Add HNO3 batch wise Add HNO3 batch wise 2ml Sipter phd thesis Sipter phd thesis H2O2 peroxide oxidation Chen et al Abdul khaliq HNO3 : Abdul khaliq HNO3 : HNO3 : HCLO4 ( 9:1) HCLO4 (1:1) HCLO4 (1:1) Chen et al 1ML MILK: 10 ML HNO3 10 ml of analytically pure HNO3: HCLO4 (9:1) concentrated H2O2 and 20 ml of analytically pure concentrated HNO3 were added, and solutions were hold overnight; Bibi et al. Bibi et al. 1ML MILK : 10 ML Two grams of each sample H2SO4 : H2O2 (8ml : 4 H2SO4 : H2O2 (4ml : 2 HNO3 were digested with 7 ml of ml) 2:1 ml) 2:1 AFTER 5 ML HCLO4 HNO3 70% in microwave digestion system and diluted to 25 ml with deionized water Kumar et al Kumar et al 1ML MILK : 10 ML Five grams of each egg- HNO3 : HCLO4 (2:1) HNO3 : HCLO4 (2:1 HNO3 white sample was weighted AFTER 5 ML HCLO4 by a digital analytical HNO3:HCLO4 1:1 HNO3:HCLO4 1:1 10 ml milk : 5 ml HNO3 balance with ± 0.0001 g 5ml H202 precision and then was HNO3:HCLO4:H2SO4 HNO3 : HCLO4 (5:1) 1ml milk 4 ml HNO3 : 2 added to a beaker (5:1:1) ml H2O2 containing a volume of 5 0.2 G SAMPLE 1 ml milk: 10 ml HNO3 1 - ml HNO3 (65%) and 2 ml 10 ML hno3:5 ML h2SO4 2 ml HCLO4 HClO4 Hno3 : hclo4 1:1 One mL of each sample 0.01 mg sensitive weighing was placed in PTFE balance and transferred to (Teflon) vessels, then four 100 ml glass beaker. To the weighed sample, 15 ml of mL HNO3 and two mL H2 supra pure HNO3 and 3 ml O2 were added of HClO4 were added and covered with the watch glass Hno3: hcl o4: h2SO4 1ml of milk : 10 ml 65% (5:1:1 ) nitric acid. :, 5 ml of per chloric acid
Solid-Phase Partitioning of Mercury in Artisanal Gold Mine Tailings From Selected Key Areas in Mindanao, Philippines, and Its Implications For Mercury Detoxification