DOI 10.1007/s13369-015-1608-y
Abstract Tight gas sandstone reservoirs parameters, such The saturation-height-function method is used to estimate
as porosity, permeability and initial water saturation, are diffi- initial water saturation, and the Swanson parameter based
cult to be precisely estimated from conventional logs. What’s model is established to calculate permeability from con-
more, the effective gas-bearing formations cannot be directly structed pseudo-capillary pressure curves. Comparisons of
identified either due to the characteristics of complicated pore estimating porosity, permeability and water saturation with
structure, strong heterogeneity and high irreducible water sat- core-derived results illustrate that these techniques are effec-
uration. Nuclear magnetic resonance (NMR) logs, which are tive in tight gas sands evaluation. Finally, the effective tight
usually used to evaluate reservoir pore structure, are found gas sands can be identified through combined use of the esti-
to be effective in evaluating tight gas sandstone reservoirs. mated reservoir parameters and constructed pseudo-capillary
In this study, typical tight gas sandstone reservoirs of south- pressure curves from NMR logs, which is verified by the drill
west China are used as examples; techniques of estimating stem test data.
porosity, permeability, initial water saturation and construct-
ing pseudo-capillary pressure curve to quantitative evaluate Keywords Tight gas sandstone reservoirs · Pore structure ·
tight sandstone reservoirs pore structure are studied. The Nuclear magnetic resonance (NMR) logs · Conventional
acoustic and NMR logs are combined to calculate porosity. logs · Reservoir evaluation
The technique proposed by Volokitin et al. (1999) is used to
construct pseudo-capillary pressure curves from NMR logs.
1 Introduction
X. Liang (B)
Key Laboratory of Geo-detection, China University With the fast development of oil and gas exploration, tight oil
of Geosciences, Ministry of Education, Beijing,
and gas sandstone reservoirs have played an important role
People’s Republic of China
e-mail: xiaoliang@cugb.edu.cn in stabilizing and increasing production. The proportion of
production from tight oil and gas sands is much high in China
X. Liang [1]. The Changqing oil field, which is the typical ultra-low
School of Geophysics and Information Technology, China
University of Geosciences, Beijing, People’s Republic of China
permeability to tight sandstones, locates in the Ordos basin
and has been the biggest oil field, and in the Sichuan basin,
M. Zhi-qiang the biggest tight gas sandstone reservoirs have been found
State Key Laboratory of Petroleum Resource and Prospecting, recently. Comparing with conventional reservoirs, tight sand-
China University of Petroleum, Beijing, People’s Republic of China
stone reservoirs evaluation is much more challenging due to
M. Zhi-qiang many factors, e.g., extreme low porosity, permeability, high
Key Laboratory of Earth Prospecting and Information Technology, irreducible water saturation, complicated pore structure and
Beijing, People’s Republic of China strong heterogeneity [2]. To improve the accuracy of tight
J. Yan
sandstone reservoirs study, the pore structure should be first
Southwest Oil and Gas Field Branch Company, PetroChina, evaluated [2]. The nuclear magnetic resonance (NMR) logs
Sichuan, People’s Republic of China can be used to provide useful evaluation for many reservoirs
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500 800
X4 X4
400 X6 600 X6
Frequency
300 400
Frequency
200 200
100
0
0
0~2 2~4 4~6 6~8 8~10 10~12 12~14
CPERM, mD
CPOR, %
Fig. 2 The distribution of core-derived permeabilities for the tight gas
Fig. 1 The distribution of core-derived porosities for the tight gas sands sands in central Sichuan basin
in central Sichuan basin
0.6
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8
3 Problems of Tight Gas Sandstone Reservoirs
Evaluation in the Central Sichuan Basin
6
In reservoir evaluation and reserves calculation, estimation
of reservoir parameters, such as porosity, permeability and
oil saturation (thus water saturation), is of great importance.
