Index: Elspun Ndia Imited

WELSPUN WORK INSTRUCTION MANUAL
INDIA LIMITED INDEX

Doc. No.
P/No. 1 Of
PAGE
SR.NO DOC. NO TITLE NO
1 Shade Development Flow Chart
WIL/RUGS/SOP-
2 D00001 PVA Checking 1
WIL/RUGS/SOP-
3 D00002 Direct Dye Dyeing 2
WIL/RUGS/SOP-
4 D00003 Reactive Dye Dyeing 3
WIL/RUGS/SOP-
5 D00004 Acid Dye Dyeing 4
WIL/RUGS/SOP-
6 D00005 Dye Testing Of Direct Dye 5
WIL/RUGS/SOP-
7 D00006 Dye Testing Of Reactive Dye 6
WIL/RUGS/SOP-
8 D00007 Dye Testing Of Acid Dye 7
9 Physical Testing
WIL/RUGS/SOP-
10 P00001 Colour Fastness To Crocking AATCC 8 2007 8
WIL/RUGS/SOP-
11 P00002 Colour Fastness To Rubbing ISO 105 X 12 9
WIL/RUGS/SOP-
12 P00003 Colour Fastness To Washing ISO 105/C06 (C2S) 10
WIL/RUGS/SOP-
13 P00004 Colour Fastness To Washing AATCC 61 2A 11
WIL/RUGS/SOP-
14 P00005 Colour Fastness To Washing AATCC 61 3A 12
WIL/RUGS/SOP- Domestic Washing And Drying Procedure ISO 6330 2000-12-
15 P00006 15 13
WIL/RUGS/SOP-
16 P00007 Domestic Washing And Drying Procedure AATCC 150 2003 14
WIL/RUGS/SOP-
17 P00008 Dimensional Change Of Fabric AATCC 135 2004 15
WIL/RUGS/SOP-
18 P00009 Colour Fastness To Washing ISO 105/C03 16
WIL/RUGS/SOP-
19 P00010 Colour Fastness To Chlorinated Water ISO 105 E03 17
WIL/RUGS/SOP- Colour Fastness To Chlorinated Pool Water AATCC 162
20 P00011 2002 18
WIL/RUGS/SOP- Bleach Safe Test (As per AATCC 150 Adding Chemical As
21
P00011a Per In-house Method) 19
WIL/RUGS/SOP-
22 P00012 Absorbency By Drop Method AATCC 79 20
WIL/RUGS/SOP-
23 P00013 Colour Fastness To Light ISO 105 B01 21
WIL/RUGS/SOP-
24 P00014 Surface Water Absorption ASTM D 4772 22
25 WIL/RUGS/SOP- Colour Fastness To Perspiration ISO 105 E04 23
P00015
WIL/RUGS/SOP-
26 P00016 Colour Fastness To Perspiration AATCC 15 2007 24
WIL/RUGS/SOP-
27 P00017 Colour Fastness To Water AATCC 107 2007 25
WIL/RUGS/SOP-
28 P00018 Colour Fastness To Water ISO 105 E01 26
WIL/RUGS/SOP-
29 P00019 Colour Fastness To Migration in To PVC ISO 105 X 10 27
WIL/RUGS/SOP-
30 P00020 Colour Fastness To Sea Water AATCC 106 2007 28
WIL/RUGS/SOP-
31 P00021 Colour Fastness To Sea Water ISO 105 E02 29
32 Chemical Testing
WIL/RUGS/SOP-
33 C00001 Chemical Testing General 30
WIL/RUGS/SOP-
34 C00002 Specification Of Chemicals (Basic Chemicals) 31
WIL/RUGS/SOP-
35 C00003 Specification Of Chemicals 32
WIL/RUGS/SOP-
36 C00004 Specification Of Chemicals( Auxiliaries) 33
WIL/RUGS/SOP-
37 C00005 Testing Method For Acetic Acid 34
WIL/RUGS/SOP-
38 C00006 Testing Method For Soda Ash 35
WIL/RUGS/SOP-
39 C00007 Testing Method For Sodium Hydroxide 36
WIL/RUGS/SOP-
40 C00008 Testing Method For Sodium Hypo chloride 37
WIL/RUGS/SOP-
41 C00009 Testing Method For Sodium Hydrosulphite 38
WIL/RUGS/SOP-
42 C00010 Testing Method For Neutra Acid/Heptol EMG 39
WIL/RUGS/SOP-
43 C00011 Testing Method For Glauber Salt(Sodium Sulphate) 40
WIL/RUGS/SOP-
44 C00012 Testing Method For Total Hardness Of Water 41
WIL/RUGS/SOP-
45 C00013 Testing Method For pH Calibration 42
46
47
48
49
50
PREPARED BY : - Welspun India AUTHORISED BY : -

Limited
JAY A. NAIK R.K.BERA
ISSUE :- 31/08/2008
WORK INSTRUCTION MANUAL
WELSPUN Doc. No.
WIL/RUGS/SOP-P000
INDIA COLOUR FASTNESS TO CROCKING
AATCC-8 2007
LIMITED P/No. 1 Of
1) Apparatus:- Crock meter, White cotton cloth, Grey scale for

Staining, White AATCC Textile Blotting paper
2) Specimen Size: 15 cm x 10 cm
3) Procedure: A) Dry Crocking
B) Wet Crocking
A) Dry Crocking:
(1) Fix the test specimen in the insert of crock meter.

(2) Mount the dry cotton cloth on the fingertip of the crock meter.
(3) Give 10 complete [20] turns.
(4) Remove the cotton cloth from the fingertip.
B) Wet Crocking:
(1) Fix the test specimen in the insert of crock meter.

