BAB IV

PERHITUNGAN NERACA MASSA

Kapasitas Produksi : 30.000 ton/tahun

Operasi Pabrik : 300 hari/tahun
Basis : 1 jam operasi
Satuan Massa : Kg (kilogram)
Bahan Baku : Etilen oksida dan Amonia
Produk Utama : Trietanolamina (C6H15NO3)
4.1. NERACA MASSA
4.1.1. Neraca Massa Mixing Point-01 (MP-01)
Input Output
Komponen Aliran 1 Aliran 12 Aliran 2
Kg Kg Kg
Etilen Oksida 0,0000 0,0000 0,0000
Amonia 9.272,4941 10.619,8059 19.892,3001
Air 15,9266 0,0000 15,9266
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
9.288,4207 10.619,8059 19.908,2266
Total
19.908,2266 19.908,2266
4.1.2. Neraca Massa Heater-01 (H-01)
Input Output
Komponen Aliran 2 Aliran 3
Kg Kg
Etilen Oksida 0,0000 0,0000
Amonia 19.892,3001 19.892,3001
Air 15,9266 15,9266
Monoetanolamina 0,0000 0,0000
Dietanolamina 0,0000 0,0000
Trietanolamina 0,0000 0,0000
Total 19.908,2266 19.908,2266

4.1.3. Neraca Massa Mixing Point-02 (MP-02)

Input Output
Komponen Aliran 3 Aliran 4 Aliran 5
Kg Kg Kg
Etilen Oksida 0,0000 19.157,7547 19.157,7547
Amonia 19.908,2266 0,0000 19.908,2266
Air 15,9266 191,5775 207,5041
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
19.924,1532 19.349,3322 39.273,4855
Total
39.273,4855 39.273,4855
4.1.4. Neraca Massa Reaktor-01 (R-01)
Input Output
Komponen Aliran 5 Aliran 6
Kg Kg
Etilen Oksida 19.157,7547 193,4742
Amonia 19.908,2266 15.301,0786
Air 207,5041 207,5041
Monoetanolamina 0,0000 7.755,0000
Dietanolamina 0,0000 13.341,4286
Trietanolamina 0,0000 2.475,0000
39.273,4855 39.273,4855
Total
39.273,4855 39.273,4855

4.1.5. Neraca Massa Stripper-01 (ST-01)

Input Output
Aliran 7 Aliran 8
Komponen Aliran 6
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 193,4742 23,5613 169,9128
Ammonia 15.301,0786 6.528,0732 8.773,0054
Air 207,5041 0,7323 206,7718
Monoetanolamina 7755,0000 0,6182 7754,3818
Dietanolamina 13.341,4286 0,0020 13.341,4266
Trietanolamina 2475,0000 0,0000 2475,0000
6.552,9871 32.720,4984
Total 39.273,4855
39.273,4855
4.1.6. Neraca Massa Reboiler-01 (RB-01)
Input Output
Aliran 9 Aliran 10
Komponen Aliran 8
Top Produk Bottom Produk
(kg)
(Kg) (Kg)
Etilen Oksida 169,9128 24,5391 145,3737
Ammonia 8.773,0054 4.091,7327 4.681,2727
Air 206,7718 1,0939 205,6779
Monoetanolamina 7754,3818 1,1542 7753,2276
Dietanolamina 13.341,4266 0,0052 13.341,4213
Trietanolamina 2475,0000 0,0000 2475,0000
4.118,5252 28.601,9732
Total 32.720,4984
32.720,4984

4.1.7. Neraca Massa Condenser-01 (CD-01)

Input Output
Aliran L Aliran 11 (D)
Komponen Aliran 7
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 10.696,9645 77,1585 10.619,8059
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
77,1585 10.619,8059
Total 10.696,9645
10.696,9645
4.1.8. Neraca Massa Accumulator-01 (ACC-01)
Input Output
Komponen Aliran 11 Aliran L Aliran 12 (D)
(Kg) (Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 10.696,9645 77,1585 10.619,8059
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
77,1585 10.619,8059
Total 10.696,9645
10.696,9645

4.1.9. Neraca Massa Mixing Point-03 (MP-03)

Input Output
Komponen Aliran 10 Aliran 24 Aliran 13
Kg Kg Kg
Etilen Oksida 193,4742 31,0587 224,5329
Amonia 4.681,2727 3.741,7767 8.423,0494
Air 207,5041 7.461,4759 7.668,9800
Monoetanolamina 7.755,0000 961,6667 8.671,6667
Dietanolamina 13.341,4286 1.100,0000 14.441,4286
Trietanolamina 2.475,0000 1.650,0000 4.125,0000
14.900,9780 28.653,6795 43.554,6575
Total
43.554,6575 43.554,6575
4.1.10. Neraca Massa Stripper-02 (ST-02)
Input Output
Aliran 14 Aliran 15
Komponen Aliran 13
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 224,5329 39,1756 185,3573
Ammonia 8.423,0494 4.363,3988 4.059,6506
Air 7.668,9800 56,5352 7.612,4448
Monoetanolamina 8.671,6667 2,0133 8.669,6534
Dietanolamina 14.441,4286 0,0105 14.441,4181
Trietanolamina 4125,0000 0,0001 4124,9999
4.461,1334 39.093,5241
Total 43.554,6575
43.554,6575

