X Y

a. A distillation column with a total condenser is separating acetone from ethanol. A distillate 0 0
X-Y X=Y
concentration of xD = 0.90 mole fraction acetone is desired. Since CMO is valid, L/V = 0.1 0.26
1.2
constant. If L/V is equal to 0.8, find the composition of the liquid leaving the fifth stage below 0.15 0.348
the total condenser. 0.2 0.417
1
b. A distillation column separating acetone and ethanol has a partial reboiler that acts as an 0.25 0.478
equilibrium contact. If the bottoms composition is xB = 0.13 mole fraction acetone and the 0.3 0.524 0.8
boilup ratio /B = 1.0, find the vapor composition leaving the second stage above the partial 0.35 0.566
reboiler. 0.4 0.605 0.6
c. The distillation column in parts a and b is separating acetone from ethanol and has xD = 0.9, xB 0.5 0.674
0.4
= 0.13, L/V = 0.8, and /B = 1.0. If the feed composition is z = 0.3 (all concentrations are mole 0.6 0.739
fraction of more volatile component), find the optimum feed plate location, total number of 0.7 0.802
0.2
stages, and required q value of the feed. Equilibrium data for acetone and ethanol at 1 atm 0.8 0.865
(Perry et al., 1963, pp. 13–4) are 0.9 0.929 0
1 1 0 0.2 0.4 0.6 0.8 1
para la pregunta a)
DATOS: componente F D B Z (supu) XD XB
Ln/Vn= 0.8 acetona 60 54 6 0.6 0.9 0.14285714
q (liquido)= 1 etanol 40 4 36 0.4 0.1 0.85714286
entonces R/(R+1)= 0.8 100 58 42
R= 4
F D B R q Ln Vn Vm Lm
100 58 42 4 1 232 290 290 332

m b X-Y X=Y XD Z XB LOR LOS LOA

XD 0.9 0.9 LOR 0.8 0.18
1.2
0.9 0 LOS 1.14482759 -0.02068966
1
Z 0.6 0.6 LOR 0.9 0.9
0.6 0 0.582 0.6456 0.8

0.6
XB 0.142857143 0.14285714 LOS 0.14285714 0.14285714
0.142857143 0 0.582 0.6456 0.4

X Y LOA 0.6 0.6 0.2

0.582 0.6456 0.582 0.6456
0
0 0.2 0.4 0.6 0.8 1

ETAPAS N
0.9 0.9 1.2
1° 0.85 0.9
0.85 0.86
1
2° 0.79 0.86
0.79 0.812
0.8
3° 0.72 0.812
0.72 0.756
4° 0.63 0.756 0.6
0.63 0.684
5° 0.52 0.684 0.4
0.52 0.57462069 CAMBIO
6° 0.36 0.57462069
0.2
0.36 0.39144828
7° 0.18 0.39144828
0.18 0.18537931 0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
8° 0.07 0.18537931
0.07 0.05944828 X-Y X=Y XD Z XB LOR LOS LOA N

Entonces el % de liquido en la 5° etapa es de 0.52

B) b. A distillation column separating acetone and ethanol has a partial reboiler that acts as an
equilibrium contact. If the bottoms composition is xB = 0.13 mole fraction acetone and the
boilup ratio /B = 1.0, find the vapor composition leaving the second stage above the partial
reboiler.
DATOS:
Vm/B= 1 componente F D B Z (supu) XD XB
q= 1.1 acetona 20 17.4 2.6 0.2 0.62589928 0.13
etanol 80 10.4 69.6 0.8 0.37410072 0.87
100 27.8 72.2 X-Y X=Y XD Z
XB LOR LOS LOA
F D B q Ln Vn Vm Lm 1.2
100 27.8 72.2 1.1 34.4 62.2 72.2 144.4
1

m b 0.8
LOR 0.553054662 0.27974277 XD 0.62589928 0.62589928 LOR 0.62589928 0.62589928
0.6
LOS 2 -0.13 0.62589928 0 0.28317778 0.43635556
0.4
X Y Z 0.2 0.2 LOS 0.13 0.13
0.2
0.283177778 0.43635556 0.2 0 0.28317778 0.43635556
0
XB 0.13 0.13 LOA 0.2 0.2 0 0.2 0.4 0.6 0.8 1
0.13 0 0.28317778 0.43635556

