIONS
a. Reactor Volume
𝑉𝑟 = 𝐻𝑅𝑇 𝑥 𝑄
Where: Q = rate of sewage input to the reactor
HRT = hydraulic retention time
Vr = volume of main reactor
𝑚3
𝑉𝑟 = 4 ℎ𝑟𝑠 𝑥 3.6273
ℎ𝑟
𝑉𝑟 = 14.51 𝑚3
Applying 20% safety factor:
𝑉𝑟 = 14.51 𝑚3 𝑥 1.20 = 17.412 𝑚3
𝑼𝒔𝒆 𝟏𝟕. 𝟒𝟏 𝒎𝟑
b. Height of the Tank
𝐻 = 𝐻𝑠 + 𝐻𝑠𝑒
Where: H = height of the tank
Hs = height of sludge layer area (main reactor)
Use Hse = 5 m
𝐻 = 6𝑚 + 5𝑚 = 11𝑚
𝑼𝒔𝒆 𝑯 = 𝟏𝟏𝒎
c. Length and Width of the Tank
𝑊 = 0.8896 𝑚
𝑼𝒔𝒆 𝑾 = 𝟎. 𝟗𝟎 𝒎
𝐿 = 2 𝑥 0.90 𝑚
𝑼𝒔𝒆 𝑳 = 𝟏. 𝟖𝟎 𝒎
d. Volume of Sludge
From the dimension of the main reactor, the height of the sedimentation area or the
sludge layer height is 5m.
𝑉𝑠 = 𝐿 𝑥 𝑊 𝑥 𝐻𝑠𝑒
𝑉𝑠 = 1.80𝑚 𝑥 0.90𝑚 𝑥 5𝑚 = 8.1𝑚3
The amount of sludge that can be extracted from the tank is only 30-50 % of its volume,
use 30%.
𝑉𝑠 = 8.1𝑚3 𝑥 0.30 = 2.43 𝑚3
𝑼𝒔𝒆 𝑽𝒔 = 𝟐. 𝟒𝟑 𝒎𝟑
𝑚3 ℎ𝑟𝑠 𝑑𝑎𝑦𝑠
𝐹𝑙𝑜𝑤 = 3.6273 × 5%( 𝑐𝑜𝑛𝑣𝑒𝑟𝑡𝑒𝑑 𝑖𝑛𝑡𝑜 𝑏𝑖𝑜𝑚𝑎𝑠𝑠) × 24 × 30
ℎ𝑟 𝑑𝑎𝑦 𝑚𝑜𝑛𝑡ℎ
𝑚3
= 130.58
𝑚𝑜𝑛𝑡ℎ
𝑘𝑔 1 1𝑑𝑎𝑦
𝐵𝑂𝐷 = 103.6588 × × = 1.1907 𝑘𝑔/𝑚3
𝑑𝑎𝑦 𝑚3 24ℎ𝑟𝑠
3.6273
ℎ𝑟
𝑘𝑔𝐶𝐻4
𝐵0 = 0.6
𝑘𝑔𝐵𝑂𝐷
𝑀𝐶𝐹 = 10%
𝑚3 𝑘𝑔𝐶𝐻4
𝐶𝐻4 = 𝛴𝑚𝑜𝑛𝑡ℎ (130.58 × 1.1907 𝑘𝑔/𝑚3 × 0.6 × 0.10)
𝑚𝑜𝑛𝑡ℎ 𝑘𝑔𝐵𝑂𝐷
CH4 = 9.33 kg/month = 0.311 kg/day
Methane Gas collection system is no longer in our capacity to design but we may
compute for the volume of methane produced per month.
W=PxV
Where: W= weight of methane
P = density of methane (0.66kg/ m3)
V = volume of methane (m3/month)
𝑘𝑔 0.66𝑘𝑔
9.33 = 𝑥𝑉
𝑚𝑜𝑛𝑡ℎ 𝑚3
𝑚3
𝑉 = 14.1364
𝑚𝑜𝑛𝑡ℎ
𝒎𝟑
𝑼𝒔𝒆 𝑽 = 𝟏𝟒. 𝟏𝟒
𝒎𝒐𝒏𝒕𝒉
6.Mass of COD removed
Calculate the amount of COD retained
𝐶𝑂𝐷𝑒𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 𝐶𝑂𝐷𝑖𝑛𝑓𝑙𝑢𝑒𝑛𝑡 (1 − 𝑒𝑓𝑓𝑖𝑐𝑖𝑒𝑛𝑐𝑦)
𝑚𝑔
𝐶𝑂𝐷𝑒𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 88352 (1 − 0.95)
𝐿
𝒎𝒈
𝑪𝑶𝑫𝒆𝒇𝒇𝒍𝒖𝒆𝒏𝒕 = 𝟒𝟒𝟏𝟕. 𝟔
𝑳
UASB 1
OPERATING DATA
Number of Units 1
DESIGN CONFIGURATION
UASB REACTOR 1
1. Upflow velocity
2. Sludge Production
3. Methane Production
4. Effluent Characteristics
1. Given the influent data (mass and density), solve for the influent volumetric
flow rate of the wastewater. This will be used in the calculation of the volume
requirements for the UASB reactor.
2. Calculate the capacity of the UASB reactor using the influent volumetric
flowrate. Apply the safety factor. This shall be used in the calculation of the
dimensions.
3. Calculate the dimensions of the UASB reactor using the computed capacity.
4. Calculate for the volume of the sludge recovered from the reactor.
5. Calculate the amount of methane gas produced in the reactor per day.
6. Compute the removed and retained COD.
7. Calculate the total volume of effluent.
DESIGN DESCRIPTION
DESIGN SELECTION
The UASB Reactor was selected to lower the COD of the wastewater. It was chosen
because of allows the use of high volumetric COD loadings compared to other
anaerobic process.
PARTS FUNCTION
Primary Clarifier Removal/entrapment of (non)biodegradable suspended
solids from the influent
Biological reactors Removal of biodegradable organic compounds by
converting them into methane. (main UASB reactor)
Secondary clarifier Clarifying the treated effluent in the settler zone at the top
part of the UASB reactor
DESIGN ASSUMPTIONS
DESIGN CONSIDERATIONS
4. The maximum amount of methane that the UASB can produce can be
estimated by multiplying BOD by the maximum methane producing capacity
of the wastewater (B0). The default B0 value for wastewater is 0.6 kg
CH4/kg BOD, as shown in the 2006 IPCC Guidelines for National
Greenhouse Gas Inventories, Volume 5, Chapter 6, Table 6.2.
6. The slope of the settler bottom (1.e. the inclined wall of the gas collector)
should be between 45-60°
7. The surface area of the apertures between the gas collectors should be 15-
20% of the reactor surface area.
8. The height of the gas collector should be between 1.5-2m at reactor heights
of 5-7m.
9. To facilitate the release and collection of gas bubbles and to combat scum
layer formation, a liquid-gas interface should be maintained in the gas
collector.
10. To avoid up-flowing gas bubbles to enter the settle compartment, the
overlap of the baffles installed beneath the apertures should be 10-20cm.
11. Generally, scum layer baffles should be installed at the effluent weirs.
12. The diameter of the gas exhaust pipes should be sufficient to guarantee the
easy removal of the biogas from the gas collection cap, particularly in case
foaming.
13. In the upper part of the gas cap, anti-foam spray nozzles should be installed
in the case of the treatment of the waste water is accompanied by heavy
foaming.
14. The removal efficiency for COD of UASB reactor is 95% (Metcalf & Eddy, 4th
ed, pg 1007).
15. The soluble COD accounts for over 80% of the total COD (Eremektar et. Al,
2005).
DESIGN REQUIREMENTS
1. Reactor Volume
4. Volume of Sludge
DESIGN CALCULATIONS
1. Reactor Volume
𝑉𝑟 = 𝐻𝑅𝑇 𝑥 𝑄
Where: Q = rate of sewage input to the reactor
HRT = hydraulic retention time
Vr = volume of main reactor
𝑚3
𝑉𝑟 = 4 ℎ𝑟𝑠 𝑥 3.3885
ℎ𝑟
𝑉𝑟 = 13.55 𝑚3
Applying 20% safety factor:
𝑉𝑟 = 13.55 𝑚3 𝑥 1.20 = 16.26 𝑚3
𝑼𝒔𝒆 𝟏𝟔. 𝟐𝟔 𝒎𝟑
2. Height of the Tank
𝐻 = 𝐻𝑠 + 𝐻𝑠𝑒
Where: H = height of the tank
Hs = height of sludge layer area (main reactor)
Hse = height of the sedimentation area (sludge layer height)
𝐻𝑠 = 𝑉𝑥𝐻𝑅𝑇
Since the soluble COD accounts for over 80% of the total COD (Eremektar et. Al,
2005), from table 3 use V (liquid upflow velocity) = 1.5 m / hr
Table 9.20 (Metcalf and Eddy, Table 10-14)
Upflow Velocity, m/hr Reactor Height, m
Wastewater type Range Typical Range Typical
1.5𝑚
𝐻𝑠 = 𝑥 4ℎ𝑟𝑠 = 6𝑚
ℎ𝑟
For Hse use the table below.
Table 9.21 (Velasquez, et. Al,2014)
COD input Sludge Layer Height
< 3000 mg / L 3–5m
> 3000 mg / L 5–7m
Use Hse = 5 m
𝐻 = 6𝑚 + 5𝑚 = 11𝑚
𝑼𝒔𝒆 𝑯 = 𝟏𝟏𝒎
3. Length and Width of the Tank
𝑉𝑠 = 𝐿 𝑥 𝑊 𝑥 𝐻𝑠𝑒
𝑉𝑠 = 1.72𝑚 𝑥 0.86𝑚 𝑥 5𝑚 = 7.40𝑚3
The amount of sludge that can be extracted from the tank is only 30-50 % of its
volume, use 30%.
