Modul AFR

LABORATORIUM PERMINYAKAN
PRAKTIKUM ANALISA FLUIDA RESERVOIR

Jurusan Teknik Perminyakan
Sekolah Tinggi Teknologi Minyak dan Gas Bumi
Balikpapan
Acara : Penentuan Kandungan Air dengan Dean & Stark Method

Hari/Tanggal :
Kelompok :
Asprak :
Tujuan Praktikum:
1. ......................................................................................................................................
2. ......................................................................................................................................
3. ......................................................................................................................................
4. ......................................................................................................................................
5. ......................................................................................................................................
Analisa:
DATA UMUM KELOMPOK
Volume Sampel (minyak ringan)

. . . . . . . . . . . . . ml . . . . . . . . . . . . . ml
Volume Solvent (kerosen)

. . . . . . . . . . . . . ml . . . . . . . . . . . . . ml
Volume Air Tertampung

. . . . . . . . . . . . . ml . . . . . . . . . . . . . ml
Persen kandungan air dalam sampel:
𝒗𝒐𝒍𝒖𝒎𝒆 𝒂𝒊𝒓
% 𝒌𝒂𝒅𝒂𝒓 𝒂𝒊𝒓 = × 𝟏𝟎𝟎 %
𝒗𝒐𝒍𝒖𝒎𝒆 𝒔𝒂𝒎𝒑𝒆𝒍
Kesimpulan Sementara:
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Balikpapan
Anggota Kelompok:
1. .....................................................
2. .....................................................
3. .....................................................
4. .....................................................
5. .....................................................
6. .....................................................
7. .....................................................
8. .....................................................
9. .....................................................
10. .....................................................
Balikpapan, ................................2018
Disetujui untuk laboratorium
Analisa Fluida Reservoir
Oleh
Asisten Praktikum
NILAI: ..........................
Balikpapan
Acara : Penentuan Kandungan Air dan Endapan (Base Sediment

&Water) dengan Centrifuge Method
Hari/Tanggal :
Kelompok :
Asprak :
Tujuan Praktikum:
1. ......................................................................................................................................
2. ......................................................................................................................................
3. ......................................................................................................................................
4. ......................................................................................................................................
5. ......................................................................................................................................
Analisa:
DATA UMUM KELOMPOK
Volume Sampel
. . . . . . . . . . . ml . . . . . . . . . . . ml
Lama Pemutaran
. . . . . . . . . . menit . . . . . . . . . . menit
Rotation Per Minute (RPM)

. . . . . . . . . RPM . . . . . . . . . RPM
Sampel Minyak I Sampel Minyak II

Parameter Analisa
Umum Kelompok Umum Kelompok
Volume Air (ml)
Volume Padatan (ml)
% BS & W
𝑽𝒐𝒍𝒖𝒎𝒆 𝑨𝒊𝒓 + 𝑽𝒐𝒍𝒖𝒎𝒆 𝑷𝒂𝒅𝒂𝒕𝒂𝒏

% 𝑩𝒂𝒔𝒆 𝑺𝒆𝒅𝒊𝒎𝒆𝒏𝒕 & 𝑊𝑎𝑡𝑒𝑟 = × 𝟏𝟎𝟎 %
𝑽𝒐𝒍𝒖𝒎𝒆 𝑺𝒂𝒎𝒑𝒆𝒍
Balikpapan
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Anggota Kelompok:
1. .....................................................
2. .....................................................
3. .....................................................
4. .....................................................
5. .....................................................
6. .....................................................
7. .....................................................
8. .....................................................
9. .....................................................
10. .....................................................
Balikpapan, ................................2018
Oleh
Asisten Praktikum
NILAI: ..........................
Balikpapan
Acara : Penentuan Specific Gravity

Hari/Tanggal :
Kelompok :
Asprak :
Tujuan Praktikum:
1. ......................................................................................................................................
2. ......................................................................................................................................
3. ......................................................................................................................................
4. ......................................................................................................................................
5. ......................................................................................................................................
Analisa:
DATA UMUM KELOMPOK
Volume Sampel
. . . . . . . . . . . ml . . . . . . . . . . . ml
Temperatur Sampel . . . . . oC . . . . . oF . . . . . oC . . . . . oF
Specific Gravity (SG) Sampel