(2) Wet the cotton cloth in distilled water (wet pick-
up to 65 + 5%).
(3) Mount the wet cotton cloth on the finger tip of the
Crock meter.
(4) Give 10 complete [20] turns.
(5) Remove the cotton cloth from the fingertip.
Evaluation: Evaluation the rating with Grey scale for staining.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOCOLOR FASTNESS TO RUBBING

ISO-105 X 12
Doc. No.
WIL/RUGS/SOP-P000
P/No. 1 Of
1) Apparatus :- Crockmeter,cotton rubbing cloth,grey scale for staining

ISO 105 A03
2) Specimen Size: 14 cm x 5 cm
3) Procedure: A) Dry Crocking
B) Wet Crocking
A) Dry Rubbing:
(1) Fix the test specimen (Fabric/Yarn) on Crock meter by

Clamps in the long direction.
(2) Fix the dry Bleached rubbing cloth on the finger tip of
The crock meter.
(3) Rub to and fro in a straight line along a track with force of 9 N
for 10 times.
(4) Take out the dry rubbing cloth from device.
(5) Check the rubbing fastness by Grey Scale.
B) Wet Rubbing:
(1) Fix the test specimen (Fabric/Yarn) on Crock meter by

clamps in the long direction.
(2) Fix the wet Bleached rubbing cloth (wet pick up 100+-
5%) on the finger tip of the crock meter
(3) Rub to and fro in a straight line along a track with force
of 9 N for 10 times.
(4) Take out the wet rubbing cloth from device and dry at
room temperature.
(5) Check the rubbing fastness by Grey Scale.

Limited
ISSUE :- 31/08/2008

COLOR FASTNESS TO WASHING Doc. No.
INDIA LIMITED
WIL/RUGS/SOP-P000
ISO 105/C06 (C2S)

P/No. 1 Of
1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre, Grey Scale

for staining (ISO 105 A03), Grey scale for color change (ISO 105
A02)
2. Chemical: - ECE Detergent, Sodium Perborate
3. Specimen Size:- 4 cm X 10 cm
4. Test Procedure:
(1) Prepare 4 g/l ECE Detergent + 1 g/l Sodium Perborate

(2) Cut the specimen in size 4 cm X 10 cm.
(3) Stitch the multifibre fabric on the specimen.
(4) Preheat the machine to 600C + 2 temp.
(5) Pour 50 ml solution of detergent in the steel beaker.
(6) Put the specimen in the steel beaker and add 25 steel
balls in it.
(7) Lock the steel beaker in the Laundrometer.
(8) Start the cycle as set on the machine that is at 60 0C for
30 min.
(10) After the completion of the cycle, remove the specimen
and wash one minute with tap water.
(11) Dry the specimen with multifibre at 600C.
(12) Condition it for 30 min.
Evaluation: Evaluate the rating of staining and color change with Grey scale.

Limited
ISSUE :- 31/08/2008

Doc. No.
INDIA LIMITED
WIL/RUGS/SOP-P000
COLOR FASTNESS TO WASHING

AATCC 61 2A 2003
P/No. 1 Of
1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre No -10, Grey

Scale for staining (ISO 105 A03), Grey scale for color change
(ISO 105 A02)
2. Chemical: - AATCC WOB Detergent, Sodium Perborate
4. Test Procedure:
(1) Prepare 1.5 g/l Detergent (WOB) Solution.

(4) Preheat the machine to 490C if not at this temp.
(5) Pour 150 ml solution of WOB detergent in the steel
beaker.
balls in it.
(7) Lock the steel beaker and put in the Launder-Ometer.
45 min.
and wash 3 times with distilled water.
(11) Brush the specimen to orient the terry in test sample
direction.
(12) Condition it at 210C and RH 65+-2% for 60 min.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOR FASTNESS TO WASHING

Doc. No.
WIL/RUGS/SOP-P000
AATCC 61 3A 2003
P/No. 1 Of
1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre No -10, Grey

Scale for staining (ISO 105 A03), Grey scale for color change
(ISO 105 A02)
2. Chemical: - AATCC WOB Detergent, Sodium Perborate
4. Test Procedure:
(1) Prepare 1.5 g/l Detergent (WOB) Solution.

(4) preheat the machine to 710C if not at this temp.
(5) Pour 50 ml solution of WOB detergent in the steel
Beaker.
balls in it.
(7) Lock the steel beaker and put in the Launder-Ometer.
45 min.
and wash 3 times with distilled water.
(10) Dry the specimen with multifibre at 60-710C.
(11) Brush the specimen to orient the terry in test sample
direction.
(12) Condition it at 210C and RH 65+-2% for 60 min.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED DOMESTIC WASHING AND DRYING PROCEDURE

Doc. No.
WIL/RUGS/SOP-P000
ISO 6330 2000-12-15
P/No. 1 Of
1. Apparatus :- Automatic Washing M/c(Front/Top Loading),Tumble dryer,

Conditioning Racks, Measuring Tape
2. Chemical: - WOB Detergent,
3. Specimen Size:- Full Rug
4. Test Procedure:
(1) Take the Rug on the table and take the measurement in
Lengthwise & widthwise.
(2) Put the sample in automatic washing machine.
(3) Set the machine at Normal or Delicate for washing as
per care instruction.
(4) Add 66 gm WOB detergent powder.
(5) Start the washing machine and complete the washing
cycle.
(6) Place the sample with load in the tumble dryer and dry
it.
(7) Condition the dry sample for at least 4hrs.Take the
measurement lengthwise & widthwise.
Evaluation : Evaluate the shrinkage lengthwise, widthwise and border wise

shrinkage using formula as given below and compare it with the
norm.
% Shrinkage = (Original Dimension – Washed Dimension) x100
Original Dimension

Limited
ISSUE :- 31/08/2008
INDIA LIMITED DOMESTIC WASHING AND DRYING PROCEDURE

Doc. No.
WIL/RUGS/SOP-P000
AATCC-150 2003
P/No. 1 Of
1. Apparatus :- Automatic Washing M/c(Top Loading),Tumble dryer,

2. Chemical: - AATCC WOB Detergent,
4. Test Procedure:
Lengthwise & widthwise.
(4) Add 66 gm AATCC detergent powder.
cycle.
it.
measurement lengthwise & widthwise.

