Appendix PDF

Lampiran 1
DAFTAR KONVERSI AYAKAN DARI MESH KE MIKRON
U. S
INCHES MICRONS MILLIMETERS
MESH
3 0,2650 6730 6,730
4 0,1870 4760 4,760
5 0,1570 4000 4,000
6 0,1320 3360 3,360
8 0,0937 2380 2,380
10 0,0787 2000 2,000
12 0,0661 1680 1,680
14 0,0555 1410 1,410
16 0,0469 1190 1,190
18 0,0394 1000 1,000
20 0,0331 841 0,841
25 0,0280 707 0,707
30 0,0232 595 0,595
35 0,0197 500 0,500
40 0,0165 400 0,400
45 0,0138 354 0,354
50 0,0117 297 0,297
60 0,0098 250 0,250
70 0,0083 210 0,210
80 0,0070 177 0,177
100 0,0059 149 0,149
120 0,0049 125 0,125
140 0,0041 105 0,105
170 0,0035 8 0,088
200 0,0029 74 0,074
230 0,0024 63 0,063
270 0,0021 53 0,053
325 0,0017 44 0,044
400 0,0015 37 0,037
625 0,0008 20 0,020
1250 0,0004 10 0,010
2500 0,0002 5 0,005
http://www.skylighter.com/fireworks/help/Mesh_to_Microns_Coversion_Chart.a
Universitas Sumatera Utara

Lampiran 2.
Hasil Pengukuran Nanopartikel Bentonit

Lampiran 3.
Data Hasil Pengukuran Viskositas Karet Alam

Lampiran 4.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit

Lampiran 5.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit-CTAB

Lampiran 6.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit-PEG

Lampiran 7.
Data Hasil Uji Tarik Nanokomposit Karet Alam/Bentonit-SDS

Lampiran 8.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit

Lampiran 9.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-CTAB

Lampiran 10.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-PEG

Lampiran 11.
Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-SDS

Lampiran 12.
Spektrum FT-IR Nanokomposit Karet Alam/Bentonit

Lampiran 13.
Spektrum FT-IR Bentonit-CTAB

Lampiran 14.
Spektrum FT-IR Bentonit-PEG

Lampiran 15.
Spektrum FT-IR Bentonit-SDS

Lampiran 16.
Spektrum XRD Bentonit
Sampel_Firman
800
700
600
500
Intensitas
400
300
200
100
0
0 20 40 60 80 100
2 theta
Pos. Rel. Int. FWHM Area Height

No. d-spacing [Å] Backgr.[cts]
[°2Th.] [%] [°2Th.] [cts*°2Th.] [cts]
1 10.7108 8.235 17.66 0.1181 7.72 277 66.25
2 22.0416 3.963993 69.09 0.2755 70.43 335 259.14
3 23.8101 3.666463 45.12 0.2362 39.43 339 169.25
4 24.4887 3.56382 31.5 0.3149 36.7 340 118.16
5 26.8025 3.253334 27.16 0.2362 23.74 333.37 101.89
6 28.0081 3.112119 100 0.3936 145.63 327 375.08
7 30.4649 2.859381 25.18 0.1968 18.33 308 94.43
8 31.6564 2.751131 10.6 0.4723 18.52 295 39.76
9 35.7053 2.438098 30.49 0.4723 53.29 265 114.38
10 42.424 2.052797 11.09 0.9446 38.75 230 41.58
11 47.0161 1.854272 11.58 0.6298 26.98 201 43.43
12 48.4997 1.798415 15.82 0.3149 18.44 195 59.35
13 49.8345 1.751102 15.46 0.4723 27.01 198 57.98
14 51.5749 1.693229 17 0.2362 14.85 197 63.75

Lampiran 17.
Spektrum XRD Bentonit-CTAB

File: THE-2.DI 29-May-2013 14:43
=============================================================
=================
Philips Analytical PC-APD, Diffraction software
Sample identification: Sampel 2

