MEMBUAT DESAIN PENELITIAN

FACTORIAL DESIGN
3 FAKTOR 2 LEVEL
RENTANG
NO FAKTOR UNIT
-1 +1
1 speed 10 20 rpm
2 lama 30 50 menit
3 suhu 50 80 oC

1. Buatlah desain penelitian full factorial design!

2. Buatlah desain penelitian 1/2 fractional factorial design!

3 FAKTOR 3 LEVEL
NO FAKTOR
1 A
2 B
3 C

1. Buatlah desain penelitian general factorial design dengan level bertanda 1, 2, dan 3!

PLACKETT-BURMAN DESIGN
1. Buatlah desain penelitian Plackett-Burman design untuk 3 faktor dengan 12 run

RESPONSE SURFACE DESIGN

CENTRAL COMPOSITE
3 FAKTOR
RENTANG
NO FAKTOR UNIT
-1 +1
1 speed 10 20 rpm
2 lama 30 50 menit
3 suhu 50 80 oC

1. Buatlah desain penelitian response surface design central composite cube points
2. Buatlah desain penelitian response surface design central composite axial points

BOX-BEHNKEN
1. Buatlah desain penelitian response surface design Box-Behnken dengan data sama dengan di atas

MIXTURE DESIGN
3 KOMPONEN
RENTANG
NO FAKTOR UNIT
0 1
1 Stearic acid 0 90 %
2 Stearyl alcohol 0 90 %
 3 Triethanolamine 0 90 %

1. Buatlah desain penelitian mixture design simplex centroid

2. Buatlah desain penelitian mixture design simplex lattice
3. Buatlah desain penelitian mixture design extreme vertices

4 KOMPONEN
RENTANG
NO FAKTOR UNIT
0 1
1 MCC 0 80 %
2 Starch X 0 80 %
3 DiCaFos 0 80 %
4 Povidone 0 80 %

1. Buatlah desain penelitian mixture design simplex centroid

2. Buatlah desain penelitian mixture design simplex lattice
3. Buatlah desain penelitian mixture design extreme vertices

TAGUCHI DESIGN
RENTANG
NO FAKTOR UNIT
-1 +1
1 speed 10 20 rpm
2 lama 30 50 menit
3 suhu 50 80 oC

1. Buatlag desain penelitian Taguchi design L4

2. Buatlag desain penelitian Taguchi design L8
3. Buatlag desain penelitian Taguchi design L12
SCREENING

MAIN EFFECT
C1 C2 C3 C4 C5 C6 C7
Spray rate Atomization Fluidization Inlet temp Product temp Outlet temp Gun distance
2 1 50 55 25 45 5
2 3 100 45 35 45 5
8 1 100 55 25 45 5
8 3 50 55 35 45 3
8 3 50 45 25 45 3
8 1 100 55 35 35 3
2 1 100 45 35 45 3
2 3 50 55 35 35 5
8 3 100 45 25 35 5
2 3 100 55 25 35 3
8 1 50 45 35 35 5
2 1 50 45 25 35 3

Bisa dicoba dengan membuat desain penelitian dengan Plackett Burman design
RENTANG
NO FAKTOR
-1 +1
1 Spray rate 2 8
2 Atomization 1 3
3 Fluidization 50 100
4 Inlet temp 45 55
5 Product temp 25 35
6 Outlet temp 35 45
7 Gun distance 3 5
8 Nr sprayer 1 3
9 Bag porosity 20 40
10 Clean freq 2 10
11 Bowl occu 40 60

Tentukan faktor berpengaruh dominan menggunakan cara:

1. ANOVA Main effect
2. DOE Pareto plot
3. ANOVA data
 C8 C9 C10 C11 C12 C13
Nr sprayer Bag porosity Clean freq Bowl occu Agglomerate Fines
1 40 10 60 4 15
1 20 2 60 2 18
3 20 2 40 16 5
1 20 10 40 12 7
3 40 2 60 13 8
1 40 2 60 14 7
3 40 10 40 3 16
3 40 2 40 2 19
1 40 10 40 11 8
3 20 10 60 1 18
3 20 10 60 18 2
1 20 2 40 5 14
OPTIMISASI DAN DESIGN SPACE