4.1.11. Neraca Massa Reboiler-02 (RB-02)

Input Output
Aliran 16 Aliran 17
Komponen Aliran 15
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 185,3573 0,0069 185,3504
Ammonia 4.059,6506 0,6411 4.059,0095
Air 7.612,4448 0,0379 7.612,4069
Monoetanolamina 8.669,6534 0,0046 8.669,6488
Dietanolamina 14.441,4181 0,0002 14.441,4179
Trietanolamina 4124,9999 0,0000 4124,9999
0,6907 39.092,8334
Total 39.093,5241
39.093,5241
4.1.12. Neraca Massa Condenser-02 (CD-02)
Input Output
Aliran L Aliran 18 (D)
Komponen Aliran 14
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 4.373,7293 9,6547 4.364,0746
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
4.373,7293 9,6547 4.364,0746
Total
4.373,7293

4.1.13. Neraca Massa Accumulator-02 (ACC-02)

Input Output
Komponen Aliran 18 Aliran L Aliran 19 (D)
(Kg) (Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 4.373,7293 9,6547 4.364,0746
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
4.373,7293 9,6547 4.364,0746
Total
4.373,7293
4.1.14. Neraca Massa Mixing Tank-01 (MT-01)
Input Output
Komponen Aliran 19 Aliran 20 Aliran 21
Kg Kg Kg
Etilen Oksida 0,0000 0,0000 0,0000
Amonia 4.364,0746 0,0000 4.364,0746
Air 0,0000 7.430,7216 7.430,7216
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
4.364,0746 7.430,7216 11.794,7962
Total
11.794,7962 11.794,7962

4.1.15. Neraca Massa Mixing Point-04 (MP-04)

Input Output
Komponen Aliran 21 Aliran 22 Aliran 23
Kg Kg Kg
Etilen Oksida 0,0000 3.075,4275 3.075,4275
Amonia 4.364,0746 0,0000 4.364,0746
Air 7.430,7216 30,7543 7.461,4759
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 0,0000 0,0000 0,0000
Trietanolamina 0,0000 0,0000 0,0000
11.794,7962 3.106,1818 14.900,9780
Total
43.554,6575 14.900,9780
4.1.16. Neraca Massa Reaktor-02 (R-02)
Input Output
Komponen Aliran 23 Aliran 24
Kg Kg
Etilen Oksida 3.075,4275 31,0587
Amonia 4.364,0746 3.741,7767
Air 7.461,4759 7.461,4759
Monoetanolamina 0,0000 916,6667
Dietanolamina 0,0000 1100,0000
Trietanolamina 0,0000 1.650,0000
14.900,9780 14.900,9780
Total
14.900,9780 14.900,9780

4.1.17. Neraca Massa Evaporator-01 (EV-01)

Input Output
Komponen Aliran 17 Aliran 25 (kg) Aliran 26 (kg)
(kg) (Top Product) (Bottom Product)
Etilen Oksida 224,5329 224,5329 0,0000
Ammonia 4.059,0095 4.059,0095 0,0000
Air 7.668,9800 7.661,3100 7,6690
Monoetanolamina 8.671,6667 0,0000 8.671,6667
Dietanolamina 14.441,4286 0,0000 14.441,4286
Trietanolamina 4125,0000 0,0000 4.125,0000
11.944,8534 27.245,7642
Total 39.190,6176
39.190,6176
4.1.18. Neraca Massa Kolom Destilasi-01 (KD-01)
Input Output
Komponen Aliran 26 Aliran 27 (kg) Aliran 28 (kg)
(kg) (Top Product) (Bottom Product)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 7,6690 7,6690 0,0000
Monoetanolamina 8.671,6667 8.662,9950 8,6717
Dietanolamina 14.441,4286 14,4414 14.426,9871
Trietanolamina 4125,0000 0,0002 4.124,9998
8.685,1056 18.560,6586
Total 27.245,7642
27.245,7642

4.1.19. Neraca Massa Condenser-03 (CD-03)

Input Output
Aliran L Aliran 29 (D)
Komponen Aliran 27
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 7,6710 0,0020 7,6690
Monoetanolamina 8.665,2567 2,2617 8.662,9950
Dietanolamina 14,4452 0,0038 14,4414
Trietanolamina 0,0002 0,0000 0,0002
8.687,3731 2,2675 8.685,1056
Total
8.687,3731
4.1.20. Neraca Massa Accumulator-03 (ACC-03)
Input Output
Komponen Aliran 29 Aliran 30 (L) Aliran 31 (D)
(Kg) (Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 7,6710 0,0020 7,6690
Monoetanolamina 8.665,2567 2,2617 8.662,9950
Dietanolamina 14,4452 0,0038 14,4414
Trietanolamina 0,0002 0,0000 0,0002
8.687,3731 2,2675 8.685,1056
Total
8.687,3731