Data measured at: 29-May-2013 12:03:00
Diffractometer type: PW1710 BASED

Tube anode: Cu
Generator tension [kV]: 40
Generator current [mA]: 30
Wavelength Alpha1 [•]: 1.54060
Intensity ratio (alpha2/alpha1): 0.500
Divergence slit: 1ø
Receiving slit: 0.45
Monochromator used: NO
Start angle [ø2é]: 5.000

End angle [ø2é]: 44.980
Step size [ø2é]: 0.020
Maximum intensity: 772.8400
Time per step [s]: 0.800
Type of scan: CONTINUOUS
Minimum peak tip width: 0.12

Maximum peak tip width: 1.00
Peak base width: 2.00
Minimum significance: 0.60
Number of peaks: 22
Angle d-value d-value Peak width Peak int Back. int Rel. int Signif.
[ø2é] à1 [•] à2 [•] [ø2é] [counts] [counts] [%]
10.775 8.2042 8.2244 0.240 77 296 10.0 2.36

13.925 6.3546 6.3702 0.240 38 299 5.0 1.01
15.440 5.7343 5.7484 0.960 13 299 1.7 0.97
20.075 4.4196 4.4304 0.480 42 324 5.5 0.98
22.160 4.0082 4.0181 0.240 552 324 71.5 8.39
23.060 3.8538 3.8633 0.280 135 324 17.4 2.05
23.885 3.7225 3.7317 0.240 317 324 41.0 4.57
24.670 3.6058 3.6147 0.160 185 324 23.9 0.96
25.765 3.4550 3.4635 0.160 130 324 16.8 0.67

26.845 3.3184 3.3266 0.160 237 324 30.7 1.59
27.975 3.1869 3.1947 0.280 773 328 100.0 6.19
28.245 3.1570 3.1648 0.120 552 328 71.5 1.98
28.665 3.1117 3.1194 0.120 240 328 31.1 1.21
29.765 2.9992 3.0065 0.160 114 328 14.8 0.96
30.610 2.9183 2.9255 0.120 188 328 24.3 0.70
31.690 2.8212 2.8282 0.240 123 328 15.9 2.27
33.340 2.6853 2.6919 0.320 66 328 8.5 2.58
33.875 2.6441 2.6506 0.160 29 328 3.8 0.64
35.765 2.5086 2.5148 0.160 259 328 33.5 0.84
39.425 2.2837 2.2893 0.480 26 313 3.4 1.28
42.550 2.1229 2.1282 0.640 58 299 7.5 0.89
43.415 2.0826 2.0878 0.320 38 296 5.0 0.62

Lampiran 18.
Spektrum XRD Bentonit-PEG

File: THE-3.DI 29-May-2013 14:43
=============================================================
=================


Tube anode: Cu


Number of peaks: 21
10.715 8.2500 8.2703 0.120 59 272 7.0 0.66

13.920 6.3568 6.3725 0.480 25 279 3.0 0.98
20.865 4.2540 4.2645 0.240 86 353 10.2 0.86
22.065 4.0253 4.0352 0.180 650 350 76.8 7.16
22.960 3.8704 3.8799 0.200 161 350 19.0 1.17
23.800 3.7356 3.7448 0.160 372 346 44.0 2.20
24.565 3.6210 3.6299 0.240 199 346 23.5 2.27
25.705 3.4629 3.4714 0.200 132 342 15.6 0.97
26.765 3.3281 3.3363 0.160 266 339 31.4 1.32

27.905 3.1947 3.2026 0.240 847 339 100.0 6.58
28.145 3.1680 3.1758 0.120 625 339 73.8 1.34
28.575 3.1213 3.1290 0.160 225 335 26.6 1.00
29.665 3.0091 3.0165 0.120 110 335 13.0 0.61
30.475 2.9309 2.9381 0.200 188 331 22.2 1.66
31.615 2.8278 2.8347 0.280 98 331 11.6 2.20
33.245 2.6927 2.6994 0.280 83 328 9.8 2.48
33.870 2.6445 2.6510 0.240 30 324 3.6 0.88
35.900 2.4995 2.5056 0.320 172 320 20.3 2.61
39.625 2.2727 2.2782 0.480 22 299 2.6 1.18
40.730 2.2135 2.2190 0.240 20 292 2.4 0.65
42.590 2.1210 2.1263 0.320 64 286 7.6 0.67
Lampiran 19.
Spektrum XRD Bentonit-SDS

