Correlations

Temperature NaCl Time TBA FFA PV

Pearson Correlation 1 ,000 ,000 ,467* -,027 ,521*

Temperature Sig. (2-tailed) 1,000 1,000 ,038 ,909 ,018

N 20 20 20 20 20 20
Pearson Correlation ,000 1 ,000 ,114 ,048 ,305
NaCl Sig. (2-tailed) 1,000 1,000 ,633 ,842 ,191
N 20 20 20 20 20 20
Pearson Correlation ,000 ,000 1 -,086 ,080 ,591**
Time Sig. (2-tailed) 1,000 1,000 ,719 ,738 ,006
N 20 20 20 20 20 20
Pearson Correlation ,467* ,114 -,086 1 -,200 ,271
TBA Sig. (2-tailed) ,038 ,633 ,719 ,397 ,248
N 20 20 20 20 20 20
Pearson Correlation -,027 ,048 ,080 -,200 1 ,302
FFA Sig. (2-tailed) ,909 ,842 ,738 ,397 ,196
N 20 20 20 20 20 20
Pearson Correlation ,521* ,305 ,591** ,271 ,302 1

PV Sig. (2-tailed) ,018 ,191 ,006 ,248 ,196

N 20 20 20 20 20 20

*. Correlation is significant at the 0.05 level (2-tailed).

**. Correlation is significant at the 0.01 level (2-tailed).
 Tests of Between-Subjects Effects

Source Dependent Variable Type III Sum of df Mean Square F Sig.

Squares

TBA 7,657a 14 ,547 1,749 ,279

Corrected Model FFA 24,739b 14 1,767 5,017 ,043

PV 44,746c 14 3,196 29,231 ,001

TBA 22,408 1 22,408 71,663 ,000
Intercept FFA 81,201 1 81,201 230,537 ,000
PV 132,308 1 132,308 1210,035 ,000
TBA 2,567 3 ,856 2,736 ,153
Temperature FFA 3,000 3 1,000 2,839 ,145
PV 16,939 3 5,646 51,640 ,000
TBA ,682 3 ,227 ,727 ,578
NaCl FFA ,988 3 ,329 ,935 ,489
PV 4,358 3 1,453 13,286 ,008
TBA 1,612 3 ,537 1,719 ,278
Time FFA 3,003 3 1,001 2,842 ,145
PV 16,680 3 5,560 50,850 ,000
TBA ,052 1 ,052 ,166 ,700
Temperature * NaCl FFA ,489 1 ,489 1,388 ,292
PV ,129 1 ,129 1,182 ,326
TBA 2,317 1 2,317 7,409 ,042
Temperature * Time FFA ,417 1 ,417 1,183 ,326
PV ,236 1 ,236 2,155 ,202
TBA ,001 1 ,001 ,002 ,964
NaCl * Time FFA ,037 1 ,037 ,104 ,760
PV ,231 1 ,231 2,111 ,206
TBA ,014 1 ,014 ,044 ,842
Temperature * NaCl * Time FFA ,206 1 ,206 ,585 ,479
PV ,013 1 ,013 ,119 ,744
TBA 1,563 5 ,313
Error FFA 1,761 5 ,352
PV ,547 5 ,109
TBA 50,978 20
Total FFA 211,685 20
PV 246,309 20
TBA 9,220 19

Corrected Total FFA 26,500 19

PV 45,293 19

a. R Squared = ,830 (Adjusted R Squared = ,356)

b. R Squared = ,934 (Adjusted R Squared = ,)
c. R Squared = ,988 (Adjusted R Squared = ,954)

————— 15/11/2018 13:58:33 ————————————————————

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Full Factorial Design

Factors: 3 Base Design: 3; 8 Resolution with blocks: IV

Runs: 20 Replicates: 1
Blocks: 2 Center pts (total): 12

Block Generators: ABC

Alias Structure

Blk = ABC

A
B
C
AB
AC
BC

Results for: Worksheet 2

Full Factorial Design

Factors: 3 Base Design: 3; 8

Runs: 14 Replicates: 1
Blocks: 1 Center pts (total): 6

All terms are free from aliasing.