𝑉𝑠 = 7.40 𝑚3 𝑥 0.30 = 2.22 𝑚3
𝑼𝒔𝒆 𝑽𝒔 = 𝟐. 𝟐𝟐 𝒎𝟑
5. Methane Gas Production
The equations proposed to calculate CH4 generation at wastewater treatment systems
are presented below:
𝐶𝐻4 = 𝛴𝑚𝑜𝑛𝑡ℎ (𝐹𝑙𝑜𝑤 𝑥 𝐵𝑂𝐷 𝑥 𝐵0 𝑥 𝑀𝐶𝐹)
Where:
CH4 = Monthly CH4 mass emissions from the UASB reactor (kg/month).
Flow = Monthly flow treated through UASB treatment system (m3/month).
BOD = Average monthly organics loading in wastewater entering UASB treatment
system (kg/m3).
B0 = Maximum CH4 producing potential of institutional wastewater (default value of
0.6 kg CH4/kg BOD).
MCF = CH4 conversion factor, indicating the extent to which the organic content
(measured as BOD) degrades anaerobically.
𝑚3 ℎ𝑟𝑠 𝑑𝑎𝑦𝑠
𝐹𝑙𝑜𝑤 = 3.3885 × 5%( 𝑐𝑜𝑛𝑣𝑒𝑟𝑡𝑒𝑑 𝑖𝑛𝑡𝑜 𝑏𝑖𝑜𝑚𝑎𝑠𝑠) × 24 × 30
ℎ𝑟 𝑑𝑎𝑦 𝑚𝑜𝑛𝑡ℎ
𝑚3
= 121.99
𝑚𝑜𝑛𝑡ℎ
𝑘𝑔 1 1𝑑𝑎𝑦
𝐵𝑂𝐷 = 103.6588 𝑥 𝑥 = 1.27 𝑘𝑔/𝑚3
𝑑𝑎𝑦 𝑚3 24ℎ𝑟𝑠
3.3885
ℎ𝑟
𝑘𝑔𝐶𝐻4
𝐵0 = 0.6
𝑘𝑔𝐵𝑂𝐷
𝑀𝐶𝐹 = 10%
𝑚3 𝑘𝑔𝐶𝐻4
𝐶𝐻4 = 𝛴𝑚𝑜𝑛𝑡ℎ (121.99 × 1.27 𝑘𝑔/𝑚3 × 0.6 × 0.10)
𝑚𝑜𝑛𝑡ℎ 𝑘𝑔𝐵𝑂𝐷
𝑘𝑔 0.66𝑘𝑔
9.30 = 𝑥𝑉
𝑚𝑜𝑛𝑡ℎ 𝑚3
𝑚3
𝑉 = 14.0909
𝑚𝑜𝑛𝑡ℎ
𝒎𝟑
𝑼𝒔𝒆 𝑽 = 𝟏𝟒. 𝟏𝟎
𝒎𝒐𝒏𝒕𝒉
6.Mass of COD removed
Calculate the amount of COD retained
𝐶𝑂𝐷𝑒𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 𝐶𝑂𝐷𝑖𝑛𝑓𝑙𝑢𝑒𝑛𝑡 (1 − 𝑒𝑓𝑓𝑖𝑐𝑖𝑒𝑛𝑐𝑦)
𝑚𝑔
𝐶𝑂𝐷𝑒𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 4417.6 (1 − 0.95)
𝐿
𝒎𝒈
𝑪𝑶𝑫𝒆𝒇𝒇𝒍𝒖𝒆𝒏𝒕 = 𝟐𝟐𝟎. 𝟖𝟖
𝑳
To calculate the amount of BOD removed:
𝑀𝐶𝑂𝐷 = 𝐶𝑂𝐷𝑖𝑛𝑓𝑙𝑢𝑒𝑛𝑡 − 𝐶𝑂𝐷𝑒𝑓𝑓𝑙𝑢𝑒𝑛𝑡
𝑚𝑔 𝑚𝑔 1𝑘𝑔 1000𝐿 81.32𝑚3
𝑀𝐶𝑂𝐷 = (4417.6 − 220.88 )( ) ( )( )
𝐿 𝐿 1𝑥106 𝑚𝑔 1𝑚3 𝑑𝑎𝑦
𝑴𝑪𝑶𝑫 = 𝟑𝟒𝟏. 𝟐𝟖 𝒌𝒈/𝒅𝒂𝒚
𝐸𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 𝑖𝑛𝑓𝑙𝑢𝑒𝑛𝑡 𝑚𝑎𝑠𝑠 𝑓𝑙𝑜𝑤 𝑟𝑎𝑡𝑒 − 𝑚𝑎𝑠𝑠 𝑜𝑓 𝐶𝑂𝐷 𝑟𝑒𝑚𝑜𝑣𝑒𝑑
Mass effluent = 103,669.55 kg – 341.28 kg
Effluent = 103,328.27 kg
DESIGN SPECIFICATIONS
UASB 2
OPERATING DATA
Number of Units 1
Mode of Operation Batch
Feed Wastewater from UASB 1
Function To reduce the COD of the wastewater
Material of Construction Reinforced Concrete
TECHNICAL DATA
Parameter Proposed Existing
Volume 16.26 m3 -
Height 11 m 5 – 20 m
Total Width 0.86 m 3 – 24 m
Total Length 1.72 m 15 – 90 m
Detention Time 4.00 h 4-9 h
EFFLUENT DATA
Mass 103,328.27 kg
BOD 1189.3 mg/L
TSS 279.3 mg/L
COD 220.88 mg/L
Methane Gas Produced 9.30 kg/month
Sludge Volume 2.22 m3
SUPPLIER INFORMATION
Company Name BONGAR ENVIROSYSTEMS TECHNOLOGIES, CORP.
310 Pilar Road, Almanza I
Company Address
Las Pinas City, Philippines, 1750
Phone Number (+632) 8013943
Contact Details
Email Address imbongar@yahoo.com
DESIGN CONFIGURATION
UASB REACTOR 2
Source: Table 1-5: Unit Operations and Processes Used to Remove Constituents
found in Wastewater, p. 13 (Wastewater Engineering: Treatment and Reuse, 4th Ed.
by Tchobanoglous, et. al., Metcalf & Eddy, Inc.)
TRICKLING FILTER
Factors to Consider in Designing a Trickling Filter
In the design of the trickling filter, consideration must be given to:
1. Hydraulic loading rate
2. BOD of influent feed
3. Depth of settling tank
4. Recirculation ratio
5. Needs for establishment of nitrifying bacteria
6. Types of filter bed to use
7. Ventilation system, either forced air or natural
Loading rate is one of the important aspects to consider before you come up
with your trickling filter design. In order to optimize on efficiency, there should be a
continuous growth of biomass to maintain a well-balanced system.
Selection of filter media for your trickle filters must consist of material with high
surface area to allow water to pass through freely without clogging. Typical packing
can either be rock, redwood, plastic vertical flow plate and each media have different
costs consideration and durability in mind.
Air flow is another fundamental aspect towards successful operation of the filter.
The driving force in an open system is draft plus natural wind. If the incoming
wastewater temperature is lower than ambient air, then air will flow towards
downward direction, which in terms of mass transfer factor, this is considered more
economical.
Step-by-Step Procedure in Designing a Trickling Filter
PARTS FUNCTION
This provides a surface for the biological slime layer to
Filter Media
attach and grow.
Provides even distribution of wastewater over the
Distributor Arms
media.
Distributor Support Provides support for the distribution system
Inlet Where the wastewater influent is introduced
Design Considerations
1. Rock media trickling filters is used for high rate trickling filters (Liu and Liptak.
1999. Environmental Engineer’s Handbook. 2nd Edition. Section 7.23).
1. The Hydraulic Loading for rock media trickling filters is 0.16 – 0.64 gal/ft2-min
(Liu and Liptak. 1999. Environmental Engineer’s Handbook. 2nd Edition.
Section 7.23).
2. The BOD Removal Efficiency of 90% is feasible on rock media trickling filter (Liu
and Liptak. 1999. Environmental Engineer’s Handbook. 2nd Edition. Section
7.23).
3. A depth of 8 ft is used (Liu and Liptak. 1999. Environmental Engineer’s
Handbook. 2nd Edition. Section 7.23).
4. For rock media trickling filters at high rate has a recirculation ratio, r of 1 (Liu
and Liptak. 1999. Environmental Engineer’s Handbook. 2nd Edition. Section
7.23).
5. The treatability constant, ko for a 12-m rock media trickling filter is 0.036/min
(Liu and Liptak. 1999. Environmental Engineer’s Handbook. 2nd Edition.
Section 7.23.3).
6. The n factor is 0.67 for rock media (Liu and Liptak. 1999. Environmental
Engineer’s Handbook. 2nd Edition. Figure 7.23.4).
7. A minimum clearance of 6 inches between the media and distributor arm is
required (Guyer, J.P. An Introduction to Trickling Filter Wastewater Treatment
Plants. p. 12).
8. The Spulkraft flushing intensity (SK) recommendations for rock filters were 2 to
6mm/pass of arm (Albertson, O.E. Slow Down That Trickling Filter!).
Design Requirements
1. Capacity
2. Treatability Constant
3. Surface Area
4. Hydraulic Loading Rate
5. Organic Loading Rate
6. Residence Time
7. Rotational Speed of Distributor Arms
8. Mass of BOD Removed
9. Mass and Volume of Effluent
10. Power Requirements
Design Calculation
1. Peak Flow Rate, Q
If there are no data for peak flow rates available, then (Guyer, J.P. An
Introduction to Trickling Filter Wastewater Treatment Plants):
Q = 3 x influent flow
Q = 3 x 81.06 m3/day
Q = 243.18 m3/day
Use: Q = 243.18 m3/day
2. Treatability Constant, k
To correct treatability constant for a certain depth (Liu and Liptak. 1999.