norm.
Original Dimension

Limited
ISSUE :- 31/08/2008
INDIA LIMITED DIMENTIONAL CHANGE OF FABRIC

Doc. No.
WIL/RUGS/SOP-P000
AATCC-135 2004
P/No. 1 Of

2. Chemical: - AATCC WOB Detergent,
4. Test Procedure:
Lengthwise & widthwise (Top-Center-Bottom).
(4) Add 66 gm AATCC detergent powder.
cycle.
it.
Measurement lengthwise & widthwise.
norm.
Original Dimension

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOR FASTNESS TO WASHING

Doc. No.
WIL/RUGS/SOP-P000
ISO 105/C03
P/No. 1 Of

A02)
2. Chemical: - ECE Detergent, Soda Ash
4. Test Procedure:
(1) Prepare 5 g/l ECE Detergent + 2 g/l Soda Ash

(4) Preheat the machine to 600C + 2 temp.
(5) Pour 50 ml solution of detergent in the steel beaker.
(6) Put the specimen in the steel beaker
(7) Lock the steel beaker in the Laundrometer.
30 min.
and wash 10 minute with tap water.
(11) Condition it for 30 min.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOR FASTNESS TO CHLORINATED WATER

Doc. No.
WIL/RUGS/SOP-P000
ISO 105 E03
P/No. 1 Of

A02), pH meter
2. Chemical: - Sodium Hypo chlorite, Distilled Water, Potassium di-
hydrogen phosphate, Disodium hydrogen phosphate
Dihydrate or disodium hydrogen phosphate decahydrate
4. Test Procedure:
(1) Prepare solution from sodium hypo chlorite 20mg/l,

50mg/l, 100 mg/l and pH 7.5
(2) 14.35 gpl (KH2PO4), 20.05 gpl (Na2HPO4.2H2O)
(3) Take above solution in steel beaker at the ratio of 100:1
(4) Put the test specimen in this solution and close the steel
beaker with container.
(5) Put steel beaker in Laundrometer at 27 0c+2. Run 1hrs.
(6) Remove the specimen and squeeze and dry it by
hanging it in air at room temperature.
Evaluation: Evaluate the rating with Grey scale for colour change.
Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOR FASTNESS TO

CHLORINATED POOL WATER
Doc. No.
WIL/RUGS/SOP-P000
AATCC 162 2002
P/No. 1 Of
1. Apparatus :- Cylinder, Grey Scale for staining , Grey scale for

color change , pH meter
2. Chemical: - Sodium Hypochlorite, Calcium Chloride, Magnesium

Chloride, Acetic Acid and Distilled Water
3. Specimen Size:- 6 cm X 6 cm Weight should be 5.0 + 0.25 gm
4. Test Procedure:
(1) Prepare Hard Water with 8.24 g/l Calcium Chloride +
5.07 g/l Magnesium Chloride.
(2) Take 50 ml of above solution and make it 5000ml.
Add
0.5ml Sodium Hypochlorite (5% Available Cl2) in it. The
available Chlorine required for this test 5ppm.
(3) Adjust pH 7.0 with Acetic Acid.
(4) Put the test specimen in the above solution for 60 min at
Room temperature.
(5) Remove the specimen and squeeze it to remove the
water.
(6) Rinse it with distilled water.
(7) Remove it and dry it by hanging in air at room
Temperature.
Evaluation: Evaluate the rating with Grey scale for colour change.
Limited
ISSUE :- 31/08/2008
INDIA LIMITED ABSORBENCY BY DROP METHOD

Doc. No.
AATCC 79 WIL/RUGS/SOP-P000
P/No. 1 Of
1. Apparatus :- Embroidery Hoop (6 Inch) or more diameter, Burette, Stopwatch

Burette Stand
2. Chemical: - Water
3. Test Procedure:
(1) Specimen condition at 65 + 2% Relative Humidity.

(2) Mount the Specimen in the Embroidery hoop.
Then place the hoop about 10 mm below the tip
of the burette.
(3) Then allow one drop of distilled water at 21°c
to fall on the embroidery cloth.
(4) At that time start the stopwatch when one drop
of water touch the surface and stop the stop watch
when disappear of water
(5) Take at least five readings.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOUR FASTNESS TO LIGHT

Doc. No.
ISO 105 B01 WIL/RUGS/SOP-P000
P/No. 1 Of
1. Apparatus :- Light Fastness tester, Blue Wool Standard

2. Specimen Size: - 50 mm x 50 mm
3. Test Procedure:
(1) Stick the test specimen on the pieces of card.

(2) The card is placed with other rectangular specimen holder.
(3) It’s top is covered with spring to keep sample stripe in place.
(4) Insert the specimen holder in glass cage. And put the rubber
rectangular cap on the glass cage.
(5) Start the electric supply till temperature inside the instrument
reached about 400C.
(6) Start the water supply.
(7) Start the timer set it 60 hours.
(8) Remove the specimen after 60 hours.
Evaluation: Evaluation the rating with the blue wool standard.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED SURFACE WATER ABSORPTION

Doc. No.
WIL/RUGS/SOP-P000
ASTM D 4772
P/No. 1 Of
1. Apparatus :- Embroidery Hoop (6 Inch) or more diameter, Stopwatch

Water Flow Tester, Base, PAN, Measuring cylinder of 50ml
2. Chemical: - Distilled Water
3. Test Procedure:
(1) Specimen condition at 65+-2% Relative Humidity.