......... .........
• Menghitung harga oAPI terukur

𝒐 𝟏𝟒𝟏. 𝟓
𝑨𝑷𝑰 𝑻𝒆𝒓𝒖𝒌𝒖𝒓 = − 𝟏𝟑𝟏. 𝟓 =. . . . . . . . . .. . dan. . . . . . . .. ..
𝑺𝑮𝒕𝒆𝒓𝒖𝒌𝒖𝒓
• Menghitung Koreksi oAPI pada 60/60 oF

𝒐
𝑨𝑷𝑰 𝒑𝒂𝒅𝒂 𝟔𝟎/𝟔𝟎 𝒐𝑭 = . . . . . .. . . . . dan . . . . . . . .
• Menghitung harga SG Koreksi pada 60/60 oF

𝟏𝟒𝟏. 𝟓
𝑺𝑮 𝟔𝟎/𝟔𝟎 𝒐𝑭 = =. . . . . . . . . dan . . . . . . . ..
𝟏𝟑𝟏. 𝟓 + 𝑨𝑷𝑰 𝟔𝟎/𝟔𝟎 𝒐𝑭
Balikpapan
• Berdasarkan data-data analisa, diperoleh harga faktor koreksi (fcorr) dari tabel
sebesar 0.00036 maka:
𝑺𝑮𝒕𝒓𝒖𝒆 = 𝑺𝑮𝟔𝟎 𝒐 + [𝒇𝒄𝒐𝒓𝒓 × (𝑻 − 𝟔𝟎𝒐𝑭)] =. . . . . . . . . dan. . . . . . ..

𝑭
𝟔𝟎
𝟏𝟒𝟏. 𝟓
𝒐
𝑨𝑷𝑰𝒕𝒓𝒖𝒆 = − 𝟏𝟑𝟏. 𝟓 =. . . . . . . . . . . . . .. . . dan . . . . . . . . . . . . ..
𝑺𝑮𝒕𝒓𝒖𝒆
Tabel Harga Koreksi oAPI

o o
API Terukur API 60/60 oF
29 27.5
30 28.5
31 29.5
32 30.5
33 31.5
34 32.5
35 33.5
36 34.5
37 35.5
38 36.5
39 37.5
40 38.5
41 39.5
42 40.5
43 41.5
44 42.5
45 43.5
46 44.5
47 45.5
48 46.5
Balikpapan
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Anggota Kelompok:
1. .....................................................
2. .....................................................
3. .....................................................
4. .....................................................
5. .....................................................
6. .....................................................
7. .....................................................
8. .....................................................
9. .....................................................
10. .....................................................
Balikpapan, ................................2018
Oleh
Asisten Praktikum
NILAI: ..........................
Balikpapan
Acara : Penetuan Titik Kabut (Cloud Point), Titik Beku (Freeze Point),
& TtitikTuang (Pour Point)
Hari/Tanggal :
Kelompok :
Asprak :
Tujuan Praktikum:
1. ......................................................................................................................................
2. ......................................................................................................................................
3. ......................................................................................................................................
4. ......................................................................................................................................
5. ......................................................................................................................................
Analisa:
Sampel
Parameter
Data Umum Data Kelompok
oC oF oC oF
K Rn K Rn
Titik Kabut
Titik Beku
Titik Tuang
Konversi:
9
( 𝑋 … … … °𝐶) + 32 = … … … °𝐹
5
Tugas:
1. Tabulasikan hasil penentuan titik kabut, titik beku, dan titik tuang setiap
kelompok dalam 1 tabel!
2. Plotkan masing-masing harga percobaan (Y) dengan kelompok praktikum (X)!
Balikpapan
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Anggota Kelompok:
1. .....................................................
2. .....................................................
3. .....................................................
4. .....................................................
5. .....................................................
6. .....................................................
7. .....................................................
8. .....................................................
9. .....................................................
10. .....................................................
Balikpapan, ................................2018
Oleh
Asisten Praktikum
NILAI: ..........................
Balikpapan
Acara : Penentuan Titik Nyala (Flash Point) & Titik Bakar (Fire Point)
Hari/Tanggal :
Kelompok :
Asprak :
Tujuan Praktikum:
1. ......................................................................................................................................
2. ......................................................................................................................................
3. ......................................................................................................................................
4. ......................................................................................................................................
5. ......................................................................................................................................
Analisa:
Sampel
Parameter
Data Umum Data Kelompok
oC oF oC oF
K Rn K Rn
Titik Nyala
Titik Bakar
Konversi:
9
( 𝑋 … … … °𝐶) + 32 = … … … °𝐹
5
Tugas:
1. Tabulasikan hasil penentuan titik nyala dan titik bakar setiap kelompok dalam 1
tabel!
2. Plotkan masing-masing harga percobaan (Y) dengan kelompok praktikum (X)!
Balikpapan
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Anggota Kelompok:
1. .....................................................
2. .....................................................
3. .....................................................
4. .....................................................
5. .....................................................
6. .....................................................
7. .....................................................
8. .....................................................
9. .....................................................
10. .....................................................
Balikpapan, ................................2018
Oleh
Asisten Praktikum
NILAI: ..........................
Balikpapan
Acara : Penentuan Viskositas Kinematik secara Coba-coba