Environmental Engineer’s Handbook. 2nd Edition.):
𝐷 𝑛
𝑘 = 𝑘𝑜 ( )
𝐷𝑂
Where: k = treatability constant corresponding to filter depth D
ko = treatability constant corresponding to filter depth Do
0.036 8 0.67
𝑘= x( ) = 0.0274/𝑚𝑖𝑛
min 12 𝑚
Use: k = 0.0274/min
3. Surface Area
Using Veltz Equation (Liu and Liptak. 1999. Environmental Engineer’s
Handbook. 2nd Edition. Eqn. 7.23-1):
𝑛
𝑆𝑖 + 𝑟𝑆𝑒 −𝑘𝐷𝐴𝑛 (1.035𝑇−20 )
𝑆𝑒 = 𝑒 𝑄
1+𝑟
Where:
Se = effluent BOD from filter, mg/L =
Si = influent BOD from filter, mg/L =
r = ratio of recirculated flow to wastewater flow =1
D = filter depth, m = 8 ft = 2.4384 m
A = surface area, m2 =to be determined
Q = wastewater flow, m3/min = 243.18 m3/day = 0.1689 m3/min
T = wastewater temperature, oC = 30
k = treatability constant, min-1 = 0.0274/min
𝑚𝑔
118.93
𝐿
𝑚𝑔 𝑚𝑔
1189.3 𝐿 + 118.93 𝐿 −0.0274/ min x 2.4384 m x 𝐴0.67
(1.03530−20 )
= 𝑥𝑒 0.16890.67
1+1
A = 12.7159 m2
d = 4.02 m
Use: A = 13 m2; d = 4.1 m
4. Hydraulic Loading Rate
It is the flow of wastewater applied to the trickling filter per unit of surface area,
calculated by:
𝑄
𝐻𝐿𝑅 =
𝐴
m3
243.18
day
𝐻𝐿𝑅 = = 18.7062 𝑚3 /𝑑𝑎𝑦/𝑚2
13 𝑚2
Use: HLR =18.8 𝒎𝟑 /𝒅𝒂𝒚/𝒎𝟐
5. Organic Loading Rate
It is defined as the pounds of Biochemical Oxygen Demand applied to the trickling
filter per 1,000 ft3 of volume of media per day, calculated by:
𝑂𝐿𝑅, 𝑙𝑏 𝐵𝑂𝐷/𝑑𝑎𝑦/1000 𝑓𝑡 3
𝑚𝑔 𝑙𝑏
𝐵𝑂𝐷, 𝐿 𝑥 𝑓𝑙𝑜𝑤, 𝑚𝑔𝑑 𝑥 8.34 𝑥 1000 𝑓𝑡 3
𝑔𝑎𝑙𝑙𝑜𝑛
=
𝑀𝑒𝑑𝑖𝑎 𝑉𝑜𝑙𝑢𝑚𝑒, 𝑓𝑡 3
𝑂𝐿𝑅, 𝑙𝑏 𝐵𝑂𝐷/𝑑𝑎𝑦/1000 𝑓𝑡 3
𝑚𝑔 𝑙𝑏
1189.3 𝐿 𝑥 0.0214 𝑚𝑔𝑑 𝑥 8.34 𝑥 1000 𝑓𝑡 3
𝑔𝑎𝑙𝑙𝑜𝑛
=
1119.45 𝑓𝑡 3
𝑂𝐿𝑅, 𝑙𝑏 𝐵𝑂𝐷/𝑑𝑎𝑦/1000 𝑓𝑡 3 = 189.6123
Use: OLR = 189.7
6. Residence Time
To calculate for residence time (Liu and Liptak. 1999. Environmental
Engineer’s Handbook. 2nd Edition. SectionFigure 7.23.4):
𝐷, 𝑓𝑡
𝑡, 𝑚𝑖𝑛 = 0.5 𝑛
𝑄, 𝑔𝑝𝑚. 𝑓𝑡 2
8
𝑡, 𝑚𝑖𝑛 = 0.5 𝑥 = 8.6040 𝑚𝑖𝑛
0.31880.67
For an area of 139.9 ft2
Use: t = 20.1 hours
7. Rotational Speed of Distributor Arms
Using the equation for Spulkraft flushing intensity (SK) calculation:
𝐻𝐿𝑅, 𝑚3 / 𝑚2 /ℎ 𝑥1000𝑚𝑚/𝑚
𝑆𝐾, 𝑚𝑚/𝑝𝑎𝑠𝑠 =
𝑎 𝑥 𝑛, 𝑟𝑝𝑚 𝑥 60 𝑚𝑖𝑛/ℎ𝑟
Where: a = number of arms = 2
n = rotational speed
0.7833 𝑚3 / 𝑚2 /ℎ 𝑥1000𝑚𝑚/𝑚
6 𝑚𝑚/𝑝𝑎𝑠𝑠 =
2 𝑥 𝑛, 𝑟𝑝𝑚 𝑥 60 𝑚𝑖𝑛/ℎ𝑟
n= 1.1
Use: n= 1.1 rpm
8. Mass of BOD Removed
𝑀𝐵𝑂𝐷𝑟𝑒𝑚𝑜𝑣𝑒𝑑 = (𝑆𝑖 − 𝑆𝑒 )(𝑖𝑛𝑓𝑙𝑢𝑒𝑛𝑡 𝑣𝑜𝑙𝑢𝑚𝑒𝑡𝑟𝑖𝑐 𝑓𝑙𝑜𝑤𝑟𝑎𝑡𝑒)
𝑚𝑔 1000 𝐿 𝑘𝑔 103,328.27 𝑘𝑔
𝑀𝐵𝑂𝐷𝑟𝑒𝑚𝑜𝑣𝑒𝑑 = (1189.3 − 118.93) 𝑥 𝑥 𝑥 ( )
𝐿 𝑚 3 6
10 𝑚𝑔 𝑘𝑔
1274.78 3
𝑚
= 86.7597 𝑘𝑔
𝑴𝑩𝑶𝑫𝒓𝒆𝒎𝒐𝒗𝒆𝒅 = 𝟖𝟔. 𝟕𝟔 𝒌𝒈
9. Mass and Volume of Effluent
𝑀𝑒𝑓𝑓 = 𝑖𝑛𝑓𝑙𝑢𝑒𝑛𝑡 𝑚𝑎𝑠𝑠 𝑓𝑙𝑜𝑤𝑟𝑎𝑡𝑒 − 𝑚𝑎𝑠𝑠 𝑜𝑓 𝐵𝑂𝐷𝑟𝑒𝑚𝑜𝑣𝑒𝑑
𝑒𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 103,328.27 𝑘𝑔 – 86.76 𝑘𝑔 = 103,241.51 𝑘𝑔
𝑬𝒇𝒇𝒍𝒖𝒆𝒏𝒕 = 𝟏𝟎𝟑, 𝟐𝟒𝟏. 𝟓𝟏 𝒌𝒈
𝑼𝒔𝒆: 𝑽𝒆𝒇𝒇 = 𝟖𝟏. 𝟎 𝒎𝟑
10. Power Requirement
For high rate rock media trickling filters, 6 kW/103 m3 is consumed, thus:
6 kW
𝑃 = 𝟐𝟒𝟑. 𝟏𝟖 𝐦𝟑 𝑤𝑎𝑠𝑡𝑒𝑤𝑎𝑡𝑒𝑟 𝑥 = 1.4591 𝑘𝑊 = 1.9566 ℎ𝑃
1000 𝑚3
Use: P = 2 hP
Design Specifications
TRICKLING FILTER
OPERATING DATA
Number of Units 1
Mode of Operation Batch
Feed Effluent from UASB
Function To reduce BOD from 1189.3 mg/L to 118.93 mg/L
Material of Construction Reinforced Concrete
TECHNICAL DATA
Parameter Proposed Existing
Surface Area 13 m3 Minimum 0.10 m2
Hydraulic Loading 18.8 m3/day/m2 Minimum 0.5 m3/day/m2
189.7 lb BOD/day/1000
Organic Loading -
ft3
Rotational Speed of
1.1 rpm -
Distributor Arm
Number of Distributor
2 2-4
Arm
Residence Time 20.1 hours 3hrs - 1 day
Power Requirement 2 hP -
EFFLUENT DATA
Mass 103,241.51 kg
BOD 118.93 mg/L
TSS 279.3 mg/L
COD 220.88 mg/L
SUPPLIER INFORMATION
Company Name Brentwood Industries Inc.
Company Address Myron L Company, Philippines (Distributor)
Cost Php 601,842.21
Expected Useful Life 30 years
AERATED LAGOON
Factors to Consider in Designing an Activated Sludge Process
In the design of the activated sludge process, consideration must be given to:
1. Selection of the reactor type
2. Applicable kinetic relationships
3. Solids retention time and loading criteria to be used
4. Sludge production
5. Oxygen requirements and transfer
6. Nutrient requirements
7. Other chemical requirements
8. Settling characteristics of bio-solids
9. Use of selectors
10. Effluent characteristics
7. Solve for the volumetric flowrate of the effluent. This shall be used in the
computation of the oxygen requirement.
8. Compute for the oxygen requirement and the needed kg of air per day. This will
be used for the power requirement calculation.
9. Calculate the power requirement.
1 – Inlet Pipe
2 – Baffle Wall
3 – Water Level
4 – Outlet Launder
5 – Net or Screen
6 – Outlet Pipe
7 – Bubble Diffusers
8 – Header Pipe
9 – Recirculated Sludge Pipeline
Parts of an Aerated Lagoon
Parts Functions
Inlet Pipe The inlet pipe brings the black liquor wastewater to aeration
tank.
Baffle Wall The baffle wall does not let the incoming wastewater go across
the tank toward the outlet pipe. The wall forces the mix toward
the bottom of the tank and thus ensuring maximum retention.