(2) Mount the Specimen in Embroidery hoop.
(3) Mount the Specimen on the base.
(4) Then adjust the Flow water tester away from
specimen 3.0 + 0.2 cm.
(5) Then push the Pan against the base so all the water
goes in the PAN.
(6) Pour 50 ml water by measuring cylinder in Funnel,
attached with Flow Water Tester and allow 25 + 5
sec. Full water coming out at 60 angles.
(7) All the water not absorbed by the specimen
remaining water goes in to the pan.
Calculation:
Surface water Absorbency % = 50ml water – Remaining water in

pan/ 50*100

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOUR FASTNESS TO PERSPIRATION

Doc. No.
WIL/RUGS/SOP-P000
ISO 105 E04
P/No. 1 Of
1. Apparatus :- Perspiration Tester, Plastic Plates, Oven, Multifibre,
Weight, Grey Scale for Color change, Grey Scale for Staining,
pH meter.
2. Chemical: - Distilled Water, Sodium Chloride, L-Histidine
Monohydrochloride Mono hydrate (C6H9O2N2.HCl.H2O)
Disodium hydrogen orthophosphate decahydrate or
disodium hydrogen orthophosphate dihydrate.
3. Specimen size: 4 cm X 10 cm
4. Test Procedure:
A) (ALKALINE METHOD)
a) Prepare 0.5 g/l L- Histidine Monohydrochloride Mono
hydrate C6H9O2N2.HCl.H2O) + 5 g/l Sodium Chloride +
2.5 g/l Disodium Hydrogen Orthophosphate
(Adjust pH 8 with 0.1 N sodium Hydroxide Solution)
B) (ACID METHOD)
b) Prepare 0.5 g/l L- Histidine Monohydrochloride
Monohydrate (C6H9O2N2.HCl.H2O) +5 g/l Sodium
Chloride + 2.2 g/l Sodium di-hydrogen Orthophosphate.
(Adjust pH 5.5 with 0.1 N Hydrochloric Acid Solution)
(1) Stitched the Multifibre on the specimen.

(2) Put this stitched specimen in the Alkaline Medium
Solution or Acid Medium Solution for 30 min at room
temperature at ratio of 50:1
(3) Remove the specimen and squeeze it.
(4) Place the squeezed specimen between two plastic plates
in perspiration tester.
(5) Apply 12.5-kpa pressure on the specimen.
(6) Put the perspiration tester in the oven at 37°c + 2°c for
4hrs.
(7) Remove the specimen from the oven and dry it by
hanging in air at a temperature not exceeding 60°c.

Limited
ISSUE :- 31/08/2008
Evaluation: Evaluate the rating with Grey scale.
INDIA LIMITED COLOUR FASTNESS TO PERSPIRATION

Doc. No.
WIL/RUGS/SOP-P000
AATCC 15 2007
P/No. 1 Of
1. Apparatus :- Perspiration Tester, Plastic Plates, Oven, Multifibre No.10,

pH meter.
2. Chemical: - Distilled Water, Sodium Chloride, Lactic Acid, L-
Histidine Monohydrochloride Sodium phosphate
dibasic anhydrous
3. Specimen size: 60 + 2 mm X 60 + 2 mm
4. Test Procedure:
(A) ALKALINE METHOD

(a) Prepare 10 g/l Sodium Chloride + 4 g/l ammonium
Chloride+1.25 g/l Disodium Hydrogen Phosphate Anhydrous +
0.25 g/l L-histidine monohydrochloride.
(Adjust pH 8 with 0.1 N sodium Hydroxide Solution)
(B) ACIDIC METHOD
(b) Prepare 10 g/l Sodium Chloride + 1 g/l Lactic acid + 1 g/l
Disodium Hydrogen Phosphate anhydrous + 0.25 g/l L-
Histidine mono hydrochloride.
(Adjust pH 4.5 with 0.1 N Hydrochloric Acid Solution)
(1) Cut the specimen of specific size and mount with

Multifibre fabric.
(2) Put the this mounted specimen in perspiration solution
for 30 + 2 min. with occasional stirring.(Each specimen
To be weight 2.25 + 0.5 times of original)
(3) Remove the specimen and squeeze it.
(4) Place the squeezed specimen between two plastic plates in
perspiration tester.
(5) Apply 4.54 KG pressure on the specimen.
(6) Put the perspiration tester in the oven at 380c + 1°c for
6 Hrs.
(8) Remove the specimen from the oven and dry it on the
Line dryer at room temp.
Evaluation: Evaluate the rating with Grey scale for staining.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOUR FASTNESS TO WATER

Doc. No.
WIL/RUGS/SOP-P000
AATCC 107 2007
P/No. 1 Of

pH meter.
2. Chemical: - Distilled Water,
4. Test Procedure:
(1) Cut the specimen of specific size and mount with multifibre
fabric.
(2) Put this mounted specimen in distilled water for 15 min at
room temp with occasional stirring.
(3) Remove the specimen and squeeze it. (Wet the specimen is
more then 3 times its dry weight)
(4) Place the squeezed specimen between two plastic plates in
perspiration tester.
(5) Apply 4.5 kg. pressure on the specimen.
(6) Put the perspiration tester in the oven at 380C for 18 Hrs.
(7) Remove the specimen from the oven and dry it by hanging in
air at room temp.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOUR FASTNESS TO WATER

Doc. No.
WIL/RUGS/SOP-P000
ISO 105 E01
P/No. 1 Of

pH meter.
2. Chemical: - Distilled Water,
3. Specimen size: 4.0 cm. X 10.0 cm.
4. Test Procedure:
(1) Cut the specimen of specific size and mount with

multifibre fabric.
(2) Put this mounted specimen in distilled water for 15 min
at room temp with occasional stirring.
(3) Remove the specimen and squeezes it.
(4) Place the squeezed specimen between two plastic
plates in perspiration tester.
(6) Put the perspiration tester in the oven at 370C for 4 Hrs.
hanging in air at room temp.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOUR FASTNESS TO MIGRATION Doc. No.

IN TO PVC WIL/RUGS/SOP-P000
ISO 105 X 10
P/No. 1 Of
1. Apparatus :- Perspiration Tester, Plastic Plates, Oven, Watch Glass

Grey Scale for Color change, Grey Scale for Staining,
pH meter.
2. Chemical: - Polyvinyl Chloride Powder,Dioctyle Phtalate(Plasticizer),
Petroleum ether
4. Test Procedure
(1) Take some amount of Polyvinyl chloride Powder in watch

glass and add Dioctyle Phthalate and paste it by glass rod
and make a film by gelled in oven at 1700C for 10 min.
(2) Put the specimen on the film.
(3) Place the specimen and film between two plates in
Perspiration Tester
(4) Apply 4.5 kg pressure on the specimen.
(5) Put the perspiration Tester in the oven at 800C for 3.5 Hrs.
(6) Remove the test sample from the PVC film and rinse the
film with Petroleum Ether and Dry it.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOUR FASTNESS TO SEA WATER

Doc. No.
WIL/RUGS/SOP-P000
AATCC 106 2007
P/No. 1 Of
1. Apparatus :- Perspiration Tester, Plastic Plates, Oven, Multifibre No.10

pH meter.
2. Chemical: - Distilled water, Sodium Chloride, Magasium Chloride
Petroleum ether
4. Test Procedure
(1) Prepare 30g/l Sodium Chloride + 5 g/l Magnesium
Chloride.
(2) Cut the specimen of specific size and stitch with
Multifibre fabric.
(3) Put this stitched specimen in sea water for 15 min
(4) Remove the specimen and squeezes it. (Wet the weight
of the specimen is more then 3times of original
weight)
(7) Put the perspiration tester in the oven at 380 +1°C for 18
hrs.
Hanging in air at room temp.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED COLOUR FASTNESS TO SEA WATER

Doc. No.
WIL/RUGS/SOP-P000
ISO 105 E02
P/No. 1 Of
1. Apparatus :- Perspiration Tester, Plastic Plates, Oven, Multifibre No.10

pH meter.
2. Chemical: - Distilled water, Sodium Chloride,
Petroleum ether
4. Test Procedure
(1) Prepare 30g/l Sodium Chloride Solution.

(2) Cut the specimen of specific size and stitch with
Multifibre fabric.
(3) Put this stitched specimen in sea water for 15 min
(4) Remove the specimen and squeezes it.
(6) Apply 12.5-kpa pressure on the specimen.
(7) Put the perspiration tester in the oven at 37 0C for 4
Hrs.
hanging in air at room temp.

Limited
ISSUE :- 31/08/2008
INDIA LIMITEDPettry CHEMICAL TESTING

Doc. No.
WIL/RUGS/SOP-C000
P/No. 1 Of
1. Apparatus :- Pettry Dish, Oven, Beaker , pH meter, Glass Rod

2. Chemical: - Distilled Water
3. Type Of Test : - A) Physical Appearance
pH Value Of 1% Solution
B) Solid Content
4. Procedure : -
A) Physical Appearnace:
Physical appearance is observed as per state at room temperature.
B) pH Value :
i) Make 1% solution of the sample
ii) Put the pH electrod in to the solution & take the pH reading of the solution.
C) Solid Content
i) Weigh approx. 2 gm. Of a sample in pettry disk & note down.
ii) Keep it in the oven at 1000 C (+/- 2) for 3 hrs.
iii) Take it out from the oven & keep it out side for cooling for some times &
weigh the residue.
iv) Calculation: -
Weight of residue obtained
Solid Content ( %) = ----------------------------------------- X 100
Weight of sample
5. Reference : -
As per specified chart ( Chemicals list)

Limited
ISSUE :- 31/08/2008
INDIA LIMITED SPECIICATION OF CHEMICALS

Doc. No.
WIL/RUGS/SOP-C000
P/No. 1 Of
PHYSICAL
SR.NO NAME APPEARANCE PURITY FUNCTION
96 % AND BASIC
1 ACETIC ACID COLORLESS LIQUID ABOVE CHEMICAL
96 % AND BASIC
2 CAUSTIC FLAKES WHITE FLAKES ABOVE CHEMICAL
BASIC
3 CAUSTIC SODA LYE COLORLESS LIQUID 45 % TO 50 % CHEMICAL
96 % AND BASIC
4 SODA ASH WHITE POWDER ABOVE CHEMICAL
48 % AND BASIC
5 HYDROGEN PEROXIDE COLORLESS LIQUID ABOVE CHEMICAL
SODIUM HYDRO BASIC
6 SULPHATE WHITE POWDER 84 % TO 88 % CHEMICAL
25 % AND BASIC
7 NEUTRA ACID COLORLESS LIQUID ABOVE CHEMICAL
25 % AND BASIC
8 REDDIX ANA COLORLESS LIQUID ABOVE CHEMICAL
25 % AND BASIC
9 SARA ACID DV COLORLESS LIQUID ABOVE CHEMICAL
BASIC
10 SODIUM HYPO CHLORIDE YELLOW LIQUID 30 GPL CHEMICAL
96 % AND BASIC
11 MAGNASIUM CHLORIDE WHITE FLAKES ABOVE CHEMICAL
PALE YELLOW 96 % AND BASIC
12 SODIUM NITRATE POWDER ABOVE CHEMICAL

Limited
ISSUE :- 31/08/2008

Doc. No.
WIL/RUGS/SOP-C000
P/No. 2 Of
PH SOLUBILITY OF TOTAL
PHYSICAL VALUE HARDNESS CHLORINE
SR NO. NAME
APPEARANCE OF 1 % 5% SOL 10% SOL OF 50 GPL CONTENT
SOL SOL
SOD.HEXA META TRACE
2 PHOSPHATE WHITE POWDER NA - SOLUBLE - PRESENT
50 PPM
3 SOD.SULPHATE WHITE POWDER 7 TO 8 - - MAX -
250 PPM
4 VACCUM SALT WHITE POWDER 7 TO 8 - - MAX -
POLY VINYL WHITE
5 ALCOHOL GRANULES 7 TO 8 SOLUBLE - - -
6 SUPERNOL WSP WHITE POWDER 8 TO 9 SOLUBLE - - -
7 COT SIZE WHITE POWDER 9 TO 10 SOLUBLE - - -
8 FABPROOF HC WHITE POWDER 3 TO 4 SOLUBLE - - -
9 SIZOL TDY WHITE POWDER 8 TO 9 SOLUBLE - - -
10 SIZE BOND TS WHITE POWDER 7 TO 8 SOLUBLE - - -
11 MARPOSIZE T-10 WHITE POWDER 7 TO 8 SOLUBLE - - -
12 VICOL WLV WHITE POWDER 7 TO 8 SOLUBLE - - -
13 SIZE UCF-4 WHITE POWDER 7 TO 8 SOLUBLE - - -
14 SIZE GTW WHITE POWDER 7 TO 8 SOLUBLE - - -
15

Limited
ISSUE :- 31/08/2008

Doc. No.
WIL/RUGS/SOP-C000
P/No. 3 Of
SR
NO Name of Auxilaries Name of Supplier Function Physical Appearance ph Value Solid Conten
of 1%
Solution % By Weigh

1 STARTEX MASX STAR CHEMICAL Stabilizer of peroxide Colorless Liquid 7 TO 8 7.31%
2 STARSOFT NB STAR CHEMICAL softener amine silicone White liquid 6 to 7 16.15%
3 STARPAN RFH STAR CHEMICAL Wetting agent Colorless Liquid 8 to 9 28.08%
4 STARLEV FTS STAR CHEMICAL Leveling agent Yellowish Liquid 9 to 10 70 +/- 5%
5 STARTEX ADB STAR CHEMICAL Stabilizer Brownish Liquid 7 TO 8 44.37%
6 STAR FIX NB 10 STAR CHEMICAL FIXER DK Brownish Liquid 7 TO 8 45+/-5
7 STARFOAM FDR STAR CHEMICAL ANTIFOAMING AGENT WHITE PASTE 6.0 to 7.0 50 +/-5%
8 STARTEX ADM STAR CHEMICAL Stabilize LT BROWNISH LIQUID 7 TO 8 12 +/- 2%
9 STARWHITE GS STAR CHEMICAL WHITNER Yellowish Liquid 7 TO 8 10 +/- 2%
10 STARFIX DF STAR CHEMICAL FIXER Colorless Liquid 5 TO 6 48+/- 2%
11 TURBULANT 86 Mirachem Softener Colorless Liquid 6.0 to 7.0 26+/- 2 %
12 MIRAFIX NFDR Mirachem Fixing Colorless Liquid 7.0 TO 8.0 35 +/- 2%
13 Meiralyzer cipha Mirachem STABILIZER Colorless Liquid 11 to 12 26 +/-2%
14 Turbosilk Mirachem Softener Colorless Liquid 7 TO 8 28+/-2%
15 Mirasol FNK Mirachem Wetting agent Colorless Liquid 7 TO 8 60+/-5%
16 CIBATEX AB 45 CIBA speciality BUFFER ACID Colorless Liquid 3.0 TO 4.0 6 +/- 1%
17 ALCOSPERSE AD CIBA speciality LEVELING Lt. Yellowish Liq. 8.0 TO 9.0 40 +/- 2%
Cibafix
18 ECO/Albafix ECO CIBA speciality Fixing Lt. Yellowish Liq. 6.0 to 7.0 45 +/- 2%
19 CIBACEL LD CIBA speciality LEVELING . Brown Liquid 8.0 TO 9.0 20 +/- 2%
20 TUBOBLANC HA CHT INDIA LTD WHITNER Lt. Yellowish Liq. 9.0 TO 10.0 40+/-2%
21 SARACOL S SAREX Washing agent Colorless Liquid 7.0 TO 8.0 30 +/- 2%
22 Emcozyme 04 Mira chem DESIZING Lt. Yellowish Liq. 7.0 to 8.0 10 +/-2%
Associated Colorless Liquid
23 Activin HLK Chemicals Replacement soda 11 to 12 60 +/-2%
24 Saracol S 1583 SAREX Washing agent Colorless Liquid 7.0 to 8.0 32+/-2%
25 Saroxy K SAREX Peroxide Killer Lt. Yellowish Liq. 7 TO 8 0.5+/-0.2 %
26 Mirasol FNK Mirachem Wetting agent Colorless Liquid 7 TO 8 60+/-5%
27 Sarafix AP SAREX Fixer Colorless Liquid 6 to 7 20+/- 2%
28 Meiralyzer cipha Mirachem STABILIZER Colorless Liquid 11 to 12 26 +/-2%
29 Turbulent 200 Mirachem Softener Colorless Liquid 7 TO 8 7+/-1%
Sarax Organic Pvt
30 Levellon WR Ltd LEVELING Lt. Yellowish Liq. 7 TO 8 35+/-2%
31 Turbosilk Mirachem Softener Colorless Liquid 7 TO 8 28+/-2%
32 BIOPAL SI SAREX BIOPOLISH Lt. Yellowish Liq. 6 TO 7 6+/- 1%
33 SARAWET NF Wetting agent Colorless Liquid 6 to 7 40 +/- 2
34 Lyogen IPA 66 clariant LEVELING Lt. Yellowish Liq. 7 TO 8
35 sarafast H sarex Fixer colorless liquid 6 to 7 44 +/- 2

Limited
ISSUE :- 31/08/2008
INDIA LIMITED PVA CHECKING

Doc. No.
WIL/RUGS/SOP-D000
P/No. 1 Of
1. Apparatus :- Beaker
2. Chemical: - Pottassium Dichromate, Sulphuric Acid, Distilled Water,
Sodium Hydroxide (48%)
3. Test Procedure
1) Preparation of chromic acid solution
Take 11.8 gm Potassium Dichromate + 50 ml water + 25ml H2SO4 (98%)
2) NaOH 48-50 %
Take 2-3 drops of chromic acid solution on fabric or yarn. Then rub
it up to 20-30 seconds. Put 2 drops of caustic lye (NaOH-48 %) and rub it.
Result:
-If color is brown, then PVA is present.
-If color is green, then PVA is removed.
Limited
ISSUE :- 31/08/2008
INDIA LIMITED DIRECT DYE DYEING

Doc. No.
WIL/RUGS/SOP-D000
P/No. 1 Of
1. Apparatus :- Technorama Dispensor,

2. Chemical: - Soft Water,Dyes, Leveling agent, Sodium Sulphate(salt),
Albatex AB 55, Fixing Agent, Softer, Soaping Agent
3. Dyeing Procedure:
(1) Pipette out the recipe as per the percentage taken.

(2) Add leveling agent and adjust pH-6.5.
(3) Run for 5 min at RT. Then raise the temperature to 70 oC.
(4) Add salt as per Table-1 and raise the temperature to 98 oC and
run for 15 min.
(5) Then cool down the temperature to 70oC and drain the bath.
4. After treatment:
(1) Give cold wash to sample in tap water.
(2) Treat with 0.5-1.0 % of fixer at 55oC for 10 min adjust pH-5 to 5.5
(3) Treat with 1-2% of softener at 48oC for 15 min adjust pH-5 to 5.5.
(4) Dry the sample and label it.
Salt at 70oC 98oC 15 min 55c 10min
fixer
Dye +Leveling agent +
70oC
Drain
48c 15 min
Softner
Programme Cycle
W ELSPUN
JAY A. NAIK
LimitedWORK INSTRUCTION MANUAL
R.K.BERA
INDIA L31/08/2008
ISSUE :- IMITED REACTIVE DYE DYEING
Doc. No.
WIL/RUGS/SOP-D000
P/No. 1 Of

Soda Ash, Albatex AB 55, Fixing Agent, Softer, Soaping
Agent
(2) Add leveling agent,adjust pH- 6.5.
(3) Run for 10 min add salt (As per table-2). Raise the temp
to 60oC and run for 30 min. Then add soda ash (As per
table-2).
(4) Run for 30 min at 60oC
(5) Drain the bath.
4. After treatment:
(2) Treat with 0.5-1.0 % of fixer at 55oC for 10 min adjust
pH-5 to 5.5
(3) Treat with 1-2% of softener at 48oC for 15 min adjust
pH-5 to 5.5.
Soda
55c 10min
30 min 30 min fixer
Salt
50oC Dye +Leveling
agent 60oC
10 min Drain
48c 15 min
Softner

Limited
ISSUE :- 31/08/2008
Programme Cycle
INDIA LIMITED ACID DYE DYEING

Doc. No.
WIL/RUGS/SOP-D000
P/No. 1 Of

2. Chemical: - Soft Water,Dyes, Leveling agent, Green Acid, Fixing
Agent,

(2) Add leveling agent and raise the temperature to 98 oC and run for
5 min. Adjust pH-5.0 with Green Acid solution.
(3) Run at 98oC for 10 min.
After treatment:
pH-5 to 5.5
Adjust pH 5.0 with Green Acid
70oC 15 min
5min 98oC 10 min
Fixer
60oC
Dye +Leveling agent Drain
Programme Cycle

Limited
ISSUE :- 31/08/2008
INDIA LIMITED DYE TESTING OF DIRECT DYE

Doc. No.
WIL/RUGS/SOP-D000
P/No. 1 Of
1. Apparatus :- Pippete, Beaker

Albatex AB 55, Fixing Agent, Softer, Soaping Agent
(1) Prepare 1% solution of standard and supply. Pipette out as
per 1% depth shade for both.
(2) Add leveling agent and adjust pH-6.5 with buffer solution.
(3) Run for 5 min at RT. Then raise the temperature to 60 oC.
(4) Add salt as per Table-1 and raise the temperature to 98 oC and run
for 15 min.
4. After treatment:
(2) Treat with 0.5-1.0 % of fixer at 55oC for 15 min adjust pH-5 to 5.5
(3) Treat with 1-2% of softener at 45oC for 15 min adjust pH-5 to 5.5.
(5) Check the supply sample against standard.
Salt at 50oC 98oC 15 min 55c 15min
fixer
Buffer sol (pH6.5) 50oC 60oC
Drain
45c 15 min
Softer

Limited
ISSUE :- 31/08/2008
Programme Cycle
INDIA LIMITED DYE TESTING OF REACTIVE DYE

Doc. No.
WIL/RUGS/SOP-D000
P/No. 1 Of

Soda Ash, Albatex AB 55, Fixing Agent, Softer, Soaping
Agent
(1) Prepare 1% solution of standard and supply. Pipette out
as per 1% depth shade for both.
(2) Add leveling agent, Salt (As per table-2)and adjust pH-
6.5 with buffer solution.
(3) Run for 30 min at 60oC. Then add soda ash (As per
table-2).
(4) Run for 30 min at 60oC
(5) Drain the bath.
4. After treatment:
pH-5 to 5.5
pH-5 to 5.5.
Soda 55oc for 10 in
30 min 30 min fixer

Buffer sol (pH6.5)+ Salt
60oC
Drain
48oc for 10 in
Softner
Programme Cycle
W ELSPUN
JAY A. NAIK
LimitedWORK INSTRUCTION MANUAL
R.K.BERA
INDIA L31/08/2008
ISSUE :- IMITED DYE TESTING OF ACID DYE
Doc. No.
WIL/RUGS/SOP-D000
P/No. 1 Of

2. Chemical: - Soft Water,Dyes, Leveling agent, Green Acid, Fixing
Agent
(1) Prepare 1% solution of standard and supply. Pipette out

as per 1% depth shade for both.
(2) Add leveling agent and adjust pH-5.0 with buffer
solution.
(3) Raise the temperature to 98oC and run for 20 min.
(4) Then cool down the temperature to 60oC and drain the
bath.
After treatment:
pH-5 to 5.5
pH-5 to 5.5.
(4) Dry the sample and label it. 70oc for 15 min
fixer
98oC 15 min
Buffer sol (pH5.0) 60oC
Drain 48oc for 10 min
softner
Programme Cycle

Limited
ISSUE :- 31/08/2008
INDIA LIMITED TESTING METHOD FOR ACETIC ACID

Doc. No.
WIL/RUGS/SOP-C000
P/No. 1 Of
1. Apparatus :- Burette, Pipette, Volumetric Flask, And Conical Flask