X-Y X=Y XD Z XB LOR LOS LOA N

ETAPA N 1.2
0.625899281 0.62589928
1° 0.42 0.62589928 1
0.42 0.51202572
2° 0.28 0.51202572
0.8
0.28 0.43459807
3° 0.21 0.43459807
0.21 0.29 CAMBIO 0.6

4° 0.12 0.29
0.12 0.11 0.4

0.2
Entonces el % de vapor en la 2° etapa es de 0.512

0
0 0.2 0.4 0.6 0.8 1
C)
c. The distillation column in parts a and b is separating acetone from ethanol and has xD = 0.9, xB
= 0.13, L/V = 0.8, and /B = 1.0. If the feed composition is z = 0.3 (all concentrations are mole
fraction of more volatile component), find the optimum feed plate location, total number of
stages, and required q value of the feed. Equilibrium data for acetone and ethanol at 1 atm
(Perry et al., 1963, pp. 13–4) are

DATOS:
Ln/Vn= 0.8 componente F D B Z XD XB X-Y X=Y XD Z XB LOR LOS LOA
entonces R/(R+1)= 0.8 acetona 30 19.8701299 10.1298701 0.3 0.9 0.13
1.2
R= 4 etanol 70 2.20779221 67.7922078 0.7 0.1 0.87
Vm/B= 1 100 22.0779221 77.9220779
1
F D B R Ln Vn Vm Lm
100 22.07792208 77.9220779 4 88.3116883 110.38961 77.9220779 155.844156 0.8

m b
0.6
LOR 0.8 0.18 XD 0.9 0.9 LOR 0.9 0.9
LOS 2 -0.13 0.9 0 0.25833333 0.38666667
0.4

X Y Z 0.3 0.3 LOS 0.13 0.13

0.258333333 0.386666667 0.3 0 0.25833333 0.38666667 0.2

XB 0.13 0.13 LOA 0.3 0.3 0

0.13 0 0.25833333 0.38666667 0 0.2 0.4 0.6 0.8 1

ETAPA N
0.9 0.9 X-Y X=Y XD Z XB
1° 0.86 0.9
LOR LOS LOA N
0.86 0.868
1.2
2° 0.809 0.868 pendiente interseccion
0.809 0.8272 LOA -2.08 0.924
1
3° 0.74 0.8272
X+
0.74 0.772
4° 0.66 0.772 0.8
X-
0.66 0.708
5° 0.56 0.708 0.6 q/(q-1) -2.08
0.56 0.628 q 0.67532468
6° 0.44 0.628 0.4
0.44 0.532
7° 0.31 0.532
0.2
0.31 0.428
8° 0.21 0.428
0
0.21 0.29 CAMBIO 0 0.2 0.4 0.6 0.8 1
9° 0.12 0.29
0.12 0.11 Posee 9 etapas
La alimentacion se encuentra el la 8° etapa
 D9. Una columna de destilación con dos alimentaciones se está separando de etanol (E) y agua a una presión de 1,0 atm.
D9. tiene
La columna A distillation column with
un condensador two feeds
de reflujo total,iscon
separating ethanoly(E)
líquido saturado unand water atparcial.
rehervidor a pressure
RSS 1ofes1.0
unaatm. X Y
líquido saturado
The column y es has
42 mol%
a totaldecondenser
etanol. Alimente 2 caudalliquid
with saturated es F2 =reflux
100 kmol
and a/ partial
h. RSS 2reboiler.
es 18% en moles
Feed 1 is a 0 0
etanol y saturated
es una mezclaliquiddeand
dosisfases que es
42 mol% 30% deFeed
ethanol. vapor. La relación
2 flow rate is de
F2 =reflujo externoFeed
100 kmol/h. es L /2Dis=181/2,
mol%y 0.019 0.17
el caudalethanol
destiladoandesisDa=two-phase
80 kmol / h.mixture
Deseamos thatuna fracción
is 30% vapor.molar del destilado
The external refluxxDratio
= 0,66 mol= 1/2, and
is L/D 0.0721 0.3891
fracción etanol y unos flow
the distillate fondosrateque
is Dse=xB80=kmol/h.
0,04 moles fraccióna etanol.
We desire distillateUsted
molepuede asumir
fraction of xDque la OCM
= 0.66 mole 0.0966 0.4375
es válido. Datos de equilibrio están en la Tabla 2-1.
fraction ethanol and a bottoms that is xB = 0.04 mole fraction ethanol. You can assume that CMO 0.1238 0.4704
a. Encuentra la caudales F1 y B.
is valid.
b. Encuentra Equilibrium
las tasas de flujodata are in Table
de líquido y vapor2-1.
en la sección media, L 'y V'. 0.1661 0.5089
a. Findy the
c. Determinar trazarflow
lasrates
líneasF1deand B.
operación. Se Ordenado. 0.2337 0.5445
b. Find
d. Encuentra the liquid
ambas and vapor
ubicaciones óptimasflowderates in the middle
alimentación (porsection,
encima delL′ and V′. parcial) y el número total de
calderín 0.2608 0.558
equilibrioc. Determine and plot the operating lines. Be neat. 0.3273 0.5826
etapas necesarias.
d. Find both Bájese de etapas
optimum feed de abajo hacia
locations (above arriba. Se Ordenado.
partial reboiler) and the total number of equilibrium 0.3965 0.6122
stages needed. Step off stages from the bottom up. Be neat. 0.5198 0.6599
0.5732 0.6841
A) 0.6763 0.7385
Comp F1 F2 F D B z1 z2 z xD xB 0.7472 0.7815
Etanol 39.3473684 18 57.3473684 52.8 4.54736842 0.42 0.18 0.29608696 0.66 0.04 0.8943 0.8943
agua 54.3368421 82 136.336842 27.2 109.136842 0.58 0.82 0.70391304 0.34 0.96 1 1
93.6842105 100 193.684211 80 113.684211
80
DATOS:
q1= 1
q2= 0.7
Ln/D= 0.5
R 0.5

