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PPM (x) ABS (y)

25 0.343 1. Membuat larutan As. Salisilat 350 ppm/ 100 ml


30 0.412
35 0.481 350 ppm = 350mg*100mL
40 0.547 = 1000ml
= 35 mg
45 0.617 BK+zat = 0,3166 g
50 0.668 Bk+sisa = 0,2810 g -
zat = 0,0356 g
A 0.017190 = 35,6 mg/100mL
B 0.013177
R 0.999086
2. Koreksi Kadar
kadar = B. penimbangan x ppm
B. perhitungan
= 35,6 x 350
35
= 356 ppm
X (Ppm) Y (abs) Y' Y-Y' (Y-Y')2
25 0.343 0.346619 -0.003619 0.00001309750566893
30 0.412 0.412505 -0.000505 0.00000025478458050
35 0.481 0.478390 0.002610 0.00000680961451247
40 0.547 0.544276 0.002724 0.00000741913832200
45 0.617 0.610162 0.006838 0.00004675954648526
50 0.668 0.676048 -0.008048 0.00006476417233560

A 0.017190 TOTAL 0.00013910476190476


B 0.013177 SY/X 0.00589713409006363
R 0.999086 LOD 1.47684082264169000
LOQ 4.47527522012634000 2%
X (Ppm) Y(Abs) KONSENTRASI
REPLIKASI ABS KONSENTRASISEBENARNYA
25 0.343 1 0.345 24.8771321191 25
30 0.412 80% 2 0.342 24.6494651633 25
35 0.481 3 0.344 24.8012431339 25
40 0.547 1 0.398 28.8992483377 30
45 0.617 100% 2 0.41 29.8099161607 30
50 0.668 3 0.399 28.9751373229 30
1 0.479 35.0462561434 35
120% 2 0.481 35.1980341139 35
A 0.017190 3 0.483 35.3498120844 35
B 0.013177
R 0.999086
%
100%
99%
99% 99.10% syarat : 98-102%
96%
99%
97% 97.43% 99.03%
100%
101%
101% 100.57%
X (Ppm) Y(Abs) REPLIKASI ABS KONSENTRASI
25 0.343 1 0.479 35.046
30 0.412 2 0.483 35.350 35 PPM
35 0.481 3 0.485 35.502
40 0.547 4 0.486 35.577
45 0.617 5 0.477 34.894
50 0.668 6 0.476 34.819
SD 0.322
A 0.017190 RATA-RATA 35.198
B 0.013177 CV 0.0091
R 0.999086
RSD 0.915% syarat = < 2%