EXPERIMENT NO:
Procedure:
Observation:
Calculation:
N2V2
i. For clear solution normality , N1=
V1
Result:
Conclusion:
EXPERIMENT NO:
CRYSTALLIZATION
Aim: To study Crystallization & find crystal yield ‘with Seeding ’ & ‘ without Seeding ’.
Apparatus: Heating Mantle, Heater, Thermometer, Weigh scale, Vacuum filter, drying apparatus.
Procedure:
Without Seeding:
With Seeding:
Observations:-
1. Room temperature -
2. Test Temperature -
3. Wt. of Crystal obtained theoretically
a) Wt. of Crystal without seeding - ______________
Calculation:-
Result:-
Conclusion:-
EXPERIMENT NO: -
MULTISTAGE LEACHING
Aim: To determine the efficiency of multistage leaching of NaOH & CaCO3 using water as solvent.
Apparatus: -Glass beakers, Magnetic stirrer, Burette, Pipette, Measuring cylinder and Conical flask.
Chemicals: 35gm CaCO3, 5gm NaOH, 0.5N HCl , water and phenolphthalein
Procedure: - .
Observation: -
Calculation:
Stage 1:
N2V2
i. For clear solution normality , N1=
V1
Stage 2:
N2V2
iv. For clear solution normality , N1=
V1
Result:
Conclusion:
EXPERIMENT NO:
Aim:-To determine the performance of single stage extraction of acetic acid and water mix with ethyl
acetic as solvent at room temperature.
Apparatus:-Measuring cylinder, Separating funnel, Magnetic stirrer, Conical flask, Burette stand,
Weight box etc.
Procedure:-
Observation:-
Calculations:-
N2V2
(1) Normality of extract , N1=
V1
NaOH recovered
(4) % Recovery of Acetic Acid =
NaOH in feed
Conclusion: