V.

PERHITUNGAN

a. Sample /Result Table Alat

No Nama Absorbansi (X) Konsentrasi(ppm)(Y)

1 Standar 2,19830 19,84100
2 Panadol 1 2,11290 19,07000
3 Panadol 2 2,12360 19,16600
4 Paramex 1 2,43540 21,98100
5 Paramex 2 2,44290 22,04800
6 Bodrex 1 1,30950 11,81900
7 Bodrex 2 1,30850 11,81000

b. Sample /Result Table Excel

No Nama Absorbansi (X) Konsentrasi(ppm)(Y)

1 Standar 2,19830 19,84062
2 Panadol 1 2,11290 19,06986
3 Panadol 2 2,12360 19,16643
4 Paramex 1 2,43540 21,98052
5 Paramex 2 2,44290 22,04821
6 Bodrex 1 1,30950 11,81893
7 Bodrex 2 1,30850 11,80991

c. Sample/ Result Table Alat

No Nama Absorbansi (X) Konsentrasi(ppm)(Y)

1 Standar 2,19830 19,84100
2 Panadol 1 2,11290 19,07000
3 Panadol 2 2,12360 19,16600
4 Paramex 1 2,43540 21,98100
5 Paramex 2 2,44290 22,04800
6 Bodrex 1 1,30950 11,81900
7 Bodrex 2 1,30850 11,81000
 1. PERHITUNGAN PEMBUATAN LARUTAN
a. Membuat Standar NaOH 0,1 N dalam 1000 ml

Gr = M x V x BM

Gr = 0,1 mol/L x 1 L x 40 gr/mol

Gr = 4 gr

b. Perhitungan Berat Sampel

𝑉𝑜𝑙𝑢𝑚𝑒 𝐴𝑞𝑢𝑎𝑑𝑒𝑠𝑡
𝐺𝑟 = 𝐵𝑒𝑟𝑎𝑡 𝐾𝑒𝑠𝑒𝑙𝑢𝑟𝑢ℎ𝑎𝑛 x Berat rata rata sampel

1. Paramex
50
𝐺𝑟 = 250 x 0,7520 = 0,1504 gr
2. Panadol
50
𝐺𝑟 = 500 x 0,6511 = 0,06511 gr
3. Bodrex
50
𝐺𝑟 = 600 x 0,8272 = 0,0689 gr

c. Menghitung ppm sampel yang sudah diencerkan

Diketahui =

Massa parasetamol = 50 mg

Volume aquadest = 50 ml

Ditanya =

M2 = ?

Dijawab =

50 mg
𝑝𝑝𝑚 =
50 ml aquadest

50 mg x 20
𝑝𝑝𝑚 =
50 ml aquadest x 20
1000 mg
𝑝𝑝𝑚 = 1000 ml
= 1000 mg /L
V1 xM1 = V2 x M2

1 ml x 1000 ppm = 50 ml x M2

M2 = 20 ppm

2. Menghitung Konsentrasi Parasetamol dalam Masing – Masing Sampel

Menggunakan Kurva secara Excel
 Standar
y = 9,0253X - 0,0003
y = (9,0253 x 2,19830) - 0,0003
y = 19,84062 ppm

 Panadol 1
y = 9,0253X - 0,0003
y = (9,0253 x 2,11290) - 0,0003
y = 19,06955637 ppm

 Panadol 2
y = 9,0253X - 0,0003
y = (9,0253 x 2,12360) - 0,0003
y = 19,16643 ppm

 Paramex 1
y = 9,0253X - 0,0003
y = (9,0253 x 2,43540) - 0,0003
y = 21,98052 ppm

 Paramex 2
y = 9,0253X - 0,0003
y = (9,0253 x 2,44290) - 0,0003
y = 22,04821 ppm

 Bodrex 1
y = 9,0253X - 0,0003
y = (9,0253 x 1,30950 ) - 0,0003
 y = 11,81893 ppm

 Bodrex 2
y = 9,0253X - 0,0003
y = (9,0253 x 1,30850) - 0,0003
y = 11,80991 ppm

Grafik Sample/ Result Table Alat

25.00000
y = 9.0253x + 0.0003
20.00000 R² = 1
Konsentrasi (ppm)

15.00000
Konsentrasi(ppm)(Y)
10.00000
Linear
5.00000 (Konsentrasi(ppm)(Y))

0.00000
0.00000 1.00000 2.00000 3.00000
Absorbansi (257 nm)
DATA PENGAMATAN

1. Calibration Table Secara Excel

No Nama Konsentrasi (X) Absorbansi(Y)

1 Standar 1 100 0,08813
2 Standar 2 200 0,17602
3 Standar 3 300 0,30686
4 Standar 4 400 0,34126
5 Standar 5 500 0,42071
6 Standar 6 600 0,49843

2. Menghitung Konsentrasi Cu dalam Sampel Menggunakan Grafik pada MS.

Excel
1. Standar 1
y = 0,0008X - 0,0232
0,08813 = 0,0008X - 0,0232
0,08813−0,0232
X = 0,0008

= 81,1625 ppm

2. Standar 2
y = 0,0008X - 0,0232
0,1760 = 0,0008X - 0,0232
0,1760−0,0232
X = 0,0008

= 191,025 ppm

3. Standar 3
y = 0,0008X - 0,0232
0,30686 = 0,0008X - 0,0232
0,30686−0,0232
X = 0,0008

= 354,575 ppm

4. Standar 4
y = 0,0008X - 0,0232
0,34126 = 0,0008X - 0,0232
 0,34126−0,0232
X = 0,0008

= 397,575` ppm

5. Standar 5
y = 0,0008X - 0,0232
0,42071 = 0,0008X - 0,0232
0,42071−0,0232
X = 0,0008

= 496,8875ppm

6. Standar 6
y = 0,0008X - 0,0232
0,49843 = 0,0008X - 0,0232
0,49843−0,0232
X = 0,0008

= 594,0375ppm

3. Calibration Curve Secara Excel

Calibration Curve
0.6
y = 0.0008x + 0.0232
0.5 R² = 0.9811
Absorbansi (604 nm)

0.4

0.3
Absorbansi(Y)
0.2 Linear (Absorbansi(Y))

0.1

0
0 200 400 600 800
Konsentrasi (ppm)