Results for: Worksheet 3

Central Composite Design

Factors: 3 Replicates: 1
Base runs: 20 Total runs: 20
Base blocks: 1 Total blocks: 1

Two-level factorial: Full factorial

Cube points: 8
Center points in cube: 6
Axial points: 6
Center points in axial: 0

Alpha: 1,68179
Results for: Worksheet 4

Central Composite Design

Factors: 3 Replicates: 1
Base runs: 20 Total runs: 20
Base blocks: 1 Total blocks: 1

Two-level factorial: Full factorial

Cube points: 8
Center points in cube: 6
Axial points: 6
Center points in axial: 0

Alpha: 1,68179

Results for: Worksheet 5

Central Composite Design

Factors: 3 Replicates: 1
Base runs: 20 Total runs: 20
Base blocks: 1 Total blocks: 1

Two-level factorial: Full factorial

Cube points: 8
Center points in cube: 6
Axial points: 6
Center points in axial: 0

Alpha: 1,68179

Design Table

Run Blk A B C
1 1 -1,00000 -1,00000 -1,00000
2 1 1,00000 -1,00000 -1,00000
3 1 -1,00000 1,00000 -1,00000
4 1 1,00000 1,00000 -1,00000
5 1 -1,00000 -1,00000 1,00000
6 1 1,00000 -1,00000 1,00000
7 1 -1,00000 1,00000 1,00000
8 1 1,00000 1,00000 1,00000
9 1 -1,68179 0,00000 0,00000
10 1 1,68179 0,00000 0,00000
11 1 0,00000 -1,68179 0,00000
12 1 0,00000 1,68179 0,00000
13 1 0,00000 0,00000 -1,68179
14 1 0,00000 0,00000 1,68179
15 1 0,00000 0,00000 0,00000
16 1 0,00000 0,00000 0,00000
17 1 0,00000 0,00000 0,00000
18 1 0,00000 0,00000 0,00000
19 1 0,00000 0,00000 0,00000
20 1 0,00000 0,00000 0,00000

Response Surface Regression: y1; y2; y3 versus Temperatur; % NaCl; Waktu

Response Surface Regression: y1 versus Temperatur; % NaCl; Waktu

The analysis was done using coded units.

Estimated Regression Coefficients for y1

Term Coef SE Coef T P

Constant 1,46726 0,2342 6,264 0,000
Temperatur 0,38332 0,1554 2,467 0,033
% NaCl 0,09190 0,1554 0,591 0,567
Waktu -0,06214 0,1554 -0,400 0,698
Temperatur*Temperatur 0,11312 0,1513 0,748 0,472
% NaCl*% NaCl -0,24750 0,1513 -1,636 0,133
Waktu*Waktu 0,10252 0,1513 0,678 0,513
Temperatur*% NaCl 0,07875 0,2030 0,388 0,706
Temperatur*Waktu 0,53875 0,2030 2,653 0,024
% NaCl*Waktu -0,00875 0,2030 -0,043 0,966

S = 0,5743 R-Sq = 64,1% R-Sq(adj) = 31,9%

Analysis of Variance for y1

Source DF Seq SS Adj SS Adj MS F P

Regression 9 5,899 5,899 0,6554 1,99 0,150
Linear 3 2,175 2,175 0,7249 2,20 0,151
Square 3 1,352 1,352 0,4506 1,37 0,309
Interaction 3 2,372 2,372 0,7907 2,40 0,129
Residual Error 10 3,298 3,298 0,3298
Lack-of-Fit 5 1,746 1,746 0,3491 1,12 0,450
Pure Error 5 1,553 1,553 0,3105
Total 19 9,197

Estimated Regression Coefficients for y1 using data in uncoded units

Term Coef
Constant 1,46726
Temperatur 0,383321
% NaCl 0,0918950
Waktu -0,0621373
Temperatur*Temperatur 0,113122
% NaCl*% NaCl -0,247503
Waktu*Waktu 0,102515
Temperatur*% NaCl 0,0787500
Temperatur*Waktu 0,538750
% NaCl*Waktu -0,00875000

Response Surface Regression: y2 versus Temperatur; % NaCl; Waktu

The analysis was done using coded units.