B)
F1 F2 D B
93.6842105 100 80.00 113.68

Vm Lm Li Vi Ln Vn
90.00 203.68 133.684211 120 40 120.00
C) X-Y X=Y XD Z1 Z2 XB
m b LOA1 0.42 0.42 LOR LOS LOA1 LOA2 LOI
XD 0.66 0.66 LOR 0.33333333 0.44 0.42 0.65 1
0.66 0 LOS 2.26315789 -0.05052632
0.9
LOA2 -2.33333333 0.6 LOA2 0.18 0.18
Z1 0.42 0.42 LOI 1.11403509 0.11210526 0.07 0.43666667 0.8

0.42 0 0.7
LOR 0.66 0.66 0.6
Z2 0.18 0.18 0.42 0.58
0.5
0.18 0
LOS 0.04 0.04 0.4

XB 0.04 0.04 0.1 0.26977099 0.3

0.04 0 0.2
LOI 0.42 0.58
0.1
0.1 0.26977099
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9
D)
1

0.9
ETAPAS N
0.04 0.04 0.8 posee 5 etapas
1° 0.04 0.245 0.7 la alimentacion optima Z1 se da en la 3° etapa
0.1305814 0.245 la alimentacion optima Z2 se da en la 2° etapa
0.6
2° 0.1305814 0.474
0.32485039 0.474 0.5
3° 0.32485039 0.578 0.4
0.41820472 0.578
0.3
4° 0.41820472 0.62
0.54 0.62 0.2
5° 0.54 0.67 0.1
0.69 0.67
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1

X-Y X=Y XD Z1 Z2 XB
LOR LOS LOA1 LOA2 LOI N
 x y 1.2
D17. A mixture of acetone and ethanol (acetone is more volatile) is fed to an enriching column that has 0 0
1
a liquid side stream withdrawn. The feed flow rate is 100.0 mol/min. Feed is 60.0 mol% acetone 0.1 0.262
and is a saturated vapor. The liquid side product is withdrawn from the second stage below the 0.15 0.348 0.8
total condenser at a flow rate of S = 15.0 mol/min. The reflux is returned as a saturated liquid. 0.2 0.417
The distillate should be 90.0 mol% acetone. The external reflux ratio is L/D = 7/2. Column 0.25 0.478 0.6 xy
pressure is 1.0 atm. Column is adiabatic and CMO is valid. Equilibrium data are in Problem 0.3 0.524 x=y
0.4
4.D7. Note: Trial and error is not required. 0.35 0.566
Find the mole fraction of acetone in the sidestream xS, the mole fraction of acetone in the bottoms 0.4 0.605 0.2
xB, and the number of equilibrium stages required. 0.5 0.674
0.6 0.739 0
0.7 0.802 0 0.2 0.4 0.6 0.8 1
componente F D B S Z XD XB XS F' 0.8 0.865
acetona 60 48.9138909 6.44144758 4.64466351 0.6 0.9 0.21015297 0.30964423 55.3553365 0.9 0.929
etanol 40 5.43487676 24.2097848 10.3553365 0.4 0.1 0.78984703 0.69035577 29.6446635 1 1
100 54.3487676 30.6512324 15
CON SOLVER
Ln/D 3.5 D XB XS B
54.3487676 0.21015297 0.30964423 30.6512324 100