File: THE-1.DI 29-May-2013 14:43
=============================================================
=================


Tube anode: Cu


Number of peaks: 18
7.700 11.4723 11.5005 0.120 26 310 3.7 0.86

10.710 8.2538 8.2741 0.200 88 276 12.5 1.55
13.875 6.3774 6.3931 0.480 26 272 3.7 0.97
22.145 4.0109 4.0208 0.220 462 339 65.3 8.49
22.965 3.8695 3.8790 0.200 77 339 10.9 0.90
23.875 3.7241 3.7332 0.160 276 335 38.9 1.87
24.660 3.6073 3.6161 0.280 139 335 19.7 2.54
25.840 3.4451 3.4536 0.120 94 331 13.3 0.80
26.830 3.3202 3.3284 0.200 207 331 29.3 2.34
27.965 3.1880 3.1958 0.240 708 328 100.0 4.46
28.255 3.1559 3.1637 0.120 484 328 68.4 0.78
28.625 3.1160 3.1236 0.120 177 328 25.0 1.14
29.760 2.9997 3.0070 0.240 94 324 13.3 1.76
30.505 2.9281 2.9353 0.160 169 324 23.9 1.23
31.635 2.8260 2.8330 0.200 86 320 12.2 0.91

33.295 2.6888 2.6954 0.240 71 317 10.0 0.66
35.800 2.5062 2.5124 0.280 222 320 31.4 3.07
39.705 2.2683 2.2738 0.640 18 299 2.5 0.70
Lampiran 20.
Spektrum XRD Nanokomposit Karet Alam/Bentonit

File: THE-9.DI 29-May-2013 14:44
=============================================================
=================



Tube anode: Cu


Number of peaks: 10
6.645 13.2911 13.3238 0.240 38 420 2.9 0.63

10.815 8.1739 8.1940 0.480 30 538 2.3 0.97
19.650 4.5142 4.5253 0.640 166 1253 12.6 0.67
22.130 4.0136 4.0235 0.480 79 1069 6.0 1.71
24.010 3.7034 3.7125 0.560 21 930 1.6 0.88
26.825 3.3208 3.3290 0.240 67 756 5.1 0.77
28.065 3.1769 3.1847 0.480 112 708 8.5 2.03
31.945 2.7993 2.8062 0.360 1011 600 76.3 14.79
34.565 2.5929 2.5993 0.320 400 557 30.2 7.19

36.340 2.4702 2.4763 0.440 1325 543 100.0 34.43
Lampiran 21.
Spektrum XRD Nanokomposit Karet Alam/Bentonit-CTAB

File: THE-5.DI 29-May-2013 14:43
=============================================================
=================


Tube anode: Cu


Number of peaks: 11

6.290 14.0404 14.0750 0.240 69 586 4.4 1.62

9.470 9.3316 9.3546 0.160 119 676 7.5 1.02
10.610 8.3314 8.3519 0.120 130 740 8.2 0.66
17.675 5.0139 5.0262 0.640 253 1296 16.0 0.69
18.840 4.7064 4.7180 0.240 292 1310 18.6 0.66
21.945 4.0470 4.0570 0.240 49 1109 3.1 0.82
27.605 3.2287 3.2367 0.240 79 745 5.0 1.04
28.555 3.1234 3.1311 0.320 71 718 4.5 0.96
31.745 2.8165 2.8234 0.180 1260 600 80.0 13.34
34.435 2.6024 2.6088 0.120 449 552 28.5 2.01
36.240 2.4768 2.4829 0.200 1576 543 100.0 19.81
Lampiran 22.
Spektrum XRD Nanokomposit Karet Alam/Bentonit PEG

File: THE-4.DI 29-May-2013 14:43
=============================================================
=================