Frequency
Fig. 4 The distribution of irreducible water saturation (Swi ) for core 3.1 Problem of Porosity Estimation in Tight Gas Sands
samples with laboratory NMR experiment
Generally, reservoir porosity is estimated from conventional
8 logs (such as density, compensated neutron or acoustic logs),
when the relationship of conventional logs with core-derived
porosity is established by using the core calibration logging
6 method [5,6]. In the target tight gas sands of central Sichuan
basin, such a traditional method was used to establish the
relationships among core-derived porosity and other para-
Frequency
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12
2.00 2.16 0.16 1.84 −0.16
3.00 3.24 0.24 2.76 −0.24
8 4.00 4.32 0.32 3.68 −0.32
5.00 5.40 0.40 4.60 −0.40
4 6.00 6.48 0.48 5.52 −0.48
7.00 7.56 0.56 6.44 −0.56
0 8.00 8.64 0.64 7.36 −0.64
2 2.2 2.4 2.6 2.8 3 9.00 9.72 0.72 8.28 −0.72
DEN, g/cm 3 10.00 10.80 0.80 9.20 −0.80
11.00 11.88 0.88 10.12 −0.88
b 20
12.00 12.96 0.96 11.04 −0.96
X4 13.00 14.04 1.04 11.96 −1.04
16 X6 14.00 15.12 1.12 12.88 −1.12
CPOR, %
12
1000
8 100
10
4
CPERM, mD
1
0
0 5 10 15 20 25 30 35 0.1
CNL, % X4_Well A
0.01
X4_Well B
c 20 X4_Well C
0.001
X4 X6_Well A
16 0.0001 X6_Well C
X6
X6_Well D
0.00001
0 5 10 15 20
12
CPOR, %
CPOR, %
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Formation factor
most suitable for water saturation evaluation from con-
ventional logs. Since the necessary input parameters were
10
first determined from rock resistivity experimental measure-
ments, this method has been widely used in the past 70 years. y = 1.8389x-1.247
R² = 0.9312
The Archie’s equations are expressed in Eqs. 1 and 2 [12].
R0 a
F= = m (1)
Rw ϕ 1
Rt 1 0.01 0.1 1
Ir = = n (2)
Ro Sw Porosity, fraction
Resistivity index
porosity in fraction; Sw is the water saturation in fraction; no.13 no.14
no.15 no.16
a is the tortuosity factor; m is the cementation exponent; n no.17 no.18
is the saturation exponent, and its value is affected by rock no.19 no.20
no.21 no.22
pore structure; a, m and n are referred to as rock resistivity no.23 no.24
no.25 no.26
parameters. no.27 no.28
Combining Eqs. 1 and 2, a derivative formula could be no.29 no.30
no.31 no.32
written in Eq. 3. no.33 no.34
no.35 no.36
1
a × Rw
Sw = n m (3) 0.1 1
ϕ × Rt Water saturation, fraction
This formula illustrates that the values of a, m, n, Rw , ϕ and Fig. 8 a The cross-plot of porosity versus formation factor for core
Rt must be first determined for water saturation calculation. samples drilled from tight gas sandstones of X4 and X6 Formations in
Generally, the deep lateral resistivity (RLLD) or deep Sichuan basin, southwest China [14]. b The cross-plot of water satu-
ration versus resistivity index for core samples drilled from tight gas
induction resistivity (RILD) can be directly used as Rt , while sandstones of X4 and X6 Formations in Sichuan basin, southwest China
Rw can be checked from the formation water salinity by using [14]
the Schlumberger’s log interpretation charts [13], and ϕ can
be accurately calculated once effective models have been
established. by expressed by using the typical power function (Fig. 8).
Determination of rock resistivity parameters is the most This is particularly challenging for the determination of n. In
important in estimating water saturation by using Eq. 3. Gen- this case, Archie’s equations are invalid in water saturation
erally, the values of a, m and n are determined by using the estimation.
statistical regression method based on laboratory resistivity
measurements of the target core samples. Determination of 3.4 Problem of Effective Formation Identification in Tight
a and m is relying on the scatter plot of porosity and forma- Gas Sands
tion factor. The value of n can be obtained from the scatter
plot of water saturation and resistivity index. For conven- Based on Figs. 1, 2, 3 and 4, it can be concluded that these
tional reservoirs, the values of rock resistivity parameters tight gas sands displayed such characteristics of ultra-low
are easily acquired by using the rock resistivity experimen- porosity, permeability and high irreducible water saturation
tal measurements, and the Archie’s equations can be used in the X4 and X6 Formations. These characteristics pose
to calculate water saturation. However, in tight gas sands, challenges for effective gas-bearing formation identification.