Ln/D 3.5 D XB XS B
54.3487676 0.21015297 0.30964423 30.6512324 100

100.00

q Ln Vn L' V' Lm Vm m b LOR-LOI 0.310 0.441

0 190.220687 244.569454 175.220687 244.569454 175.220687 144.569454 LOR 0.77777778 0.2 LOI-LOA 0.532 0.600
LOA 0 0.6 LOI-LOS 0.532 0.600
LOI 0.71644551 0.21899118
XD 0.9 0.9 1.2 LOS 1.21201735 -0.04455608
0.9 0 xy
1 x=y LOR 0.9 0.9
XB 0.210152972 0.21015297 0.8 XD 0.800 0.822
0.210152972 0 XB
0.6 LOA 0.6 0.6
XS
XS 0.309644234 0.30964423 0.532 0.6
0.4 Z
0.309644234 0
LOA
0.2 LOI 0.800 0.822
Z 0.6 0.6 LOR 0.532 0.600
0.6 0 0 LOA
0 0.2 0.4 0.6 0.8 1
LOS 0.21015297 0.21015297
0.532 0.600

N 1.2
0.9 0.9 xy

0.855 0.9 1 x=y

0.855 0.865 0.8 XD
0.8 0.865 XB
0.8 0.82222222 0.6
XS
0.734 0.82222222
0.4 Z
0.734 0.77088889
0.654 0.77088889 LOA
0.2
0.654 0.70866667 LOR
0.56 0.70866667 0
LOA
0 0.2 0.4 0.6 0.8 1
0.56 0.62020067
0.424 0.62020067
0.424 0.46933928
0.244 0.46933928
0.244 0.25117616
0.098 0.25117616
0.098 0.092
 D19.* A distillation column is separating acetone and ethanol. The column effectively has six
equilibrium stages plus a partial reboiler. Feed is a two-phase feed that is 40% liquid and 75
mol% acetone. Feed rate is 1000 kmol/h, and the feed stage is fourth from the top. The column is
now operating at a steady state with the bottoms flow valve shut off. However, a distillate product
is drawn off, and the vapor is boiled up in the reboiler. L0/D = 2. Reflux is a saturated liquid.
CMO can be assumed. p = 1 atm. Equilibrium data are in Problem 4.D7. Find the distillate X-Y X=Y
composition. If one drop of liquid in the reboiler is withdrawn and analyzed, predict xB. 1.2
componente F D B Z XD XB x y
acetona 700 698.836565 1.1634349 0.7 0.742 0.02 0 0 1
etanol 300 242.99169 57.0083102 0.3 0.258 0.98 0.1 0.262
1000 941.828255 58.1717452 0.15 0.348 0.8
DATOS: 0.2 0.417
0.6
N 6 0.25 0.478
q 0.4 0.3 0.524 0.4
Ln/D 2 0.35 0.566
0.4 0.605 0.2
F D B R q Vn Ln 0.5 0.674
1000 941.828255 58.1717452 2 0.4 2825.48476 1883.65651 0.6 0.739 0
0 0.2 0.4 0.6 0.8 1 1.2
0.7 0.802
Vm Lm 0.8 0.865
2225.484765 2283.65651 0.9 0.929
1 1
X Y
0.6895 0.707 N 1.2
Z 0.7 0.7 0.742 0.742
0.7 0 LOR 0.742 0.742 0.6 0.742 1
0.6895 0.707 0.6 0.61516057
0.8
XD 0.742 0.742 0.418 0.61516057
0.742 0 LOS 0.02 0.02 0.418 0.42840329
0.6
0.6895 0.707 0.21 0.42840329
XB 0.02 0.02 0.21 0.21496639 0.4
0.02 0 LOA 0.7 0.7 0.08 0.21496639
0.6895 0.707 0.08 0.08156833 0.2
m b 0.03 0.08156833
LOR 0.666666667 0.24733333 0.03 0.03026139 0
0 0.2 0.4 0.6 0.8 1 1.2
LOS 1.02613891 -0.00052278 0.01 0.03026139
0.01 0.00973861 X-Y X=Y Z XD XB LOR LOS LOA N
D21. Una columna enriquecedor tiene dos alimentaciones. Alimentar F1 (entrada en la parte inferior) es un vapor
saturado. caudal
D21. An enricher column has two feeds. Feed F1 (input at the bottom) is a saturated vapor. Flow rate
F1 = 100,0 kmol / h. Este feed está 20,0% en moles de metanol y 80,0% en moles de agua. Alimente F2 (parte de
entrada F1 = 100.0 kmol/h. This feed is 20.0 mol% methanol and 80.0 mol% water. Feed F2 (input part
camino hastaway up the column)
la columna) is a two-phase
es una mezcla mixture
de dos fases quethat is 90
es 90% de%líquido.
liquid. Caudal
Flow rate
F2 =F280,0
= 80.0 kmol/h.
kmol / h. Feed con solver
alimentaciónF2 is 45.0 moles % methanol and 55.0 mol% water. We desire a distillate that is 95.0 mol% XB D
methanol.
F2 es 45,0 moles% Reflux isy 55,0%
de metanol returned as a saturated
en moles de agua.liquid.
DeseamosPressure is one atmosphere.
un destilado que es 95,0%L/D = 1.375.
en moles 0.11326958 42.5602606
metanol. El reflujo
AssumeseCMO.
devuelve
Datacomo un líquido
are available insaturado.
Table 2-7.La presión es de una atmósfera. L / D = 1,375.
Asumir OCM.Find:
Los datos están
D, B, xB, disponibles
optimum feed en la Tabla
location 2-7.
and number of equilibrium stages required. 179.999948

Comp F1 F2 F D B z1 z2 z xD xB
metanol 20 36 56 40.4322475 15.5677422 0.2 0.45 0.31111111 0.95 0.113269584
agua 80 44 124 2.12801303 121.871997 0.8 0.55 0.68888889 0.05 0.886730416
100 80 180 42.5602606 137.439739

DATOS
q1= 0 F1 F2 D B
q2= 0.9 100 80 42.56 137.44
Ln/D= 1.375
R= 1.375 Vm Lm Li Vi Ln Vn
35.64 173.08 101.080619 43.6408794 58.5203583 101.08

x y
0 0 XD 0.95 0.95
X-Y X=Y XD Z1 Z2 XB
0.02 0.134 0.95 0
1.2
0.04 0.23
0.06 0.305 Z1 0.2 0.2
1
0.08 0.365 0.2 0
0.1 0.418 0.8
0.15 0.517 Z2 0.45 0.45
0.2 0.579 0.45 0 0.6
0.3 0.665
0.4 0.729 XB 0.11326958 0.11326958 0.4

0.5 0.779 0.11326958 0

0.2
0.6 0.825
0.7 0.87 0
0.8 0.915 0 0.2 0.4 0.6 0.8 1 1.2
0.9 0.958
0.95 0.979
1 1

LOA1 0.2 0.2 X-Y X=Y XD Z1 Z2 XB

m b 0 0.2 LOA1 LOA2 LOR LOS LOI
LOR 0.57894737 0.4 1.2
LOS 4.85623872 -0.43679456 LOA2 0.45 0.45
LOA1 0 0.2 0.41 0.81 1
LOA2 -9 4.5
0.8
LOI 1.50214516 0.00302495 LOR 0.95 0.95
0.43 0.64894737 0.6

LOS 0.11326958 0.11326958 0.4

0.1 0.2
0.2

LOI 0.43 0.64894737 0

0.1 0.2 0 0.2 0.4 0.6 0.8 1 1.2

ETAPAS N 1.2
0.95 0.95
1° 0.89 0.95 RPTA
0.89 0.91526316 1 posee 7 etapas
2° 0.809 0.91526316 la etapa en la que se encuentrala alimentacion Z1 es 7 ma
0.809 0.86836842 la etapa en la que se encuentrala alimentacion Z2 es 5°
3° 0.71 0.86836842 0.8
0.71 0.81105263
4° 0.575 0.81105263
0.575 0.73289474 0.6
5° 0.41 0.73289474
0.41 0.61890447
6° 0.25 0.61890447 0.4
0.25 0.37856124
7° 0.085 0.37856124
0.085 0.090000 0.2