Tube anode: Cu


Number of peaks: 10
10.300 8.5814 8.6026 0.320 18 475 1.4 0.73

19.150 4.6309 4.6423 0.800 125 918 10.1 1.36
21.865 4.0616 4.0716 0.480 44 762 3.5 1.23
22.965 3.8695 3.8790 0.200 207 702 16.7 2.08
26.635 3.3441 3.3523 0.160 86 520 7.0 0.69
27.575 3.2322 3.2401 0.240 130 488 10.5 1.65
31.620 2.8273 2.8343 0.140 1043 392 84.2 4.24
34.305 2.6119 2.6184 0.280 335 361 27.0 8.03
36.085 2.4871 2.4932 0.120 1239 353 100.0 3.24
42.785 2.1118 2.1170 0.120 66 313 5.3 1.16

Lampiran 23.
Spektrum XRD Nanokomposit Karet Alam/Bentonit-SDS

File: THE-8.DI 29-May-2013 14:44
=============================================================
=================


Tube anode: Cu


Number of peaks: 16

10.540 8.3866 8.4072 0.240 45 655 2.4 0.73
11.465 7.7119 7.7309 0.200 114 708 6.2 2.09
16.685 5.3091 5.3222 0.800 119 1176 6.4 0.64
17.780 4.9845 4.9968 0.640 196 1267 10.6 0.91
21.885 4.0580 4.0680 0.160 243 1109 13.2 1.77
23.025 3.8596 3.8691 0.160 1436 992 77.7 14.33
25.815 3.4484 3.4569 0.120 79 795 4.3 0.92
26.495 3.3614 3.3697 0.480 77 767 4.2 2.30
27.705 3.2173 3.2252 0.160 225 724 12.2 1.19
27.975 3.1869 3.1947 0.120 154 713 8.3 0.68
28.560 3.1229 3.1306 0.240 72 692 3.9 0.68
31.760 2.8152 2.8221 0.200 1537 590 83.1 21.62
34.375 2.6068 2.6132 0.240 515 552 27.9 8.46
36.250 2.4761 2.4822 0.160 1849 538 100.0 13.05
37.800 2.3781 2.3839 0.480 24 529 1.3 1.16
42.435 2.1284 2.1337 0.800 27 493 1.5 0.93

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Lampiran 1

DAFTAR KONVERSI AYAKAN DARI MESH KE MIKRON

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit

Universitas Sumatera Utara

Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-CTAB

Universitas Sumatera Utara

Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-PEG

Universitas Sumatera Utara

Data Hasil Analisis Uji Kestabilan Termal Nanokomposit Karet Alam/Bentonit-SDS

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Pos. Rel. Int. FWHM Area Height

Universitas Sumatera Utara

Universitas Sumatera Utara

Sample identification: Sampel 2

Diffractometer type: PW1710 BASED

Start angle [ø2é]: 5.000

Minimum peak tip width: 0.12

10.775 8.2042 8.2244 0.240 77 296 10.0 2.36

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Sample identification: Sampel 3

Diffractometer type: PW1710 BASED

Start angle [ø2é]: 5.000

Minimum peak tip width: 0.12

10.715 8.2500 8.2703 0.120 59 272 7.0 0.66

Universitas Sumatera Utara

Universitas Sumatera Utara

Sample identification: Sampel 1

Universitas Sumatera Utara

Diffractometer type: PW1710 BASED

Start angle [ø2é]: 5.000

Minimum peak tip width: 0.12

7.700 11.4723 11.5005 0.120 26 310 3.7 0.86

Universitas Sumatera Utara

Universitas Sumatera Utara

Universitas Sumatera Utara

Sample identification: Sampel 9

Diffractometer type: PW1710 BASED

Start angle [ø2é]: 5.000

Minimum peak tip width: 0.12

6.645 13.2911 13.3238 0.240 38 420 2.9 0.63

Universitas Sumatera Utara

Universitas Sumatera Utara

Sample identification: Sampel 5

Diffractometer type: PW1710 BASED

Start angle [ø2é]: 5.000

Minimum peak tip width: 0.12

Universitas Sumatera Utara

6.290 14.0404 14.0750 0.240 69 586 4.4 1.62

Universitas Sumatera Utara

Universitas Sumatera Utara