the values of rock resistivity parameters are difficult to be The resistivity contrast of gas-bearing formations and water-
obtained, because the relationships between porosity and for- saturated layers is lower than that of the conventional reser-
mation factor, water saturation and resistivity index, cannot voirs. Figure 9a, b shows the conventional log responses of
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Fig. 9 a Conventional log response of gas-bearing formation [2]. b Conventional log response of water-saturated layer [2]
two adjacent wells. From the drill stem test data, it can be seen the pore structure should be first evaluated [2]. The NMR
that for the interval of xx39–xx51 m in Fig. 9a, gas production logs have significant advantage in reservoir characterization,
was estimated as 10.578 × 104 m3 /day. While the interval of especially in tight sandstone reservoirs with ultra-low poros-
xx70–xx07 m displayed in Fig. 9b, it is pure water-saturated ity, permeability and complicated pore structure [3,4]. In oil
layers. With detailed analysis of these two tested intervals, bearing or water-saturated formations, reservoir porosity can
it can be further observed that these two intervals almost be determined from NMR logs, whereas in tight gas sands,
present the same bulk density of 2.4 g/cm3 , which denotes the extracted porosity is often underestimated due to the low
similar porosity. For the resistivity response, the gas-bearing hydrogen index of natural gas [15]. Based on the analysis of
formation shows that the resistivity is about 9 m, and the the NMR T2 spectrum, pore structure of the formation can be
resistivity of the water-saturated layer is about 5 m. The qualitatively estimated. However, it still remains a challenge
resistivity difference between these two intervals is lower in quantitatively estimating the pore throat radius and pore
than that of the conventional gas-bearing and water reser- structure parameters from NMR logs. To effectively evaluate
voirs. This poses a challenge for effective identification of tight gas sands using the log data, a method that combines
tight gas-bearing formations from conventional methods [2]. conventional and NMR logs should be proposed. In the next
section, we will introduce an effective method for tight gas
sands evaluation.
4 Novel Methods of Estimating Tight Gas Sandstone
Reservoir Parameters
4.1 Estimation of Porosity from NMR and Acoustic Logs
Based on the discussion in the previous paragraphs, we can
conclude that tight gas sandstone reservoirs evaluation using 4.1.1 Principle of Calculating Porosity from NMR
conventional methods faces great challenge in the Xujiahe and Acoustic Logs
Formation. The challenge is primarily caused by the com-
plicated pore structure and strong heterogeneity of tight gas In gas-bearing formations, to correct the effect of low hydro-
sandstone reservoirs. To improve tight gas sands evaluation, gen index of natural gas on NMR porosity, Coates et al. [3]
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and Dunn [4] proposed the NMR porosity correction method on porosity. It is difficult in calculating porosity only from
in Eq. 4: conventional interval transit time log [5].
If we define two parameters of α and β,
CMRP = φ × Sg × HIg × Pg + φ × HI f × (1 − Sg ) (4) where
t − tma
where α=
t f − tma
− TTw
Pg = 1 − e 1,g β = 1 − HIg × Pg
where CMRP is the NMR porosity in % and can be directly Substituting these two parameters into Eqs. 4 and 8, respec-
obtained from NMR logs; φ is the formation porosity in %; Sg tively, Eq. 9 can be derived,
is the gas saturation in fraction; HIg is the gas hydrogen index,
HIf is the pore fluid hydrogen index and the units of them are β α
φ= × PHIS + × CMRP (9)
fraction; Pg is the polarization factor; Tw is the polarization α+β α+β
time in microseconds; and T1,g is the longitudinal relaxation
time for natural gas in microseconds. If we further define the following two parameters m and n:
For fully water-saturated rocks where HIf is designed as β
1.0, Eq. 4 can be rewritten in Eq. 5: m=
α+β
α
CMRP n=
= 1 − Sg × (1 − HIg × Pg ) (5) α+β
φ
Equation 9 can be simplified as follows:
Equation 5 illustrates that the values of Sg , HIg and Pg should
be first determined to obtain porosity from NMR logs for gas- φ = m × PHIS + n × CMRP (10)
bearing reservoirs. Actually, these parameters are difficult to
be obtained from conventional logs at present, bringing the where
difficulty of porosity estimation from NMR logs.
β α
Based on the general form of the Wyllie’s average time m+n = + =1
equation, the response equation of interval transit time log α+β α+β
can be expressed as follows [16]: The effects of natural gas to conventional and NMR logs can
be calibrated by using Eq. 10, and formation porosity can be
t = tma ×(1−φ)+tw ×φ ×(1− Sg )+tg ×φ × Sg (6) estimated by integrating interval transit time and NMR logs
once the values of m and n are determined.
where t is the log measured interval transit time; tma is
the interval transit time of rock matrix for sandstone, and its 4.1.2 Calibration of m and n in the Target Tight Gas Sands
value is 55.5 µs/ft; tw is the interval transit time of water,
and its value is 189; tg is the interval transit time of gas. From Eq. 10, it can be observed that parameters m and n
All parameters in the unit of them are microsecond per feet. should be first calibrated before the equation can be applied
For clean sandstone, the porosity can be calculated from to calculate tight gas sandstone porosity. To calibrate m and
Eq. 7: n, more than seven hundreds of core samples are used for
calibration and the rest are used for validation.
t − tma
PHIS = (7) The core-derived porosity can be considered as the true
t f − tma
formation porosity. After both sides of Eq. 10 are divided by
where PHIS is porosity from acoustic log in fraction; tf is CMRP, Eq. 10 can be rewritten as:
the interval transit time of pore fluid.