Outlet Launder The outlet launder collects the wastewater and delivers it to
the outlet pipe. It should be located farthest from the inlet
pipe
Net or Screen The net or screen prevents entry of debris in the outlet pipe.
Outlet Pipe The outlet pipe takes the wastewater to the final clarifier.
Bubble Diffusers The bubble diffusers are rigid pipes with long slots, which are
covered with rubber membranes. The compressed air is
released throughout the length of the diffusers, through
minute holes punched in the rubber membrane.
Header Pipe The header pipe supplies the compressed air in the diffusers.
Recirculated The recirculated sludge pipeline brings bacteria floc back to
Sludge Pipeline the aeration tank. It is always located very close to the inlet so
that the raw wastewater and bacteria get mixed thoroughly.
Design Assumptions
1. The wastewater from trickling filter is 103,241.51 kg.
2. The BOD of the influent wastewater is 118.93 ppm.
Design Requirements
1. Characteristics of Effluent
a. BOD
b. COD
c. TSS
2. Volumetric Flowrate of Effluent
3. Detention Time
4. Capacity
5. Surface Area
6. Activated Sludge Reactor Dimensions
7. Oxygen Requirement
8. Power Requirement
Design Calculations
1. Characteristics of Effluent
The characteristics of the effluent are determined by the efficiency of removal.
a. BOD 𝐵𝑂𝐷𝐸𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 𝐵𝑂𝐷𝐼𝑛𝑙𝑢𝑒𝑛𝑡 (1 − 𝑒𝑓𝑓𝑖𝑐𝑖𝑒𝑛𝑐𝑦)
𝐵𝑂𝐷𝐸𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = (118.93 𝑝𝑝𝑚)(1 − 0.85)
𝑩𝑶𝑫𝑬𝒇𝒇𝒍𝒖𝒆𝒏𝒕 = 𝟏𝟕. 𝟖𝟒 𝒑𝒑𝒎
b. COD 𝐶𝑂𝐷𝐸𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 𝐶𝑂𝐷𝐼𝑛𝑙𝑢𝑒𝑛𝑡 (1 − 𝑒𝑓𝑓𝑖𝑐𝑖𝑒𝑛𝑐𝑦)
𝐶𝑂𝐷𝐸𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = (220.88 𝑝𝑝𝑚)(1 − 0.80)
𝑪𝑶𝑫𝑬𝒇𝒇𝒍𝒖𝒆𝒏𝒕 = 𝟒𝟒. 𝟏𝟖 𝒑𝒑𝒎
c. TSS 𝑇𝑆𝑆𝐸𝑓𝑓𝑙𝑢𝑒𝑛𝑡 = 𝑇𝑆𝑆𝐼𝑛𝑙𝑢𝑒𝑛𝑡 (1 − 𝑒𝑓𝑓𝑖𝑐𝑖𝑒𝑛𝑐𝑦)
𝐿 = 2.55 𝑚
USE 𝑾 = 𝟏. 𝟕𝟎 𝒎
𝑳 = 𝟐. 𝟔𝟎 𝒎
7. Oxygen Requirement
The oxygen utilization of the activated-sludge system is based on total of the
oxygen required for energy or for oxidation and oxygen required for endogenous
respiration.
𝑇𝑜𝑡𝑎𝑙 𝑂𝑥𝑦𝑔𝑒𝑛 𝑅𝑒𝑞𝑢𝑖𝑟𝑒𝑑
= 𝑂𝑥𝑦𝑔𝑒𝑛 𝑓𝑜𝑟 𝐸𝑛𝑒𝑟𝑔𝑦 + 𝑂𝑥𝑦𝑔𝑒𝑛 𝑓𝑜𝑟 𝐸𝑛𝑑𝑜𝑔𝑒𝑛𝑜𝑢𝑠 𝑅𝑒𝑠𝑝𝑖𝑟𝑎𝑡𝑖𝑜𝑛
𝑇𝑜𝑡𝑎𝑙 𝑂𝑥𝑦𝑔𝑒𝑛 𝑅𝑒𝑞𝑢𝑖𝑟𝑒𝑑 = 𝑎′ (∆𝐵𝑂𝐷)𝑄 + 𝑏 ′ (𝑇𝑆𝑆𝑖𝑛𝑓𝑙𝑢𝑒𝑛𝑡 )𝑉
𝑇𝑜𝑡𝑎𝑙 𝑂𝑥𝑦𝑔𝑒𝑛 𝑅𝑒𝑞𝑢𝑖𝑟𝑒𝑑
𝑙𝑏 𝑂2 𝑚𝑔
= [0.79 (118.93 − 17.84 )
𝑙𝑏 𝐵𝑂𝐷𝑟 𝐿
T is the temperature in R
P1 is the absolute inlet pressure in psi
P2 is the absolute outlet pressure in psi
n = 0.0283 for air
e is efficiency, (usual range for compressor is 0.7 to 0.9)
𝑘𝑔 2.205 𝑙𝑏 1𝑑 𝑓𝑡 ∗ 𝑙𝑏
(29.39 )( ) (86,400 𝑠) (53.3 )(546 𝑅) 30.0 𝑝𝑠𝑖 0.283
𝑑 1 𝑘𝑔 𝑙𝑏 𝑎𝑖𝑟 ∗ 𝑅
𝑃= [( )
550 (0.0283)(0.80) 14.7 𝑝𝑠𝑖
− 1] = 0.3921ℎ𝑃
Design Specification
AERATED LAGOON SPECIFICATION SHEET
OPERATING DATA
Mode of Operation Continuous
Number of Units 1
To reduce BOD, COD and TSS prior to discharge to
Function
receiving body
Compound Raw Influent Treated Effluent
Volume
81.00 80.96
(m3/wk)
Feed
BOD (mg/L) 118.93 17.84
COD (mg/L) 220.88 44.18
TSS (mg/L) 279.30 55.86
TECHNICAL DATA
Detention Time 30.96 hours
Capacity 17.35 cu. m.
Surface Area 4.34 sq. m.
Height 3.50 m
Length 2.60 m
Width 1.70 m
Surface Loading Rate 4 m3/m2-d
Air Requirement 29.39 kg Air/d
Power Requirement 0.50 hP
Materials of Construction Concrete
EFFLUENT DATA
Flowrate 17.45 m3/d
EXISTING EQUIPMENT
Supplier Energreen Technology Inc.
Width = 1.7 m
Height = 3.5 m
Length = 2.6 m
Air Diffusers
Capacity = 17.35 m3
Concrete Tank
PIPING
Introduction
Piping includes pipe, flanges, fittings, bolting, gaskets, valves, and the pressure
containing portions of other piping components. It also includes pipe hangers and
supports and other items necessary to prevent overpressurization and overstressing
of the pressure-containing components. It is evident that pipe is one element or a part
of piping. Therefore, pipe sections when joined with fittings, valves, and other
mechanical equipment and properly supported by hangers and supports, are called
piping.
Oil and gas industries and other process industries are complex installation.
Piping systems are used in these plants to transport various fluids. These pipelines
transport various industrial materials such as gases such as air, nitrogen, oxygen,
hydrogen etc., liquids such as water, acids, hydrocarbon, toxic materials etc.
Without proper pipe color code, it is extremely difficult to identify the material
pipeline transporting. To reduces the safety hazard, reduce the possibility of mistakes
in identification and accidents associated with wrong identification of pipeline during
the emergency situation, systematic color coding of pipeline and piping system is
essential. Uniformity of color marking promotes greater safety, lessens the chances of
error and reduces hazards involved in the handling of material inside the pipelines.
One of the standards used for uniform color coding in industries is the ASME
A13.1 – Scheme for the Identification of Piping Systems. The purpose of ASME/ANSI
A13.1 Standard is to establish a common system that assists in the identification of
hazardous materials conveyed in piping systems and their hazards when released into
the environment.
ASME A13.1 – 2015 edition has six fixed colors and 4 users define colors that
can be used to identify the hazardous material. In this standard, following category are
used:
1) Flammable – fluids or a vapor or produce vapors that can be ignited and
continue to burn in air.
2) Combustible – fluids that can burn, but are not flammable.
3) Oxidizing – oxidizing fluid is any gas or liquid that may, generally by providing
oxygen, cause or contribute to the combustion of other material more than air
does.
4) Toxic and Corrosive – fluids that are corrosive or toxic, or will produce corrosive
or toxic substances when released.
5) Fire Quenching – fluid Such as water, foam, and CO2 used in sprinkler systems
and firefighting piping systems.
Pressure-Piping Codes
The code for pressure piping (ASME B31) consists of a number of sections
which collectively constitute the code. Table 10-18 of Perry's Chemical Engineers'
Handbook shows the status of the B31 code as of July 2005. The sections are
published as separate documents for simplicity and convenience. The sections differ
extensively. The ASME B31 code prescribes minimum requirements for materials,
design, fabrication, assembly, support, erection, examination, inspection, and testing
of piping systems subject to pressure or vacuum. The scope of the piping covered by
B31.3 is illustrated in Fig. 10-127.
The code also excludes piping systems designed for internal gauge pressures
at or above zero but less than 0.105 MPa (15 lbf/in2) provided the fluid handled is
nonflammable, nontoxic, and not damaging to human tissues, and its design
temperature is from −29°C (−20°F) through 186°C (366°F). Refer to the code for
definitions of nonflammable and nontoxic.
Some of the more significant requirements of ASME B31.3 (2004 edition) have
been summarized and incorporated in this section of the Handbook. For a more
A. Pipes
A.1 Classification of Pipes
Pipes are divided into two main categories: seamless and welded. Both have
advantages and disadvantages in terms of economy and function. Specifications
governing the production of these products dictate the permissible mechanical and
dimensional variations, and code design calculations account for these variations.