0
0 0.2 0.4 0.6 0.8 1 1.2

X-Y X=Y XD Z1 Z2 XB
 x y
0 0
0.02 0.134
0.04 0.23
0.06 0.305
0.08 0.365
0.1 0.418
0.15 0.517
0.2 0.579
0.3 0.665
0.4 0.729
0.5 0.779
0.6 0.825
0.7 0.87
0.8 0.915
0.9 0.958
0.95 0.979
1 1

componentes F D B Z XD XB componentesF D B Z XD XB
metanol 960 876.190 83.810 0.48 0.92 0.08 metanol 186.76 -426.880 613.640 0.09333333 -0.10666667 -0.30666667
agua 1040 76.190 963.810 0.52 0.08 0.92 agua 1040.52 4428.880 -2614.640 0.52 1.10666667 1.30666667
2000 952.381 1047.619 2001 4002.000 -2001.000

DATOS: Ln/D R 1 DATOS: Ln/D R 2

Vm/D 0.5 Vm/D 0.5
q 4 subenfriado q mayor a 1 q 4 subenfriado q mayor a 2

F D B q Ln Vn Vm Lm F D B q Ln Vn Vm
1.2
2000 952.381 1047.619 4 952.380952 7904.762 7904.762 8952.381 N 2001 4002.000 -2001.000 5 8004 2001.000 2001.000
0.92 0.92
0.815 0.92
1
1.2 0.815 0.8675
Z 0.48 0.48 LOR 0.92 0.92 0.7 0.8675 Z 0.09333333 0.09333333 LOR -0.10666667 -0.10666667
0.48 0 0.744 0.832 1 0.7 0.78216867 0.09333333 1 -0.40666667 -0.30666667
0.8
0.51 0.78216867
0.8
XD 0.92 0.92 LOS 0.08 0.08 0.51 0.56698795 XD -0.10666667 -0.10666667 LOS -0.30666667 -0.30666667
0.92 0 0.744 0.832 0.6 0.19 0.56698795 0.6-0.10666667 1 -0.40666667 -0.30666667
0.19 0.20457831
0.4
XB 0.08 0.08 LOA 0.48 0.48 0.04 0.20457831 XB -0.30666667 -0.30666667 LOA 0.09333333 0.09333333
0.08 0 0.744 0.832 0.2 0.04 0.0346988 0.4-0.30666667 1 -0.40666667 -0.30666667

m b 0 Posee 5 etapas m b
0 0.2 0.4 0.6 0.8 1
LOR 0.5 0.46 LOR
la alimentacion en la 2 da etapa 0.2 0.66666667 -0.03555556
LOS 1.13253012 -0.01060241 X-Y X=Y Z XD XB LOR LOS LOA LOS 0 -0.30666667

X Y 0X Y
0.744 0.832 0 0.2 0.3
0.1 -0.30666667
-0.40666667 0.4 0.5 0.6 0.7 0.8 0.9 1

X=Y Z XD XB LOR LOS LOA X-Y N

D29. A distillation column will use the optimum feed stage. A liquid side stream is withdrawn on the X Y 1.2
third stage below the total condenser at a rate of 15.0 kmol/h. The feed is a two phase mixture that 0 0
is 20% vapor. Feed to the column is 100.0 kmol/h. The feed is 60.0 mol% acetone and 40.0 mol% 0.1 0.262 1
ethanol. We desire a distillate composition that is 90.0 mol% ethanol. We operate with an 0.15 0.348
external reflux ratio of L/D = 3. The bottoms product is 10.0 mol% acetone. A partial reboiler is 0.2 0.417 0.8
used. Find the mole fraction ethanol in the side stream xs, the optimum feed location, and the total 0.25 0.478
number of equilibrium contacts needed. Equilibrium data are available in Problem 4.D7. 0.3 0.524 0.6 Series1
0.35 0.566 X=Y
0.4 0.605 0.4
0.5 0.674
0.6 0.739 0.2
0.7 0.802
0.8 0.865 0
con solver 0.9 0.929 0 0.2 0.4 0.6 0.8 1 1.2
D XS B 1 1
49.599925 0.788 35.4000751

99.9999 100
DATOS:
q= 0.8
Ln/D 3

componente F D B S Z XD XB XS F'
acetona 60 44.6399325 3.54000751 11.82 0.60 0.9 0.1 0.788 48.18
etanol 40 4.9599925 31.8600675 3.18 0.40 0.1 0.9 0.212 36.82
100 49.599925 35.4000751 15

q Ln Vn L' V' Lm Vm
0.8 148.799775 198.3997 133.799775 198.3997 213.799775 178.3997