FACTORIAL DESIGN
C1 C2 C3 C4 C5
RUN/ ROW x1 x2 Yield Visco MolWt
1 80 170 76.5 62 2940
2 80 180 77.0 60 3470
3 90 170 78.0 66 3680
4 90 180 79.5 59 3890
5 85 175 79.9 72 3480
6 85 175 80.3 69 3200
7 85 175 80.0 68 3410
8 85 175 79.7 70 3290
9 85 175 79.8 71 3500
10 92.07 175 78.4 68 3360
11 77.93 175 75.6 71 3020
12 85 182.07 78.5 58 3630
13 85 167.93 77.0 57 3150

Tampilkan grafik respons secara:

1. Contour plot
2. Surface plot

DESIGN SPACE
Tentukan design space menggunakan Overlaid Contour plot, dengan expected responses:
MolWt : 2800 – 3400
Visco : 64 – 66
Yield : 77 - 80

RESPONSE OPTIMIZER
Lakukan response optimization dengan:
Respons Goal Low Target High Weight Importance
MolWt do not optimize
Visco minimize 57 57 72 1 1
Yield maximize 75.6 80.3 80.3 1 1

Respons Goal Low Target High Weight Importance

MolWt do not optimize
Visco minimize 60 60 70 1 1
Yield maximize 76 80 80 1 1

MIXTURE DESIGN
C1 C2 C3 C4 C5 C6 C7
Run/ Row Sterol Stecid TEA Sebar Lekat Visko StdOrder
1 90 0 0 4.48 0.463 45.5 1
 2 0 90 0 5.10 0.430 38.6 2
3 0 0 90 8.00 0.343 6.3 3
4 45 45 0 4.65 0.473 41.2 4
5 0 45 45 6.10 0.420 13.3 5
6 45 0 45 6.90 0.413 10.6 6
7 30 30 30 5.35 0.430 31.7 7
8 90 0 0 4.50 0.490 44.2 8
9 0 90 0 5.00 0.423 37.8 9
10 0 0 90 8.20 0.357 6.5 10
11 45 45 0 4.60 0.447 42.5 11
12 0 45 45 6.05 0.433 11.5 12
13 45 0 45 6.85 0.430 11.0 13
14 30 30 30 5.30 0.443 30.8 14
15 90 0 0 4.50 0.487 45.3 15
16 0 90 0 5.08 0.417 39.1 16
17 0 0 90 7.93 0.347 6.2 17
18 45 45 0 4.55 0.467 42.3 18
19 0 45 45 6.10 0.407 15.2 19
20 45 0 45 6.85 0.427 9.5 20
21 30 30 30 5.35 0.413 31.5 21

Tampilkan grafik respons secara:

1. Contour plot
2. Surface plot

DESIGN SPACE
Tentukan design space menggunakan Overlaid Contour plot, dengan expected responses:
Daya sebar : 5,5 – 6,5
Daya lekat : 0,41 – 0,44
Viskositas : 15 – 25

RESPONSE OPTIMIZER
Lakukan response optimization dengan:
Respons Goal Low Target High Weight Importance
Sebar maximize 0 5 1 1
Lekat maximize 0 0.3 1 1
Visko maximize 0 25 1 1
 C8 C9 C10
RunOrder Blocks PtType
1 1 1
 2 1 1
3 1 1
4 1 1
5 1 1
6 1 1
7 1 1
8 1 1
9 1 1
10 1 1
11 1 1
12 1 1
13 1 1
14 1 1
15 1 1
16 1 1
17 1 1
18 1 1
19 1 1
20 1 1
21 1 1