March 1, 2012
Edtorial Revision September 13, 2013
1.1 This standard contains performance requirements D 16 Standard Terminology for Paint, Related
for a high-performance, single-component, moisture-curing Coatings, Materials, and Applications
UV-stable polyurethane topcoat (ASTM D 16, Type II polyure- D 523 Standard Test Method for Specular
thane) for use on steel substrates. The coating is intended to be Gloss
used as a topcoat that provides good color and gloss retention. * D 562 Standard Test Method for Consis-
tency of Paints Measuring Krebs Units
1.2 Coatings meeting the requirements of this standard (KU) Viscosity Using the Stormer-Type
are generally suitable for exposures in SSPC Environmental Viscometer
Zones 1A (interior, normally dry), 1B (exterior, normally dry), D 1014 Standard Practice for Conducting Exte-
2A (frequently wet by fresh water, excluding immersion), 2B rior Exposure Tests of Paints and
(frequently wet by salt water, excluding immersion), 3B (chem- Coatings on Metal Substrates
ical exposure, neutral) and 3C (chemical exposure, alkaline)1. * D 1296 Standard Test Method for Odor of Vola-
tile Solvents and Diluents
1.3 The coating is intended for application by brush, spray, * D 1475 Standard Test Method for Density of
or roller over a primer or intermediate coating. Liquid Coatings, Inks, and Related
Products
2. Description * D 1535 Standard Practice for Specifying Color
by the Munsell System
2.1 This single-package moisture-curing polyurethane * D 1640 Standard Test Methods for Drying,
coating is characterized by the presence of free polyisocyanate Curing, or Film Formation of Organic
groups capable of reacting with atmospheric moisture in order Coatings at Room Temperature
to form a film. D 2244 Standard Test Method for Calculation of
Color Tolerances and Color Differences
2.2 WEATHERING LEVELS: This standard contains three From Instrumentally Measured Color
levels of accelerated (A) and South Florida weathering (SF) Coordinates
performance described in Section 7.2. * D 2369 Standard Test Method for Volatile
Content of Coatings
3. Referenced Standards * D 2371 Standard Test Method for Pigment
Content of Solvent-Reducible Paints
3.1 The latest issue, revision, or amendment of the refer- * D 2621 Standard Test Method for Infrared
enced standards in effect on the date of invitation to bid shall Identification of Vehicle Solids from
govern, unless otherwise specified. Standards marked with Solvent-Reducible Paints
an asterisk (*) are referenced only in the Notes, which are not * D 2697 Standard Test Method for Volume
requirements of this standard. Nonvolatile Matter in Clear or Pigmented
Coatings
3.2 If there is a conflict between the requirements of any of D 2794 Standard Test Method for Resistance of
the cited referenced standards and this standard, the require- Organic Coatings to the Effects of Rapid
ments of this standard shall prevail. Deformation (Impact)
D 4214 Standard Test Methods for Evaluating
3.3 SSPC STANDARD: Degree of Chalking of Exterior Paint
Films
Guide 13 Guide for the Identification and Use of
Industrial Coating Materials in Comput- 2
ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA
erized Product Databases 19428-2959. For referenced ASTM standards, visit the ASTM website,
www.astm.org, or contact ASTM Customer Service at service@astm.
org. For Annual Book of ASTM Standards volume information, refer to
1
SSPC Environmental Zones are defined in “About SSPC Standards the standard’s Document Summary page on the ASTM website.
and Guides” available online from <http://www.sspc.org>.
1
SSPC-Paint 38
March 1, 2012
Editorial Revision September 13, 2013
D 4541 Standard Test Method for Pull-Off 5.2 APPLICATION PROPERTIES: All guidance provided by
Strength of Coatings Using Portable the manufacturer regarding thinning requirements and special
Adhesion Testers application requirements shall be followed (see Note 11.3). The
D 4587 Standard Practice for Fluorescent coating shall be easily applied by brush, roller, or spray in accor-
UV-Condensation Exposures of Paint dance with the manufacturer’s written instructions. The coating
and Related Coatings shall have no streaking, running, or sagging or other defects
D 5402 Standard Practice for Assessing the during application or while drying.