1.2
Z 0.60 0.60 m b LOR 0.9 0.9
1
0.60 0 LOR 0.75 0.225 0.788 0.816
LOA -3.99984274 2.99990564 0.8
XD 0.9 0.9 LOI 0.67439505 0.2845767 LOA 0.60 0.60
0.9 0 LOS 1.19843125 -0.01984312 0.581 0.676 0.6

0.4
XB 0.1 0.1 LOR-LOI 0.788 0.816 LOI 0.788 0.816
0.1 0 LOI-LOA -0.581 -0.107 0.581 0.676 0.2

LOI-LOS 0.581 0.676 0

XS 0.788 0.788 LOS 0.1 0.1 0 0.2 0.4 0.6 0.8 1
0.788 0 0.581 0.676
Series1 X=Y Z XD XB
XS LOR LOA LOI LOS

N
0.9 0.9 1.2
0.858 0.9 Series1

0.858 0.8685 1 X=Y

0.81 0.8685 Z
0.81 0.8325 0.8 XD
0.75 0.8325
XB
0.75 0.79037299 0.6
XS
0.684 0.79037299
0.684 0.74586292 LOR
0.4
0.614 0.74586292 LOA
0.614 0.69865526 0.2 LOI
0.54 0.69865526 LOS
0.54 0.62730975 0
N
0.438 0.62730975 0 0.2 0.4 0.6 0.8 1
0.438 0.50506976
0.282 0.50506976 POSEE 10 ETAPAS
0.282 0.31811449
0.135 0.31811449
0.135 0.14194509
0.0556 0.14194509
0.0556 0.04678965
 1.2
D31.* A distillation column with a total condenser and a partial reboiler is separating ethanol from
1
water. Feed is a saturated liquid that is 25 mol% ethanol. Feed flow rate is 150 mol/h. Reflux is a
saturated liquid and CMO is valid. The column has three equilibrium stages (i.e., four equilibrium 0.8
contacts), and the feed stage is second from the condenser. We desire a bottoms composition that
is 5 mol% ethanol and a distillate composition that is 63 mol% ethanol. Find the required external 0.6 x-y
reflux ratio. Data are in Table 2-1 and Figure 2-2. x=y
0.4

X Y
0.2
0 0
0.019 0.17 0
0.0721 0.3891 0 0.5 1 1.5
0.0966 0.4375
0.1238 0.4704 componente F D B Z XD XB
0.1661 0.5089 etanol 37.5 32.5862069 4.9137931 0.25 0.63 0.05
0.2337 0.5445 agua 112.5 19.137931 93.362069 0.75 0.37 0.95
0.2608 0.558 150 51.7241379 98.2758621
0.3273 0.5826
0.3965 0.6122
0.5198 0.6599 DATOS: q= 1
0.5732 0.6841 N= 3
0.6763 0.7385 Z en segunda etapa
0.7472 0.7815
0.8943 0.8943 Ln/D 1
1 1
F D B R q Ln Vn Vm Lm
x-y x=y XD Z XB
150 51.7241379 98.2758621 1 1 51.7241379 103.448276 103.448276 201.724138
LOR LOS LOA N
XD 0.63 0.63
0.63 0 m b
1
LOR 0.5 0.315 X Y
Z 0.25 0.25 LOS 1.95 -0.0475 0.25 0.44
0.8
0.25 0
0.6
XB 0.05 0.05 LOR 0.63 0.63 N
0.05 0 0.4 0.25 0.44 0.63 0.63
0.44 0.63
0.2
LOS 0.05 0.05 0.44 0.535
0.25 0.44 0.22 0.535
0
0 0.2 0.4 0.6 0.8 1 0.22 0.3815
LOA 0.25 0.25 0.07 0.3815
0.25 0.44 0.07 0.089
 UNIVERSIDAD NACIONAL DE SAN
ANTONIO ABAD DEL CUSCO

FACULTAD DE INGENIERIA DE PROCESOS

ESCUELA PROFESIONAL : INGENIERIA QUIMICA

ASIGNATURA: OPERACIONES UNITARIAS III

DOCENTE: Ing. ANTONIO BUENO

ALUMNO: OCON TTITO ANA HIDALIA

CODIGO: 144894