❖ Seamless Pipe
Seamless pipe may be formed by
various methods. A common technique involves
piercing solid round forgings, followed by rolling
and drawing. Since seamless products have no
weld joints, there is no reduction of strength due to weld joint efficiency. Standard
seamless pipes are more commonly used than welded pipes and they tend to be
more pressure resistant. Because of their lighter weight and thin walls, they are
used in liquid transportation.
Advantages
Seamless steel pipes have increased ability to withstand pressure.
Seamless steel pipe is a continuous extrusion of the alloy, meaning
that it will have a round cross section that you can count on, which
is helpful when you’re installing pipes or adding fittings.
Seamless pipes can perform well in harsh conditions, which means
that they can be used in extremely cold or hot environments.
❖ Welded Pipe
These products are typically made by forming strips
or plate into cylinders and seam-welding by various
methods. Manufacturing by welding permits the production
of larger diameter pipe than is possible with seamless
manufacturing methods, as well as larger diameter/wall thickness ratios. Welded
pipes are not typically used in high-pressure projects and are heavier than
seamless pipes. They transport gas more often than liquid.
Advantages
Welded pipes are typically more cost effective than their seamless
equivalents.
Welded pipes are usually more readily available than seamless.
The wall thickness of welded pipes is generally more consistent
than that of seamless pipes.
The internal surface of welded tubes can be checked before
manufacturing, which isn’t possible with seamless.
There are three (3) methods in joining pipes discussed. These are: welded joints,
branched connections and threaded joints.
❖ Welded Joints
The most widely used joint in
piping systems is the butt-weld joint.
In all ductile pipe metals which can be
welded, pipe, elbows, tees, laterals,
reducers, caps, valves, flanges, and V-
clamp joints are available in all sizes
and wall thicknesses with ends
prepared for butt welding. Joint strength equal to the original pipe (except for
❖ Branch Connections
Branch connections may be made with
manufactured tees, fabricated reinforced and
non-reinforced branch connections or
manufactured integrally reinforced branch
connections. Butt-welded fittings offer the best
opportunity for nondestructive examination; however, branch connections are
commonly specified for branches smaller than the header, and often best satisfy
the design and economic requirements.
❖ Threaded joints
Principal use of threaded joints
is in sizes 2 in. and smaller, in metals
for which the most economically
produced walls are thick enough to
withstand pressure and corrosion after
reduction in thickness due to
threading. For threaded joints over 2 in, assembly difficulty and cost of tools
increase rapidly. Careful alignment, required at the start of assembly and during
rotation of the components, as well as variation in length produced by diametral
tolerances in the threads, severely limits preassembly of the components.
Threading is not a precise machining operation, and filler materials known as
“pipe dope” are necessary to block the spiral leakage path.
B. Valves
Valves are an essential part of any piping system which serve the functions of
allowing, stopping, regulating, and controlling the flow, to fulfill the intended objectives
of the system. When fluid pressure builds up beyond a set limit, the valves relieve the
overpressure to safeguard the integrity of the piping system or a component. Valves
help in maintaining or breaking a vacuum. Valves also assist in maintaining the
pressure or temperature of the flow medium within the desired range or limit.
(L-R) gate valve, globe valve, diaphragm valve, pinch valve and lift check valves
❖ Rotary Motion Valves
When the valve-closure member travels along an angular or circular path, as
in butterfly, ball, plug, eccentric- and swing check valves, the valves are called
rotary motion valves.
(L-R) butterfly valve, ball valve, plug valve and swing check valves
Typical Applications
Socket or butt-welding end-gate valves in air, fuel gas, feed water, steam,
lube oil, and other systems are typical applications. Threaded-end gate valves may
be used in air, gaseous, or liquid systems. Concern for leakage from threaded
connection can be addressed by seal welding the threaded connection or by using
❖ Globe Valve
Conventional globe valves may be used for
isolation and throttling services. Although these
valves exhibit slightly higher pressure drops than
straight-through valves (e.g., gate, plug, ball, etc.),
they may be used where the pressure drop through
the valve is not a controlling factor
.
Advantages
3. High-point vents and low-point drains when leak tightness and safety are
major considerations.
4. Feed water, chemical feed, condenser air extraction, and extraction drain
systems.
5. Boiler vents and drains, main steam vents and drains, and heater drains.
❖ Ball Valves
The ball valve is a quarter-turn valve
suitable for clean gas, compressed air, and
liquid service. They also can be used for
slurry service, but provisions for prevention
of crud build-up must be made. The use of
soft-seat materials such as nylon, delrin,
synthetic rubbers, and fluorinated polymers imparts excellent sealing ability. With
fluorinated polymer seats, ball valves can be used for service temperatures ranging
from 450 to 500ºF (270º to 260ºC); with graphite seats, service temperatures to
1000ºF (538ºC) or even higher are possible. Also, with metal-backing seats, the valves
can be used in fire-safe services. Ball valves are nonbinding and provide leak-tight
closure. The valves exhibit negligible resistance to flow because of their smooth body
and port.
Advantages
❖ Plug Valve
Plug valves, also called cocks, generally are used
for the same full-flow service as gate valves, where
quick shutoff is required. Plug valves are not generally
designed for the regulation of flow. Nevertheless, in
some applications, specially designed plugs are used
for this purpose, particularly for gas-flow throttling.
Advantages
Simple design with few parts
Quick to open or close.
Can be serviced in place.
Typical applications
As indicated earlier, the plug valves can be and have been used in many
different fluid services. They perform well in slurry applications. They are primarily
used in bubble-tight services as on-off stop valves. The wiping-off action of a plug
does not permit suspended particles to accumulate and form crud. The following
are some typical applications of plug valves:
1. Air, gaseous, and vapor services
2. Natural gas piping systems
3. Coal slurries, mineral ores, mud, and sewage applications
4. Oil piping systems 5. Vacuum to high-pressure applications
❖ Diaphragm Valves
These valves consist of a rigid body formed with a weir placed in the flow path, a
flexible diaphragm which forms the upper pressure boundary of the valve, a
compressor which is used to force the diaphragm against the weir, and the bonnet and
hand-wheel which secure the diaphragm to the body and actuate the compressor.
Diaphragm valves are available in a wide choice of body, diaphragm, and lining
materials that are suitable for service with a wide variety of chemicals. For severe
corrosive applications, diaphragm valves are made of stainless steel or PVC plastics,
or they are lined with glass, rubber, lead, plastics, titanium, or still other materials.
Some of the common materials used for diaphragms are listed in table given.
Advantages
Can be used as on-off and throttling service valves
Offer good chemical resistance due to variety of linings available
Stem leakage is eliminated
Provides bubble-tight service
Does not have pockets to trap solids, slurries, and other impurities. It is
suitable for slurries and viscous fluids
These valves are particularly suitable for hazardous chemicals and
radioactive fluids
These valves do not permit contamination of flow medium, thus they are
used extensively in food processing, pharmaceutical, brewing, and other
applications which cannot tolerate any contamination.
Disadvantages
The weir may prevent full drainage of piping\
Working temperatures and pressures are limited by the diaphragm
material. Generally, the pressures are limited to 200 psi (1380 kPa) and
temperatures up to 400ºF (204ºC)
The diaphragm may also limit the hydrostatic pressure.
The diaphragm may experience erosion when used extensively in severe
throttling service containing impurities
Diaphragm valves are available in limited sizes, usually NPS ¹⁄₂ to 12 (DN
15 to 300).
Typical Applications
❖ Butterfly Valves
Butterfly valves are used to control and regulate or
throttle the flow. They are characterized by fast operation
and low-pressure drop. They require only a quarter-turn from
closed to full-open position. A butterfly valve has a short
circular body, a round disc, shaft, metal-to-metal or soft
seats, top and bottom shaft bearings, and the stuffing box. Sometimes butterfly valves
are manufactured in rectangular or square configurations.
Advantages
The compact design requires considerably less space, compared to gate,
globe, or other valves
Light in weight
Quick acting; as a quarter-turn valve, it requires less time to open or close
It is available in large sizes, ranging from NPS 1¹⁄₂ (DN 40) to over NPS
200 (DN 5000)
They have low-pressure drop and high-pressure recovery
Provide bubble-tight service.
Disadvantages
Throttling service is limited to low differential pressure
Throttling is restricted to a 30- to 80-degree disc opening. Location of
valve, pipe routing, free, and closed discharge are to be considered while
using a butterfly valve in a throttling application
Cavitation and choked flow are two potential concerns
The disc movement is unguided and affected by flow turbulence
Typical Applications
Concentric or low-pressure and low-temperature butterfly valves, the high-
performance butterfly valves, cover a wide range of applications. These
applications include:
1. Cooling water, air, gases, and other similar applications, such as fire
protection, circulating water, etc.
2. Corrosive services requiring lined valves
3. Food processing, chemical, and pharmaceutical services
4. Slurry and similar services
5. High-pressure and high-temperature water and steam services
❖ Check Valves
Check valves are designed to pass flow in one direction with minimum resistance
and to prevent reverse or backflow with minimal leakage. Check valves are available
in sizes from NPS ¹⁄₄ (DN 6) through NPS 72 (DN 1800). Other sizes may be made
available to meet specific size requirements. Depending upon the design requirements
of a piping system, a check valve may have butt welding, socket welding, threaded, or
flanged ends.
Advantages
Check valves are self-actuated
Check valves require no external means to actuate the valve either to
open or close.
Check valves are fast acting
Disadvantages
Since all moving parts are enclosed, it is difficult to determine whether
the valve is open or closed. Furthermore, the condition of internal parts
cannot be assessed.
Each type of check valve has limitations on its installation configurations
C. Fittings
Directional changes in piping systems are typically made with bends or welded
fittings. Bends are made as either hot bends or cold bends. Cold bending is done at
temperatures below the material transformation temperature. Depending on the
material and the amount of strain involved, annealing or stress relief may be required
after bending.