Solvent Resistance of Organic Coatings
Using Solvent Rubs 6. Test Panel Preparation
G 154 Standard Practice for Operating Fluores-
cent Light Apparatus for UV Exposure of Triplicate test panels shall be prepared for each test. Prior
Nonmetallic Materials to application of the topcoat to be tested, a compatible primer
and intermediate coat recommended by the manufacturer of the
3.5 AMERICAN NATIONAL STANDARDS INSTITUTE topcoat to be tested shall be applied to the panels and cured
(ANSI) STANDARD:3 in accordance with the manufacturer’s written instructions. The
topcoat to be tested shall be applied according to the manufac-
Z129.1 Hazardous Industrial Chemicals – turer’s written recommendations.
Precautionary Labeling
7. Weathering Requirements
3.6 AMERICAN ASSOCIATION OF STATE HIGHWAY AND
TRANSPORTATION OFFICIALS (AASHTO) STANDARD:4
7.1 WEATHERING RESISTANCE: Two weathering test
procedures are defined below. Performance levels are estab-
TP 67-03 Standard Method of Test for Analysis of
lished using whites and light colors. It is left to the discretion of
Structural Steel Coatings for Isocyanate
the specifier whether to accept Florida data from a similar color
Content
or to use UV-A data in lieu of South Florida weathering data.
[NOTE: Commercial test sites in North America conforming to
4. Composition Requirements
this requirement are located in southern Florida and Arizona.]
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TABLE 3
SUMMARY OF PERFORMANCE TESTING RESULTS FOR COLOR AND GLOSS RETENTION
Procedure –Test according to ASTM D 4587 Cycle 2 according to ASTM D 523. Table 3 summarizes the tests of
procedure. This eight-hour duration comprises one test cycle. Section 7 as well as the minimum acceptance criteria. See Note
Continue cycle testing to achieve the exposure hours defined in 11.4 regarding test results for darker colors.
the required performance levels (as shown in Table 1).
8. Laboratory Physical Tests of Applied Coatings
Smaller values of color change (less than 3.0 ∆E*) may be
visible, but the noticeable change maximum of 3.0 ∆E* required 8.1 RECOATABILITY: Intercoat and substrate adhesion
by this standard is acceptable for most industrial and marine properties of the polyurethane topcoats shall be determined by
applications. The specifier has the option to require more strin- measurement of adhesion values between:
gent gloss and color retention. a) primer and the substrate,
b) polyurethane topcoat and the primer or intermediate
7.1.2 South Florida Weathering: South Florida weath- coat, and, if applicable
ering shall be performed in accordance with ASTM D 1014 (45˚ c) the second coat of polyurethane topcoat and the same
south exposure, washed with mild detergent before readings previously applied topcoat.
are taken). Coating manufacturers shall provide acceptable window (time
frame) ranges between applications of coats in a multi-coat
7.2 Performance Levels: Tables 1 and 2 specify the system. Unless the purchaser specifically requests a variance,
amount of time the coating must perform before noticeable the maximum dry film thickness and the minimum curing time
change in order to achieve the defined performance level. (with reported conditions for temperature and humidity) as
Polyurethane topcoats are available in a wide range of color stated on the manufacturer’s product data sheets will be used
and gloss. Procurement documents shall state the desired for coating application prior to adhesion testing. All testing shall
level of performance, exposure method (in accordance with be performed on a minimum of three steel test panels each with
Tables 1 and 2), color, and gloss. For example, a specifier may minimum dimensions of 75 x 150 x 6 mm (3 x 6 x ¼ inches). The
require Level 2SF Florida exposure, initial gloss greater than panels shall be prepared to the minimum surface preparation
80, matched to a specific color. A certain level of accelerated recommendations of the coating manufacturer.
weathering does not necessarily correspond to a particular level
of atmospheric weathering and they need to be specified inde- 8.2 ADHESION
pendently. These are two independent complementary tests for
measuring coating performance. If no level is specified, either 8.2.1 Primer Adhesion to Steel Substrate: Apply the
Accelerated Level 3 or South Florida Level 3 data is acceptable. primer to the steel panel and cure according to the manufac-
The coating manufacturer shall report the type of testing used to turer’s recommendations. Test adhesion according to ASTM D
generate the data. 4541 and identify the type of adhesion tester used (Type II, III,
IV, or V). The minimum adhesion acceptance value of the primer
7.2.1 Each replicate panel must meet the minimum accep- to the substrate shall be 4.1 MPa (or 600 psi in U.S. units).
tance criteria. Clear coatings must be tested over the intended
basecoat. Initially, and at the end of the exposure period for 8.2.2 Polyurethane Topcoat Adhesion to the Primer:
each level, tristimulus color values shall be measured according Apply topcoat to panels (previously primed as described in 8.2.1)
to ASTM D 2244, and 60 degree gloss shall be measured and cure according to the manufacturer’s recommendations.