Hari/Tanggal :
Kelompok :
Asprak :
Tujuan Praktikum:
1. ......................................................................................................................................
2. ......................................................................................................................................
3. ......................................................................................................................................
4. ......................................................................................................................................
5. ......................................................................................................................................
Analisa:
Viscometer Waktu Alir

Sampel Viscometer Konstanta
Kinematic (sekon)
Air I (25) VhA= 1.0038 TA = . . .

Kalibrasi
𝑽𝒉𝑨
pada suhu 𝑪𝑨 =
Minyak 𝑻
0 II (50) (Vh = CA x T1) T1 = . . . 𝑨
20 C Standar
=...
Minyak
I (50) (Vh1 = CA x T2A) T2A = . . .
Sampel 𝑽𝒉𝟏
Analisa =...
𝑪𝟐𝑨 =
𝑻 𝟐𝑨
Minyak
II (100) (Vh2 = C2A x T2B) T2B = . . .
Sampel
=...
1. Kalibrasi peralatan untuk menentukan koefisien viscometer (B):

Balikpapan
̅ ):
2. Konstanta Peralatan Keseluruhan (𝑪
3. Menghitung harga viskositas kinematik dengan ketentuan:

a. Jika harga (B/T2B) ≥ (0.001 x 𝑪̅x T) maka menggunakan persamaan
viscositas kinematik = 𝑪̅x T2B
. Jika harga (B/T2B) < (0.001 x 𝑪̅x T) maka menggunakan persamaan
b
viscositas kinematik = 𝑪̅x T2B– (B/T2B)
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Balikpapan
Anggota Kelompok:
1. .....................................................
2. .....................................................
3. .....................................................
4. .....................................................
5. .....................................................
6. .....................................................
7. .....................................................
8. .....................................................
9. .....................................................
10. .....................................................
Balikpapan, ................................2018
Oleh
Asisten Praktikum
NILAI: ..........................
Balikpapan
Acara : Analisa Kimia Air Formasi

Hari/Tanggal :
Kelompok :
Asprak :
Tujuan Praktikum:
1. ......................................................................................................................................
2. ......................................................................................................................................
3. ......................................................................................................................................
4. ......................................................................................................................................
5. ......................................................................................................................................
Analisa:
pH Air =............
Volume Sampel = ....................... cc
Konsentrasi ion CO3- = ....................... me/L
Konsentrasi ion OH- = ........................ me/L
Penentuan Sodium (Na+):

Tabulasi Hasil Analisa
Konsentrasi Anion Konsentrasi Kation
Anion BM Mg/L Me/ L(*) Kation BM Mg/L Me/L
Cl− 35,5 Ca++ 40
SO42− 96 Mg++ 24
2−
CO3 60 Fe+++ 56
HCO3− 61 Ba++ 137
OH− 17 Na+ 23
Anion Kation
Konversi mg/L ke me/L = ((mg/L) x valensi/BM)