Pipe fittings are either male fittings or female fittings. In threaded pipe fittings,
female threads are on the inside while male threads are on the outside. Pipe fittings
that have one female end and one male end are called street fittings. Pipe fittings are
used to connect pipes or tubes in two ways:
• By slip fit: Slip fit pipes use sleeves that slip into one another. The plastic pipes
are either threaded or slip fit.
Couplings
Adapters
Unions
Flanges
45º elbow
90º elbow
Tees
Cross
Wyes
Reducers
FACTORS TO BE CONSIDERED
The following items should be considered by the engineer when developing the
design for a piping system:
Identification of parts needed for design will generally give you an outlook on
what you are about to design. This will incorporate chemical engineering principles in
line with what is required as a standard. Determining this will also set your focus on
what parameter must be firstly acquired.
This image shows a picture of several component of one part in a piping system.
But in general, fluid, pipe, valves, fittings, fasteners, measuring devices and pump are
the basic and most important parts of piping system. This will determine what are
needed in your design.
7
5 3
6
4
2
PARTS DESCRIPTION
1. Fluid Material that is being transported
2. Pipe Material where the fluid is being transported
After knowing and identifying the parts, we must know underlying principles and
the method of designing the piping system.
FLUIDS
Transportation and the storage of fluids (gases and liquids) involve the
understanding of the properties and behavior of fluids. Flows can be classified into two
major categories: (a) incompressible and (b) compressible flow. Most liquids fall into
the incompressible flow category, while most gases are compressible in nature. A
perfect fluid can be defined as a fluid that is nonviscous and nonconducting. Fluid flow,
compressible or incompressible, can be classified by the ratio of the inertial forces to
the viscous forces. This ratio is represented by the Reynolds number (NRe).
𝐷𝜈𝜌
𝑁𝑅𝑒 =
𝜇
where, ρ is the density of the fluid, V the velocity, D the diameter, and μ the
viscosity of the fluid. At a low Reynolds number, the flow is considered to be laminar,
and at high Reynolds numbers, the flow is considered to be turbulent.
Materials of Construction
Materials of construction will determine the required property of the pipe that
will not allow any damage in terms of corrosion, thermal expansion and even internal
and external stress.
Standards allow designers and users of materials to work with confidence that
the materials supplied will have the expected minimum properties. A few of the
organizations which generate standards of major importance to the chemical-process
industries in the United States are listed below.
3. American Society for Testing and Materials (ASTM). This society generates
specifications for most of the materials used in the ANSI Piping Codes and the
ASME Boiler and Pressure Vessel Codes.
PIPE
Sizing
The design engineer must specify the diameter of pipe that will be used in given
piping system, and economic factors must be considered in determining the optimum
pipe diameter.
Pipe Strength
Iron and steel pipes were originally classified on the basis of wall thickness as
standard, extra-strong, and double-extra-strong. Modem industrial demands for more
exact specifications have made these three classifications obsolete. Pipes are now
specified according to wall thickness by a standard formula for schedule number as
designated by the American Standards Association.
2 ST tm
Pb =
Dm
Pipe sizes are based on the approximate diameter and are reported as nominal
pipe sizes. Although the wall thickness varies depending on the schedule number, the
outside diameter of any pipe having a given nominal size is constant and independent
of the schedule number. This permits the use of standard fittings and threading tools
on pipes of different schedule numbers.
Valves are mechanical devices that control the flow and pressure within a
system or process. They are essential components of a piping system that conveys
liquids, gases, vapours, slurries etc. Some valves are self-operated while others
manually or with an actuator or pneumatic or hydraulic is operated. Its functions were
to slow down or stop the flow of a fluid, to reduce or increase the flow rate of a fluid,
to control the direction of a flow and to regulate process pressure.
Pipe fittings are widely demanded for any piping and plumbing systems used in
industrial and commercial applications. Fittings allow pipes to be joined or installed in
the appropriate place and terminated or closed where necessary. Fittings are available
in various shapes and sizes. They can be expensive, require time, and different
materials and tools to install. They are an essential part of piping and plumbing
systems. There are thousands of specialized fittings manufactured. Each type of pipe
or tube requires its own type of fitting, but usually all pipe fittings share some common
features. Pipe fittings are available everywhere where plumbing materials are sold.
Frictional Loss
0.046
f =
(N Re )0.2
0.04
f =
(N Re )0.16
Fanning Equation
If the linear velocity, density, and viscosity of the flowing fluid remain constant
and the pipe diameter is uniform over a total pipe length L, the equation will give:
−p f 2 fV 2 L
F= =
gc D
PUMPS/COMPRESSORS
Pump Selection
Pumps are used to transfer fluids from one location to another. The pump
accomplishes this transfer by increasing the pressure of the fluid and, thereby,
supplying the driving force necessary for flow. The different types of pumps commonly
employed in industrial operations can be classified as
2. Rotary positive-displacement pumps with no valve action: gear pumps, lobe pumps,
screw pumps, eccentric-cam pumps, metering pumps
3. Rotary centrifugal pumps with no valve action: open impeller, closed impeller, volute
pumps, turbine pumps
4. Air-displacement systems: air lifts, acid eggs or blow cases, jet pumps, barometric
legs
Many different factors can influence the final choice of a pump for a particular
operation. The following list indicates the major factors that govern pump selection:
1. The amount of fluid that must be pumped. This factor determines the size of pump
(or pumps) necessary.
2. The properties of the fluid. The density and the viscosity of the fluid influence the
power requirement for a given set of operating conditions; corrosive properties of
the fluid determine the acceptable materials of construction. If solid particles are
suspended in the fluid, this factor dictates the amount of clearance necessary and
may eliminate the possibility of using certain types of pumps.
3. The increase in pressure of the fluid due to the work input of the pumps. The head
change across the pump is influenced by the inlet and downstream-reservoir
pressures, the change in vertical height of the delivery line, and frictional effects.
This factor is a major item in determining the power requirements.
Power Requirements
A major factor involved in the design of pumping and piping systems is the
amount of power that is required for the particular operation. Mechanical power must
be supplied by the pump to overcome frictional resistance, changes in elevation,
changes in internal energy, and other resistances set up in the flow system. The various
forms of energy can be related by the total energy balance or the total mechanical-
energy balance.
In differential form,
g V dV
dZ + vdP + i i = SWs − F
gc gc
To cause liquid to flow, work must be expended. A pump may raise the liquid to
a higher elevation, force it into a vessel at higher pressure, provide the head to
overcome pipe friction, or perform any combination of these. Regardless of the service
required of a pump, all energy imparted to the liquid in performing this service must
be accounted for; consistent units for all quantities must be employed in arriving at the
work or power performed.
MEASURING EQUIPMENT
Flow
Orifice meters, venturi meters, rotameters, and displacement meters are used
extensively in industrial operations for measuring the rate of fluid flow. Other flow-
measuring devices, such as weirs, pitot tubes, anemometers, and wet-test meters, are
also useful in industrial operations.
Temperature
Thermocouples
There are certain general principles that should be adhered to in the design of
piping systems as well as the selection and application of fittings. Some of the following
are:
Wherever possible, pipe lines should be run in straight lines with right-angled
turns. It is undesirable to run a pipe lines at odd angles even though it shortens
the line and reduces the number of fittings.
When a pipe makes a right-angled turn, it is good practice to use a tee with one
opening closed by a pipe plug or cap or a cross with two closed openings rather
than an elbow. This will permit subsequent connections without breaking a
number of joints and will facilitate cleaning.
For connections that are not feasible with the right-angles turns, the use of two
45° elbows is suggested for most cases.
For screwed fittings, pipe should be carefully cut to the proper length and the
interior edge burred or reamed to prevent constriction and sharp edges.
Special fabricated fittings such as expansion bends and coiled piping must be
carefully specified so that they will fit properly.
In all piping systems, valves should be installed in such a manner that they
may be repacked, if necessary, without closing the line. Valves should not be
used to brace a pipe or carry the weight of the line, since distortion of the valve
may result in inefficient operation and require an excessive amount of
maintenance.
DESIGN PROCEDURE
Establish the location of the pipelines: its source and destination, required bends, the
terrain over which it will pass.
1. Determine the total length of straight pipeline and all the fittings required.
2. Establish the characteristics of the fluid to be carried, including its density,
viscosity, and amount.
3. From the piping design equations given by Peters and Timmerhaus, calculate
the time of transport
4. Calculate the pipe dimensions, of which the diameter and wall thickness is
inclusive of
5. Calculate the total head, including friction losses, potential, kinetic, and
pressure heads
6. Calculate for the net positive suction head (NPSH)
7. Calculate for the power requirement of the pump
DESIGN PROBLEM
Wastewater amounting to 107,976.96 kg/batch needs to be transported to the
neutralization contact basin from the flow equalization basin. Design a piping system
of optimal aspects and dimensions.
DESIGN DESCRIPTION
Wastewater from the process equipment is conveyed using a piping system to
the wastewater receiving basin to be treated in the subsequent processes. A pump
provides the required head to transport the fluid and a valve is used to regulate the
flow. Valves and fittings modify, control, and regulates the flow.
