A.

Perhitungan Kebutuhan Larutan HCl pekat

3,65 x V
Vx = mL
10 x k x L
3,65 x 250
Vx = mL
10 x 1,19 x 37
912,5
Vx = mL
440,3
Vx = 2,0724 mL
B. Standarisasi Larutan HCl 0,1 N
Volume Na2CO3 Volume Titrasi HCl 0,1 N (mL)
10 ml 11,3
10 ml 10,7
10 ml 10,8
11,3+10,7+10,8
Rata-rata volume penambahan = = 10,9 mL
3
Standarisasi larutan HCl 0,1 N
1000 x G x 2 1000 x 1,5380 x 2 1,076
NHCl = = = = 0,0931
V:v x VHCL x 106 100:10 x 10,9 x 106 11,554

C. Analisa larutan campuran NaHCO3 dan Na2CO3

Larutan campuran Titrasi HCl 0,1 N
NaHCO3 dan Na2CO3 Indikator PP (A mL) Indikator MO (B mL)
10 mL 3,5 32,9
10 mL 3,2 33,1
10 mL 3,6 32,9
Rata-rata 3,4 32,96
1 Na2CO3 = 2A x NHCl x 5,3 mgram NaHCO3 = (B - A) x NHCl x 84

= 2(3,5) x 0,0931 x 53 = (32,9 - 3,5) x 0,0931 x 84

= 34, 5 = 29,4x 0,0931 x 84

= 229,67

2 Na2CO3 = 2A x NHCl x 5,3 mgram NaHCO3 = (B - A) x NHCl x 84

= 2(3,2) x 0,0931 x 53 = (33,1 - 3,2) x 0,0931 x 84

 = 31,54 = 29,9 x 0,0931 x 84

= 233,57

3 Na2CO3 = 2A x NHCl x 5,3 mgram NaHCO3 = (B - A) x NHCl x 84

= 2(3,6) x 0,0931 x 53 = (32,9 – 3,6) x 0,0931 x 84

= 35,48 = 29,3 x 0,0931 x 84

= 229,13

Menghitung Standar Deviasi

No X X – X- (X – X-)2

1 229,67 -1,12 1,2544

2 233,57 2,78 7,7284

3 229,13 -1,66 2,7556

X- = 230,79 ∑ = 11, 7384

∑(X – X−)2
SD = √ 𝑛−1

𝟏𝟏,𝟕𝟑𝟖𝟒
SD = √ 3−1

SD = √5, 8692

SD = 2,42

Standarisasi larutan HCl 0,1 N

0,0931−0,1
% kesalahan = x 100% = 0,7%
0,1