Estimated Regression Coefficients for y2

Term Coef SE Coef T P

Constant 2,74904 0,6350 4,329 0,001
Temperatur -0,03811 0,4213 -0,090 0,930
% NaCl 0,06573 0,4213 0,156 0,879
Waktu 0,08790 0,4213 0,209 0,839
Temperatur*Temperatur 0,09542 0,4101 0,233 0,821
% NaCl*% NaCl 0,27574 0,4101 0,672 0,517
Waktu*Waktu 0,06007 0,4101 0,146 0,886
Temperatur*% NaCl -0,24750 0,5505 -0,450 0,663
Temperatur*Waktu -0,22750 0,5505 -0,413 0,688
% NaCl*Waktu 0,06750 0,5505 0,123 0,905
S = 1,557 R-Sq = 8,7% R-Sq(adj) = 0,0%

Analysis of Variance for y2

Source DF Seq SS Adj SS Adj MS F P

Regression 9 2,2983 2,2983 0,25537 0,11 0,999
Linear 3 0,1844 0,1844 0,06146 0,03 0,994
Square 3 1,1734 1,1734 0,39114 0,16 0,920
Interaction 3 0,9405 0,9405 0,31352 0,13 0,940
Residual Error 10 24,2427 24,2427 2,42427
Lack-of-Fit 5 22,4908 22,4908 4,49815 12,84 0,007
Pure Error 5 1,7519 1,7519 0,35039
Total 19 26,5411

Estimated Regression Coefficients for y2 using data in uncoded units

Term Coef
Constant 2,74904
Temperatur -0,0381106
% NaCl 0,0657344
Waktu 0,0879008
Temperatur*Temperatur 0,0954246
% NaCl*% NaCl 0,275737
Waktu*Waktu 0,0600692
Temperatur*% NaCl -0,247500
Temperatur*Waktu -0,227500
% NaCl*Waktu 0,0675000

Response Surface Regression: y3 versus Temperatur; % NaCl; Waktu

The analysis was done using coded units.

Estimated Regression Coefficients for y3

Term Coef SE Coef T P

Constant 2,2774 0,2700 8,434 0,000
Temperatur 0,9488 0,1791 5,296 0,000
% NaCl 0,5555 0,1791 3,101 0,011
Waktu 1,0738 0,1791 5,994 0,000
Temperatur*Temperatur 0,6387 0,1744 3,662 0,004
% NaCl*% NaCl 0,2657 0,1744 1,523 0,159
Waktu*Waktu 0,4035 0,1744 2,314 0,043
Temperatur*% NaCl -0,1275 0,2341 -0,545 0,598
Temperatur*Waktu 0,1725 0,2341 0,737 0,478
% NaCl*Waktu 0,1700 0,2341 0,726 0,484

S = 0,6620 R-Sq = 90,3% R-Sq(adj) = 81,6%

Analysis of Variance for y3

Source DF Seq SS Adj SS Adj MS F P

Regression 9 40,8474 40,8474 4,5386 10,35 0,001
Linear 3 32,2543 32,2543 10,7514 24,53 0,000
Square 3 7,9938 7,9938 2,6646 6,08 0,013
Interaction 3 0,5993 0,5993 0,1998 0,46 0,719
Residual Error 10 4,3831 4,3831 0,4383
Lack-of-Fit 5 3,8364 3,8364 0,7673 7,02 0,026
Pure Error 5 0,5467 0,5467 0,1093
Total 19 45,2305
Unusual Observations for y3

Obs StdOrder y3 Fit SE Fit Residual St Resid

9 9 1,330 2,488 0,516 -1,158 -2,79 R

R denotes an observation with a large standardized residual.

Estimated Regression Coefficients for y3 using data in uncoded units

Term Coef
Constant 2,27743
Temperatur 0,948766
% NaCl 0,555462
Waktu 1,07381
Temperatur*Temperatur 0,638662
% NaCl*% NaCl 0,265663
Waktu*Waktu 0,403549
Temperatur*% NaCl -0,127500
Temperatur*Waktu 0,172500
% NaCl*Waktu 0,170000