DESIGN SELECTION
Among the choices of piping material, carbon steel is chosen as it is the most
compatible and suitable material in handling a wide variety of common chemical
substances. (Metcalf and Eddy). For general conveying of liquids with water-like
properties, low pressure drop, and short to medium distances, a single centrifugal
pump is most suitable (Peters and Timmerhaus). Globe valves are used for general
conveying of dirty liquids with water-like properties with or withouth throttling required
(Process Equipment Design)
DESIGN CONSIDERATION
1. The material of construction of pipeline is carbon steel. (Metcalf and Eddy)
2. The fluid velocity recommended for water-like fluids ranges from 1.0 to 3.0 m/s.
Fluid velocity of 1.0 m/s is considered (Plant Design and Economics for
Chemical Engineers by Peters and Timmerhaus 5th Ed., Table 12-3, p.501)
3. The efficiency of centrifugal pumps is 45% at 100 gpm, 70% at 500 gpm, 80%
at 10,000 gpm (Chemical Process Equipment by Couper, p. xviii)
DESIGN REQUIREMENTS
1. Time of Transport c. Kinetic Head
2. Pipe Dimensions d. Pressure Head
3. Total Head 4. Net Positive Suction Head
a. Friction Losses (NPSH)
b. Potential Head 5. Power Requirement
DESIGN CALCULATIONS
1. Time of Transport
In computing for the piping time, the optimum diameter equation for turbulent flow
by Timmerhaus (Chemical Engineering Design 5th Ed., Equation 12-15 p. 501) and
the fluid velocity formula is used. The optimum diameter formula is,
𝐷𝑖,𝑜𝑝𝑡 = 0.363𝑄 0.45 𝜌0.13 (1)
where
Di,opt = optimum diameter
Q = volumetric flowrate
ρ = the fluid density
The fluid velocity formula is,
𝑄
𝑣= (2)
𝐴
where
v = fluid velocity
A = cross-sectional area of pipe
Q = volumetric flowrate
Elaborating equation (2),
𝑚
𝜌𝑡
𝑣= 𝜋 (3)
𝐴 4 𝐷𝑖,𝑜𝑝𝑡 2
By relating equations (1) and (3), the diameter variable is eliminated and the
time variable can be isolated, giving,
10
9.6627𝑚0.10
𝑡=( ) (4)
𝑣𝜌0.36
9.6627(107,976.96 kg)0.10
𝑡=
𝑚 𝑘𝑔 0.36
(1.0 𝑠 ) (1059.06 3 )
( 𝑚 )
𝑚𝑖𝑛
𝑡 = 9876.48 𝑠 ×
60𝑠
𝑡 = 164.61 𝑚𝑖𝑛
Use = 165 minutes
2. Pipe Diameter
The volumetric flowrate is first calculated as,
𝑉
𝑄=
𝑡
107,976.96 𝑘𝑔
( )
𝑘𝑔
1059.06 3
𝑄= 𝑚
9876.48𝑠
𝑚3
𝑄 = 0.0103
𝑠
Substituting know and calculated values to equation (1),
𝐷𝑖,𝑜𝑝𝑡 = 0.363𝑄 0.45 𝜌0.13
0.45
𝑚3 𝑘𝑔 0.13
𝐷𝑖,𝑜𝑝𝑡 = 0.363 (0.0103 ) (1059.06 )
𝑠 𝑚3
39.37 𝑖𝑛
𝐷𝑖,𝑜𝑝𝑡 = 0.1146 ×
𝑚
𝐷𝑖,𝑜𝑝𝑡 = 4.5118 𝑖𝑛
Use: 5.0 in, Sch. 40
From Appendix A.5 of Principles of Transport Processes and Unit Operation by
Geankoplis (p.892), the standard dimensions of 5-in nominal pipe are,
Inner Outer
Nominal Pipe Thickness Cross-Sectional
Diameter Diameter
Size (in) Area (ft2)
(in) (in)
3. Total Head
The total head is calculated using the mechanical energy balance:
∆v 2 g ∆P
−Ws = lw𝑓 + + ∆z +
2g c gc ρ
a. Friction Losses (lwf)
To solve for the friction loss, the friction loss formula by Brown is used (Unit
Operations, Equation 63, p.136):
𝑓𝐿𝑣 2
𝑙𝑤𝑓 =
2𝑔𝑐 𝐷
where
lwf = friction losses
f = friction factor
L = equivalent length of pipe
V = fluid velocity
D = internal diameter of pipe
where
f = friction factor
ε = roughness (0.00015m for commercial steel pipes)
NRe = Reynold’s number
D = pipe diameter
0.00015 𝑚
( 𝑚 )
1 5.047𝑖𝑛 × 39.37 𝑖𝑛 2.52
= −2 log +
√f 3.7 (67,882.43)√f
( )
𝑓 = 0.02362
The equivalent length (L) of the piping system is calculated using Figure 127 of
Unit Operations by Brown (p. 141)
3.28084 𝑓𝑡
𝐿 = (12 𝑚 × ) + 160 𝑓𝑡 + 14𝑓𝑡
𝑚
𝐿 = 213.37𝑓𝑡
𝑓𝐿𝑣 2
𝑙𝑤𝑓 =
2𝑔𝑐 𝐷
2
𝑚 1 𝑓𝑡
(0.02362)( 213.37𝑓𝑡) (1.0
𝑠 × 0.3048 𝑚)
𝑙𝑤𝑓 =
𝑙𝑏 − 𝑓𝑡 1 𝑓𝑡
2 (32.2 ) (5.047𝑖𝑛 × 12 𝑖𝑛)
𝑙𝑏𝑓 − 𝑠 2
𝑓𝑡 − 𝑙𝑏𝑓
𝑙𝑤𝑓 = 2.0026
𝑙𝑏𝑚
b. Potential Head
The potential head is calculated using the elevation in the piping system,
𝑔
∆𝑧 =0
𝑔𝑐
c. Kinetic Head
Since there are no reductions and enlargement in pipe size,
∆𝑣 2
=0
2𝑔𝑐
d. Pressure Head
Since the inlet and outlet of the piping system are both at atmospheric
pressure,
∆𝑃
=0
𝜌
𝑘𝑔 𝐽 1𝑁𝑚 1𝑃𝑎
𝑁𝑃𝑆𝐻 = (1059.06 ) (3.2563 × × ) − (3,168𝑃𝑎)
𝑚3 𝑘𝑔 1𝐽 1𝑁
𝑚2
𝑚3
𝑁𝑃𝑆𝐻 = 3445.45 𝑃𝑎 × = 3.2533 𝐽/𝑘𝑔
1059.06𝑘𝑔
Use: 3.25 J/kg
5. Power Requirement
The theoretical power requirement is calculated based on the mass flowrate and
the total head:
𝑃𝑡ℎ𝑒𝑜𝑟𝑒𝑡𝑖𝑐𝑎𝑙 = 𝑚̇𝑊𝑠
107976.96𝑘𝑔 𝐽
𝑃𝑡ℎ𝑒𝑜𝑟𝑒𝑡𝑖𝑐𝑎𝑙 = ( ) (3.2563 )
9876.476212𝑠 𝑘𝑔
𝑃𝑡ℎ𝑒𝑜𝑟𝑒𝑡𝑖𝑐𝑎𝑙 = 35.60𝑊
35.60 𝑊
𝑃𝑎𝑐𝑡𝑢𝑎𝑙 =
0.45
ℎ𝑝
𝑃𝑎𝑐𝑡𝑢𝑎𝑙 = 79.11 ×
745.7 𝑊
𝑃𝑎𝑐𝑡𝑢𝑎𝑙 = 0.1061 ℎ𝑝
Use = 0.25 hp
DESIGN SPECIFICATIONS
PIPING SYSTEM
OPERATING DATA
Control systems are used to maintain process conditions at their desired values
by manipulating certain process variables to adjust the variables of interest.
The type of control system shown in the figure is termed a closed-loop feedback
control system. Closed-loop refers to the fact that the controller automatically acts to
return the controlled variable to its desired value. In contrast, an open-loop system
would have the measurement signal disconnected from the controller, and the
controller output would have to be manually adjusted to change the value of the
controlled variable. An open-loop system is sometimes said to be in manual mode as
opposed to automatic mode (closed-loop).
DEFINITIONS
Block diagram — Diagram that indicates the flow of information around the control
system and the function of each part of the system.
Closed loop — In closed loop, the measured value of the controlled variable is fed back
to the controller.
Controller — A device that outputs a signal to the process based on the magnitude of
the error signal. A proportional controller outputs a signal proportional to the error.
Disturbances — Any process variables that can cause the controlled variable to change.
In general, disturbances are variables that we have no control over.
Error — The difference between the values of the set point and the measured variable.
Negative feedback — In negative feedback, the error is the difference between the set
point and the measured variable (this is usually the desired configuration).
Open loop — In open loop, the measured value of the controlled variable is not fed back
to the controller.
Block diagram indicates the flow of information around the control system and
the function of each part of the system.
TYPES OF CONTROLLERS
Response of a typical control system showing the effects of various modes of control
TYPES OF SENSORS
A. Temperature Sensors
THERMISTOR. Thermistors are one of the most commonly used devices
for the measurement of temperature. Thermistors are thermal resistors. They
are resistors whose resistance changes with the temperature. There are two
kinds of thermistors,
Advantage of Thermistors
Advantage of Thermocouples
Disadvantages of Thermocouples
• Thermocouples generate a quite low level output signal. Besides, the resulting
output tends to be non-linear due to which a sensitive and stable device is
needed for temperature measurement. The measuring device should be
B. Pressure Sensors
THERMAL PRESSURE SENSOR. Thermal Pressure Sensor Uses the
changes in thermal conductivity of a gas due to density changes to measure
pressure. A common example of this type is the Pirani gauge. The Pirani gauge
is a robust thermal conductivity gauge used for the measurement of the
pressures in vacuum systems. It was invented in 1906 by Marcello Pirani.
Hg, differential pressures up to 750 in. water, and gauge pressures up to 6,000
psig (42 MPa).
C. Level Sensors
FLOAT SENSOR. Float sensors are so called because of its main system
that appears to float in the body of certain liquid substance.
TYPES OF ACTUATORS
FEATURES:
OPERATION:
Design Procedure
1. Describe and explain the equipment operation and the process control
operation of the equipment
3. Determine the Controller Mode and Final Control Elements and explain why they
were selected
5. Determine the control system of the equipment and create block diagrams
based on the number of the controlled variables.