CPOR PHIS
Substituting Eq. 6 into Eq. 7, a derivative expression could =m× +n (11)
be obtained as follows: CMRP CMRP
Parameters m and n are calibrated using the core samples.
PHIS t − tma
= 1 + Sg × (8) Equation 11 is expressed in Fig. 10 and Eq. 12.
φ t f − tma
φ = 0.809 × PHIS + 0.191 × CMRP, R 2 = 0.8939 (12)
Equation 8 illustrates that Sg and tf are the two important
input parameters in calculating porosity using interval transit From Fig. 10, we find strong correlation among CPOR,
time log. However, the determination of Sg and tf is relied CMRP and PHIS. The correlation coefficient is high enough.
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SHg/Pc
1 10
0.1 0
1 10 100 0 20 40 60 80 100
SHg, % SHg, %
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1 S
= ρ2 = Fs (15)
10
T2 V pore rpor
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c
Amplitude, v/v A D 1
Pc = 1+ × × (21)
1 0.8 0.6 0.4 0.2 0 B × T2 + 1 K T2
10 0.1
where A, B, C, D and K are the mentioned input parameters
1 in the conversion function, all of which needed to be first
1
T2 relaxation time, ms
calibrated.
10 Volokitin’s model had been applied to many areas of China
1/T2, ms -1
0.1
and had been verified to be effective [27–29]. It is also applied
100 in our study. Results illustrate that it is an effective method
0.01 for our case study. Hence, in this study, the model expressed
1000
in Eq. 21 is used to construct pseudo-capillary pressure curve
NMR reverse cumulative curve
0.001
10000
from NMR logs.
NMR T2 distribution
1
Pc, MPa
0.01
0.1
0.001
0.01
0.0001
0.001 0.00001
100 80 60 40 20 0 100 80 60 40 20 0
SHg, % So, %
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Fig. 15 Comparisons of
capillary pressure curves
a 1000 b 10000
acquired from two different Por=10.6% Por=7.9%
100 1000 Perm=0.323mD
methods Perm=1.05mD
100
10
Pc, MPa
Pc, MPa
10
1
1
0.1
MICP curve 0.1 MICP curve
0.01 Pseudo capillary pressure 0.01 Pseudo capillary pressure
curve curve
0.001 0.001
100 80 60 40 20 0 100 80 60 40 20 0
SHg, % SHg, %
c 1000 d 1000
Por=7.5% Por=14.7%
100 Perm=0.851mD 100 Perm=5.06mD
10 10
Pc, MPa
Pc, MPa
1 1
0.1 0.1
MICP curve MICP curve
0.01 Pseudo capillary pressure 0.01 Pseudo capillary pressure
curve curve
0.001 0.001
100 80 60 40 20 0 100 80 60 40 20 0
SHg, % SHg, %
struct pseudo-capillary pressure curves. We then compare the called irreducible water. Figure 4 displays that in our target
shapes of the constructed pseudo-capillary pressure curves tight gas sands, the average Swi is close to 45 %, leading to
with the MICP curves. Figure 15 displays the comparisons of low resistivity contrast. It is therefore difficult in identifying
four representative core samples. From these comparisons, effective gas-bearing formation from water-saturated layers.
we can observe that all the constructed capillary pressure Estimated Swi could be used to overlap with initial water
curves match with the laboratory MICP curves very well, saturation; gas-bearing formation could then be effectively
illustrating that Eq. 21 is effective in our target tight gas identified.
sands in constructing capillary pressure curves from NMR The NMR logs have unique advantages in estimating Swi .
logs. However, Fig. 5 illustrates that in our target tight gas sands,
If this technique is extended to field application, the unified T2cutoff cannot be obtained from laboratory NMR
pseudo-capillary pressure curve, the corresponding pore experimental measurements. Hence, the T2cutoff technique
throat radius distribution and the pore structure evaluation cannot be used to extract Swi from NMR logs in the X4 and
parameters, including the average pore throat radius, the X6 sections.
threshold pressure and median pore throat radius, can also Based on the theoretical analysis of the classical Timur
be estimated from the pseudo-capillary pressure curves in and the SDR model [30–32], Xiao et al. [33] derived a model
the interval with which NMR logs had been acquired. that combines porosity and T2 logarithmic mean of the NMR
T2 spectrum (T2lm ) to estimate Swi . This model is effective in
Swi estimation in the Xujiahe Formation. Hence, it is directly
4.4 Calculation of Irreducible Water Saturation from NMR applied in our target tight gas sands. This model is expressed
Logs as follows:
−0.24518
Irreducible water saturation (Swi ) is a very important para- Swi = 118.91 × ϕ −0.08326 × T2lm (22)
meter in tight gas sandstone reservoirs evaluation. This is
because in tight gas sands, the pore space is mainly occu- where ϕ is the porosity in %, which can be estimated by
pied by water that cannot flow into the borehole, which is using Eq. 12; T2lm is the T2 logarithmic mean of the NMR
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NMR logs.