4.1.21. Neraca Massa Cooler-01 (C-01)

Input Output
Komponen Aliran 31 Aliran 32
Kg Kg
Etilen Oksida 0,0000 0,0000
Amonia 0,0000 0,0000
Air 7,6690 7,6690
Monoetanolamina 8.662,9950 8.662,9950
Dietanolamina 14,4414 14,4414
Trietanolamina 0,0002 0,0002
Total 8.685,1056 8.685,1056
4.1.22. Neraca Massa Reboiler-03 (RB-03)
Input Output
Aliran 32 Aliran 34
Komponen Aliran 28
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 16,1558 7,4841 8,6717
Dietanolamina 26.878,3098 12.451,3227 14.426,9871
Trietanolamina 7.685,1127 3.560,1129 4.124,9998
16.018,9197 18.560,6586
Total 34.579,5783
34.579,5783

4.1.23. Neraca Massa Kolom Destilasi-02 (KD-02)

Input Output
Komponen Aliran 26 Aliran 27 (kg) Aliran 28 (kg)
(kg) (Top Product) (Bottom Product)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 8,6717 0,0000 0,0000
Monoetanolamina 8,6717 8,6617 0,0000
Dietanolamina 14.442,9871 14.282,7173 144,2699
Trietanolamina 4125,9998 0,4125 4.124,5873
14.291,8014 4.268,8571
Total 18.560,6586
18.560,6586
4.1.24. Neraca Massa Condenser-04 (CD-04)
Input Output
Aliran L Aliran 37 (D)
Komponen Aliran 35
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 9,4521 0,7805 8,6717
Dietanolamina 15.568,1730 1.285,4557 14.282,7173
Trietanolamina 0,4496 0,0371 0,4125
1.286,2733 14.291,8014
Total 15.578,0747
15.578,0747

4.1.25. Neraca Massa Accumulator-04 (ACC-04)

Input Output
Komponen Aliran 37 Aliran 38 (L) Aliran 39 (D)
(Kg) (Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 9,4521 0,7805 8,6717
Dietanolamina 15.568,1730 1.285,4557 14.282,7173
Trietanolamina 0,4496 0,0371 0,4125
1.286,2733 14.291,8014
Total 15.578,0747
15.578,0747
4.1.26. Neraca Massa Cooler-02 (C-02)
Input Output
Komponen Aliran 39 Aliran 40
Kg Kg
Etilen Oksida 0,0000 0,0000
Amonia 0,0000 0,0000
Air 0,0000 0,0000
Monoetanolamina 8,6717 8,6717
Dietanolamina 14.282,7173 14.282,7173
Trietanolamina 0,4125 0,4125
Total 14.291,8014 14.291,8014

4.1.27. Neraca Massa Reboiler-04 (RB-04)

Input Output
Aliran 41 Aliran 42
Komponen Aliran 36
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 881,2140 736,9442 144,2699
Trietanolamina 25.193,3694 21.068,7821 4.124,5873
21.805,7263 4.268,8571
Total 26.074,5834
26.074,5834
4.1.28. Neraca Massa Kolom Destilasi-03 (KD-03)
Input Output
Komponen Aliran 42 Aliran 43 (kg) Aliran 44 (kg)
(kg) (Top Product) (Bottom Product)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 144,2699 97,6032 46,6667
Trietanolamina 4.124,5873 4,5873 4.120,0000
102,1904 4.166,6667
Total 4.268,8571
4.268,8571

4.1.29. Neraca Massa Condenser-05 (CD-05)

Input Output
Aliran L Aliran 45 (D)
Komponen Aliran 43
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 303,4587 205,8556 97,6032
Trietanolamina 14,2623 9,6751 4,5873
215,5306 102,1904
Total 317,7211
317,7211
4.1.30. Neraca Massa Accumulator-05 (ACC-05)
Input Output
Komponen Aliran 45 Aliran 46 (L) Aliran 47 (D)
(Kg) (Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 303,4587 205,8556 97,6032
Trietanolamina 14,2623 9,6751 4,5873
215,5306 102,1904
Total 317,7211
317,7211

4.1.31. Neraca Massa Reboiler-05 (RB-05)

Input Output
Aliran 48 Aliran 49
Komponen Aliran 44
Top Produk Bottom Produk
(Kg)
(Kg) (Kg)
Etilen Oksida 0,0000 0,0000 0,0000
Ammonia 0,0000 0,0000 0,0000
Air 0,0000 0,0000 0,0000
Monoetanolamina 0,0000 0,0000 0,0000
Dietanolamina 51,6259 4,9592 46,6667
Trietanolamina 4.557,8278 437,8278 4.120,0000
442,7870 4.166,6667
Total 4.609,4537
4.609,4537
4.1.32. Neraca Massa Cooler-03 (C-03)
Input Output
Komponen Aliran 49 Aliran 50
Kg Kg
Etilen Oksida 0,0000 0,0000
Amonia 0,0000 0,0000
Air 0,0000 0,0000
Monoetanolamina 0,0000 0,0000
Dietanolamina 46,6667 46,6667
Trietanolamina 4.120,0000 4.120,0000
Total 4.166,6667 4.166,6667