SAMPLE DESIGN
G. Setpoints: 105°C
The temperature inside the horizontal paddle dryer is should be fixed at 105°C. A
variable change of 5% was considered for each parameter.
Figure 8.46: Piping and Instrumentation Diagram of Acetic Acid Storage Tank
where: LT = level transmitter LC = level control
I. Operation
A. Equipment Operation
The storage tank is used to store 1,787.89 kg acetic acid which is sufficient for
a 13-batch operation (137.53 kg/batch). The acetic acid is sourced from Czembi
Chemical in Kawit, Cavite and the refill of fluid inside the storage is done every week.
A normally open gate valve and spectacle blind is installed in the inlet line to allow the
introduction of acetic acid in the tank. A float-activated chain level gauge is used to
monitor the level inside the tank and it sends electric signal to the gate valve for the
control of acetic acid discharge. A centrifugal pump is used to transport the methanol
to the Nutsche filter 3.
Figure 8.47: Float-Activated Chain Level Gauge as Measuring Element Applied in the
Acetic acid Storage Tank
To monitor the acetic acid level, a float-activated chain level gauge is applied.
It consists of a float which rests on the surface of the liquid. The movement of the float
is transmitted to a pointer which indicates the liquid level on a calibrated scale. This
particular type of level indicator is low in cost, reliable, and operate over a large
temperature range (Instrumentation and Process Control, 2nd Edition by Kumar et al,
p. 24).
The mechanism of the float-activated chain level gauge depends on the liquid
level rise in the iso-butanol storage tank and the movement of the float installed. The
arm of the float causes the wiper to move over a potential divider whose output
terminals are connected to a voltmeter. As the float rises, a greater part of the potential
divider is included in the output circuit giving an increased output voltage. Hence, the
output voltage is directly proportional to the liquid level. The output terminals from the
potential divider is taken to a remote for display and is used to send electric signal to
the final control element.
D. Controller Mode: Proportional Integral Derivative (PID) Controller
The PID controller, also known as the three mode controller, was adopted in all
the process controls of Esolite Chemicals Inc. It is the most versatile of all controller
actions. The proportional part of this controller multiplies the error by a constant. The
integral part integrates the error. Finally, the derivative part differentiates the error.
The functions of the individual proportional, integral, and derivative controllers
complement each other. The combination of the three results to a system that
responds quickly to changes, tracks required positions, and reduces steady state
errors. When the controller detects a detrimental change in the system, the controller
automatically integrates or derives the error back to the setpoint.
E. Final Control Element: One (1) Gate Valve
Figure 8.48: Gate Valve as Final Control Element Applied in the Acetic Acid Storage
Tank
Control valves are the single most common type of final control element in a
process. For the level control of the methanol storage tank, a gate valve was used. The
actuators of these control valves are powered by an electric motor. Electric actuators
employ an electromagnet that move the stem which allows the valve to either be fully
opened or closed. The intensity of magnetic field created by the electromagnet is
influenced by the signals transmitted by the measuring elements. It offers the highest
precision-control positioning with an accuracy of +/- 0.000315 in. and a repeatability
of less than 0.0000394 in (Penton Corporate, 2017). Their setups are scalable for any
purpose or force requirement, and are quiet, smooth, and repeatable. Furthermore,
since there are no fluid leaks such as in the case of pneumatic or hydraulic actuators,
environmental hazards are eliminated.
F. Control System: Feedback Control Closed-Loop System
Feedback control closed-loop system utilizes loop structure with negative
feedback that brings a measurement to the desired setpoint. It is selected over the
open-loop as it allows corrective actions leading to the desired accuracy of the involved
parameter. The block diagram depicting the loop of level control was presented in
Figure 8.49.
Alkalization Reactor
I. Operation
A. Equipment Operation
The alkalization tank is used to mix the ground abaca stripping waste and the
formulated 18% NaOH solution to produce a mixture containing alkali cellulose. This
is done by introducing first the 1,970.20 kg of NaOH solution to the top inlet nozzle of
the tank. Afterwards, 656.73 kg of abaca stripping waste are fed in the top opening of
the equipment via screw conveyor. Then, a process control engineer will switch on the
propeller agitator which is powered by an electric motor. A resistance thermometer
detector is mounted on the tank to ensure that the temperature is maintained at 70°C.
A C-spring Bourdon tube pressure gauge is mounted as well to vent a portion of the
vapor in case of occurrence of build-up pressure during the operation. Lastly, a float-
activated chain level gauge is installed to ensure that the process is operated within
the target liquid level limits.
B. Process Control Operation
The equipment requires three process controls: pressure control, temperature
control, and level control. These parameters were measured using C-spring Bourdon
tube pressure gauge, resistance thermometer detector, and float-activated chain level
gauge, respectively. Control valves, particularly two (2) gate valves, were used as the
final control elements for the pressure and level control system. On the other hand, for
the temperature control, a bulb-and-capillary thermostat is used.
Proportional Integral Derivative Controller is applied as it is the most versatile
of all controller actions that can respond quickly to changes (derivative mode), track
required positions (proportional mode), and reduce steady state errors (integral mode).
Finally, a feedback control closed-loop system is selected over the open-loop as it
allows corrective actions leading to the desired accuracy of parameters.
C. Mode of Operation: Batch Process
D. Residence Time: 1 hour
II. Equipment Control
A. Controlled Variables: Pressure, Temperature, and Liquid Level
In alkalization, the pressure, temperature, and liquid level inside the tank must
be set at constant value. In this way, consistent quality and quantity of alkalization
mixture will be obtained.
B. Manipulated Variables: Vent Vapor Flowrate, Electric Current, and Alkalization
Mixture Flowrate
The pressure inside the alkalization tank is manipulated by opening or closing
the gate valve installed in the vent pipeline. On the other hand, the temperature and
liquid level is manipulated by the bulb-and-capillary thermostat for electric current and
gate valve for the discharge alkalization mixture flowrate, respectively.
C. Measuring Elements: C-Spring Bourdon Tube Pressure Gauge, Resistance
Thermometer Detector, and Float-Activated Chain Level Gauge
a b c
in units of temperature instead of units in ohms. This is selected over the other
temperature sensors as it is applicable for a temperature range of -80 to 320°C with
a measurement inaccuracy of only 0.5% which is 10 times more accurate than a
thermocouple. Since the operating temperature of the alkalization tank is only 70°C,
then this particular instrument is deemed to be applicable for the intended equipment
(Perry's Chemical Engineering Handbook, 8th Edition by Perry and Green, p. 8-56 to 8-
57).
Lastly, to monitor the level of alkalization mixture, a float-activated chain level
gauge is applied. It consists of a float which rests on the surface of the liquid. The
movement of the float is transmitted to a pointer which indicates the liquid level on a
calibrated scale. This particular type of level indicator are low in cost, reliable, and
operate over a large temperature range (Instrumentation and Process Control, 2nd
Edition by Kumar et al, p. 24).
The mechanism of the float-activated chain level gauge depends on the liquid
level rise in the alkalization tank and on the movement of the float installed. The arm
of the float causes the wiper to move over a potential divider whose output terminals
are connected to a voltmeter. As the float rises, a greater part of the potential divider
is included in the output circuit giving an increased output voltage. Hence, the output
voltage is directly proportional to the liquid level. The output terminals from the
potential divider is taken to a remote for display and is used to send electric signal to
the final control element.
D. Controller Mode: Proportional Integral Derivative (PID) Controller
The PID controller, also known as the three mode controller, was adopted in all
the process controls of Esolite Chemicals Inc. It is the most versatile of all controller
actions. The proportional part of this controller multiplies the error by a constant. The
integral part integrates the error. Finally, the derivative part differentiates the error.
The functions of the individual proportional, integral, and derivative controllers
complement each other. The combination of the three results to a system that
responds quickly to changes, tracks required positions, and reduces steady state
errors. When the controller detects a detrimental change in the system, the controller
automatically integrates or derives the error back to the setpoint.
E. Final Control Elements: Two (2) Gate Valves and One (1) Bulb-and-Capillary
Thermostat
a b
(a)
(b)
(c)
Figure 8.17: Loops for (a) Pressure Control, (b) Temperature Control, and (c) Level
Control
G. Setpoints: 101.325 kPa, 70°C, and 2,626.93 kg alkalization mixture removal per
batch
The pressure, as well as the temperature and liquid level inside the alkalization
tank, is fixed at 101.325 kPa, 70°C, and 2,626.93 kg alkalization mixture removal per
batch, respectively. A variable change of 5% was considered for each parameter.
Final
Controlled Measuring Manipulated Controlle
Equipment Control Setpoint
Variable Element Variable r Mode
Element
Resistance Bulb-and-
1. Horizontal Electric PID
Temperature Thermometer Capillary 105oC
Paddle Dryer Current Controller
Detector Thermostat
Float-
Discharge
2. Acetic Acid Activated Globe PID 137.53
Liquid Level Acetic Acid
Storage Tank Chain Level Valve Controller kg/batch
Flowrate
Gauge
C-Spring
Bourdon Tube Vent Vapor PID 101,325
Pressure Gate Valve
Pressure Flowrate Controller kPa
Gauge
Resistance Bulb-and-
3. Alkalization Electric PID
Temperature Thermometer Capillary 70oC
Reactor Current Controller
Detector Thermostat
Float- Discharge
Activated Alkalization PID 2,626.93
Liquid Level Gate Valve
Chain Level Mixture Controller kg/batch
Gauge Flowrate
Total Number of Resistance Thermometer Detector
Total Number of C-Spring Bourdon Tube Pressure Gauge
Total Number of Positive-Displacement Meter
Total Number of Float-Activated Chain Level Gauge
Total Number of Rotating Paddle Wheel Level Sensor
Total Number of Gate Valve
Total Number of Globe Valve
Total Number of Rotary Valve
Total Number of Bulb-and-Capillary Thermostat