By using Eq. 22, Swi can be calculated from NMR logs.
40
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Fig. 17 A field example of evaluating tight gas sandstone reservoir by using NMR logs
displayed in the eighth track is estimated initial water satura- capillary pressure are coincided with the core-derived results.
tion from the pseudo-capillary pressure curves using the SHF This demonstrates the effectiveness of the technique of con-
method. SWICAL is the estimated irreducible water satura- structing pseudo-capillary pressure curves from field NMR
tion using Eq. 21, and SWICORE is the irreducible water logs.
saturation obtained from the core samples with laboratory From the estimated results, it can be found that in the
NMR experimental measurements. From the comparison of interval of xx88–xx00m, although the estimated initial water
the values of several kinds of the water saturation, it can be saturation reaches to 40–50 %, it is coincided with the irre-
concluded that the SWCAL and SWICAL are coincided with ducible water saturation. This denotes that no free water
each other very well. Additionally, they are closed to the core- can be produced. After analyzing the constructed pseudo-
derived results. This illustrates that the estimated SWCAL capillary pressure, estimated porosity, permeability and pore
and SWICAL are accurate, and the proposed method is reli- structure evaluation parameters, it can be concluded that the
able. PERM displayed in the ninth track is the estimated pore structure of this interval is good. If necessary fracture
permeability from pseudo-capillary pressure curves by using treatments are applied, this interval is worth of developing.
the Swanson-based permeability model displayed in Fig. 12. Such conclusion is confirmed by the drill stem testing data.
A good consistency of estimated permeability with core- The drill stem testing data illustrate that this interval is pure
derived permeability (CPERM) illustrates that the Swanson- gas-bearing formation, where no water is produced. This field
based permeability model is valuable in tight gas sands per- example illustrates that the proposed method in this study is
meability estimation. From the tenth to twelve tracks, we valuable in tight gas reservoirs evaluation, and they can be
compare the estimated average pore throat radius (RM), further extended to be applied to other types of tight sand-
maximum pore throat radius (RMAX) and threshold pres- stone reservoirs.
sure (PD) from the pseudo-capillary pressure curves with
the core-derived average pore throat radius (CRM), maxi-
mum pore throat radius (CRMAX) and threshold pressure 6 Discussion
(CPD), separately. In the last track, we compare the Swan-
son parameter acquired from two different kinds of methods. Detailed observing Eq. 21, we can find that in the process of
Swanson is the estimated Swanson parameters from con- constructing pseudo-capillary pressure curves in our target
structed pseudo-capillary pressure curve using the method tight gas sands, the unitary input parameters in the Volok-
illustrated in Fig. 11, and Cswanson is the extracted Swan- itin’s model are calibrated and used. This is because in our
son parameters from experimental MICP data. Comparison target tight gas sandstone reservoirs of X4 and X6 Forma-
shows that the pore structure evaluation parameters and the tions, the heterogeneity is not strong enough, and this can
Swanson parameter acquired from the constructed pseudo- be verified by the displayed MICP curves in Fig. 14a. From
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Fig. 14a, it can be observed that the shapes of all 20 core Acknowledgments This research work was supported by National
samples are relative regular, and they are not divergent. In Natural Science Foundation of China (No. 41302106), China Post-
doctoral Science Foundation funded project (Nos. 2012M520347,
this case, the unified model can be used. However, if forma- 2013T60147), National Science and Technology Major Project (No.
tions are inhomogeneous, the unified function cannot be used 2011ZX05044), the Fundamental Research Funds for the Central
to construct pseudo Pc curve [25]. In this case, formations Universities and Open Fund of Key Laboratory of Geo-detection
should be classified into several types by other methods, and (China University of Geosciences, Beijing), Ministry of Education (No.
GDL1204).
in every type of formation, individual mentioned input para-
meters in the Volokitin’s model should be calibrated. Mean-
while, it need to be noticed that the SHF method is applicative
only in the structural hydrocarbon reservoir. This is because References
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