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TABLE 4
ADDITIONAL REQUIRED PERFORMANCE PROPERTIES
MINIMUM
TEST ASTM METHOD RESULT (UNITS) ACCEPTABLE VALUE
Adhesion (to substrate,
primer, intermediate coat, or
D 4541 MPa (psi) 4.1 (600)
previously applied topcoat)
(Section 8.2 and subsections)
kg-force per square
Direct Impact Resistance
D 2794 centimeter 4.2 (60)
(Section 8.4)
(lb-force per square inch)
Solvent (MEK) Resistance 4 sets of 25 with no
D 5402 Number of double-rubs
(Section 8.5) topcoat visible on cloth
Evaluating degree of chalking Photographic stan-
D 4214 6, where 10 is no chalking*
in exterior paints (Section 8.6) dard rating method
* At desired weathering level.
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However, many state and local governments and/or air quality material. The pass/fail criterion is that the measurement of the
management areas have more stringent VOC regulations than test sample shall fall within two standard deviations of the target
those in the federal rule. In the U.S., information on the VOC value. The contracting parties must agree on a target value.
content of each container before mixing or thinning is found
on the container label and in the manufacturer’s safety data 11.2.2 Quality Assurance Testing Procedures: Quality
sheet. The coating manufacturer’s product data sheet usually assurance tests include but are not limited to: infrared analysis
provides information on the total VOC content of a coating after (ASTM D 2621), viscosity (ASTM D 562), weight per gallon
mixing and any recommended thinning. (ASTM D 1475), total solids (ASTM D 2369), volume solids
(ASTM D 2697), dry time (ASTM D 1640), percent pigment
11.2 QUALITY ASSURANCE TESTS: Quality assurance (ASTM D 2371), gloss (ASTM D 523), color (ASTM D 1535,
tests are used to determine whether the supplied products are ASTM D 2244), odor (ASTM D 1296), and isocyanate content
of the same type and quality as those originally tested. The (AASHTO TP 67-03).
selected tests should rapidly and accurately measure the phys-
ical and chemical characteristics of the coating necessary to 11.3 These coatings may be susceptible to pinholing if
verify that the supplied material is substantially the same as the applied under adverse conditions such as high humidity. The
previously accepted material. All of the quality assurance tests degree of pinholing depends on formulation variables. Consult
must be performed on the originally submitted qualification the coating manufacturer’s recommendations for formulation
sample. The results of these tests are used to establish pass/ additives that may be used to address this problem.
fail criteria for quality assurance testing of supplied products.
11.4 Test results for color and gloss of deeper colors (i.e.,
11.2.1 Establishing Quality Assurance Acceptance having a Munsell value below 9) will vary significantly due to
Criteria: Many ASTM test methods contain precision and bias differences in pigment weathering properties, and may not
statements. Specification developers should be cognizant of the meet the requirements of Section 7 without use of additional
fact that these statements exist. Quality assurance test criteria procedures such as clear coating. Alternatively, the specifier
should not be more stringent than the interlaboratory precision may accept a greater change in gloss and color for deeper
of the test methods used. The specifier may require additional colors.
technical data to satisfy QA or local regulatory requirements.
Where precision and bias data are not available for a given The coating manufacturer should be contacted if the
test method, determine the standard deviation of a minimum of user desires color change of less than 2.0 ∆E* for a specific
five measurements taken on the originally tested and certified application. In order to achieve this requirement, additional
procedures such as clear coating may be needed.
Copyright ©
SSPC standards, guides, and technical reports are copyrighted
world-wide by SSPC: The Society for Protective Coatings. Any
photocopying, re-selling, or redistribution of these standards,
guides, and technical reports by printed, electronic, or any other
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of SSPC: The Society of Protective Coatings and a formal
licensing agreement.