Konversi Sodium (Na) = ƩAnion - ƩKation
=..................=............
Balikpapan
Buatlah Diagram Stiff – Davis
Perhitungan Indeks Stabilitas CaCO3
Konsentrasi Faktor Koreksi Ion Strength

Ion
Me/L x Koreksi
Me/L Me/L
Cl− 6  10−4
2-
SO4 1  10−3
2-
CO3 1,5  10−3
-
HCO3 5  10−3
Ca2+ 2  10−3
Mg2+ 1  10−3
Fe3+ 1,5  10−3
Ba2+ Negatif
Na+ 2  10−4
Σ Molar Ionic Strength
Balikpapan
Dari grafik diperoleh:

Tenaga Ion Keseluruhan (k) pada suhu:
Pada temperatur 0 C = .......
Harga pCa =.......

Harga pAlk =.......
Harga Indeks Stabilitas CaCO3 (SI) = pH – K – pCa – palk
Hitung harga SI pada tiap suhu yang ditetapkan, dan buat grafik hubungan antara SI (X)
dan Suhu (Y)!
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Balikpapan
Anggota Kelompok:
1. .....................................................
2. .....................................................
3. .....................................................
4. .....................................................
5. .....................................................
6. .....................................................
7. .....................................................
8. .....................................................
9. .....................................................
10. .....................................................
Balikpapan, ................................2018
Oleh
Asisten Praktikum
NILAI: ..........................
Balikpapan
Grafik Penentuan harga k pada CaCO3

Balikpapan
Grafik Penentuan harga pCa dan pAlk

Modul AFR

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LABORATORIUM PERMINYAKAN

PRAKTIKUM ANALISA FLUIDA RESERVOIR

Acara : Penentuan Kandungan Air dengan Dean & Stark Method

Volume Sampel (minyak ringan)

Volume Solvent (kerosen)

Volume Air Tertampung

Persen kandungan air dalam sampel:

Acara : Penentuan Kandungan Air dan Endapan (Base Sediment

Rotation Per Minute (RPM)

Sampel Minyak I Sampel Minyak II

Volume Padatan (ml)

𝑽𝒐𝒍𝒖𝒎𝒆 𝑨𝒊𝒓 + 𝑽𝒐𝒍𝒖𝒎𝒆 𝑷𝒂𝒅𝒂𝒕𝒂𝒏

Acara : Penentuan Specific Gravity

DATA UMUM KELOMPOK

Specific Gravity (SG) Sampel

• Menghitung harga oAPI terukur

• Menghitung Koreksi oAPI pada 60/60 oF

• Menghitung harga SG Koreksi pada 60/60 oF

𝑺𝑮𝒕𝒓𝒖𝒆 = 𝑺𝑮𝟔𝟎 𝒐 + [𝒇𝒄𝒐𝒓𝒓 × (𝑻 − 𝟔𝟎𝒐𝑭)] =. . . . . . . . . dan. . . . . . ..

Tabel Harga Koreksi oAPI

Acara : Penentuan Viskositas Kinematik secara Coba-coba

Viscometer Waktu Alir

Air I (25) VhA= 1.0038 TA = . . .

1. Kalibrasi peralatan untuk menentukan koefisien viscometer (B):

3. Menghitung harga viskositas kinematik dengan ketentuan:

Acara : Analisa Kimia Air Formasi

Penentuan Sodium (Na+):

Anion BM Mg/L Me/ L(*) Kation BM Mg/L Me/L

Cl− 35,5 Ca++ 40

HCO3− 61 Ba++ 137

Konversi mg/L ke me/L = ((mg/L) x valensi/BM)

Buatlah Diagram Stiff – Davis

Perhitungan Indeks Stabilitas CaCO3

Konsentrasi Faktor Koreksi Ion Strength

Dari grafik diperoleh:

Harga pCa =.......

Grafik Penentuan harga k pada CaCO3

Grafik Penentuan harga pCa dan pAlk

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