2. Chemical: - Acetic Acid(CH3COOH), 0.1 N Sodium Hydroxide(NaOH)
Solution, Phenolpthaline Indicator
3. Procedure : -
1. Take 1.00 grams of acetic acid sample into a volumetric

flask and make it volume to 250 ml.
2. Take 25 ml of above solution in a conical flask and add 2/3
drops of Phenolphthalein Indicator.
3. Titrate it against 0.1 N Sodium Hydroxide solution from
burette.
4. End Point: - Colour less to light persistent Pink.
Calculation Part: -
Burette Reading (B.R) X 6.03 X 0.1 X 250

% Purity Of STD % Purity Of Acetic Acid = 96.0% & Above
Acetic Acid = ----------------------------------------------------
Weight Of Sample X 25

Limited
ISSUE :- 31/08/2008
INDIA LIMITED TESTING METHOD FOR SODA ASH

Doc. No.
WIL/RUGS/SOP-C000
P/No. 1 Of

2. Chemical: - Sodium Hydroxide (NAOH) 0.1 N Hydrochloric Acid (HCL), and
Methyl Orange Indicator Solution.
3. Procedure : -
1. Take 1.00 grams of Soda ash sample into a volumetric
flask and make it volume to 250 ml.
2. Take 25 ml of above solution in a conical flask and
Add 2/3 drops of Methyl Orange Indicator Solution.
3. Titrate it against 0.1 N Hydrochloric Acid (HCL)
solutions from burette.
4. End Point: - Yellow to Orange.
Calculation Part: -
Burette Reading (B.R) X5.30 X 0.1 X 250
% Purity Of Soda Ash = -----------------------------------------------------------
STD % Purity Of Soda Ash =96.0% & above.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED TESTING METHOD FOR SODIUM HYDROXIDE

Doc. No.
WIL/RUGS/SOP-C000
NaOH (FLAKES & LYE)
P/No. 1 Of

2. Chemical: - Sodium Hydroxide (NAOH) 0.1 N Hydrochloric Acid (HCL), and
Phenolphthalein Indicator Solution.
3. Procedure : -
1. Take 1.00 grams of Caustic Soda sample into a
volumetric flask and make it volume to 250 ml.
add 2/3 drops of Phenolphthalein Indicator.
3. Titrate it against 0.1 N Hydrochloric Acid (HCL)
solution from burette.
4. End Point: - Pink. to Colorless
Calculation Part: -
Burette Reading (B.R) X 4.0 X 0.1 X 250
% Purity Of Caustic Soda = --------------------------------------------------
STD % Purity Of Caustic Soda Flakes =96.0% & above
STD % Purity Of Caustic Soda lye =45% to 50 %

Limited
ISSUE :- 31/08/2008
WORK INSTRUCTION MANUAL

WELSPUN Doc. No.
WIL/RUGS/SOP-C000
INDIA LIMITED TESTING METHOD FOR SODIUM HYPOCHLORIDE
P/No. 1 Of

2. Chemical: - Sodium Hypo chloride (Soda Bleach) Sample, Potassium Iodide
(KI) Powder, Acetic Acid (98%).
3. Procedure : -
1. Take 10.00 ml of Sodium hypo chloride sample into a
2.Take 10 ml of above solution in a conical flask and add
25ml of plain tap water, approx. 2.0 Gms of Potassium
Iodide powder and 2/3 drops of acetic acid.
3. Titrate it against 0.1 N Sodium Thiosulphate
(Na2S2O3) solution from burette.
4. End Point: - Yellow to colorless.
Calculation Part: -
Available Chlorine In gpl = ------------------------------------------------------
10 X 10
Standard Available Chlorine in gpl =30 gpl (minimum).

Limited
ISSUE :- 31/08/2008

Doc. No.
INDIA LIMITED
WIL/RUGS/SOP-C000
TESTING METHOD FOR SODIUM
HYDROSULPHITE
P/No. 1 Of

2. Chemical: - Formaldehyde Sol.n , 0.1 N Sodium Hydroxide (NaOH) 0.1 N
Iodine Sol.n, Phenolphthalein Indicator 0.1 N Sodium
Thiosulphate Sol.n , hydro chloric Acid (Conc.)
3. Procedure : -
a) Take 9 ml Formaldehyde in a beaker.
b) Add 20 ml water and 2-3 drop of phenolphthalein Indicator.
c) Neutralize with 0.1 N Sodium Hydroxide till solution
turn from colorless to pink.
d) Add about 2 gm Sodium Hydrosulphite to it and make it to
250 ml in volumetric flask by adding water. Keep it for 15
min.
e) Take 25 ml Iodine solution in conical flask.
f) Add 10 ml Sodium Hydrosulphite solution from volumetric
flask and 4-5 drops of Hydrochloric acid (conc).
g) Shake it for 5 min.
h) Titrate against 0.1 N Sodium Thiosulphate solution .
i) End point –Dark Brown to Colorless . Note the reading B.
j) Take 25 ml of iodine solution in conical flask and Titrate
against 0.1 N Sodium Thiosulphate solution .
k) End point –Dark Brown to Colorless, Note the reading A.
Calculation Part: - Purity % by weight = (A – B) X 4.352 X 0.1 X 250
STD % Purity Of Hydro = 84 to 88 %

Limited
ISSUE :- 31/08/2008
INDIA LIMITED TESTING METHOD FOR

Doc. No.
NEUTRA ACID /HEPTOP EMG WIL/RUGS/SOP-C000
P/No. 1 Of

2. Chemical: - Neutra Acid/ Heptol EMG, 0.10 N NaOH, and Phenolphthalein
Indicator Solution.
3. Procedure : -
1. Take 1.00 ml of Neutra Acid/ Heptol EMG sample into
a volumetric flask and make it volume to 250 ml.
2.Take 25 ml of above solution in a conical flask and,
add 2/3 drops of indicator.
3. Titrate it against 0.1 N NaOH solution from burette.
4. End Point: - Colourless to Pink.
Calculation Part: -
% Purity Of Neutra Acid = __________________________________
% Purity Of Neutra Acid =28% and above

% Purity Of Heptol EMG = 25% and above.

Limited
ISSUE :- 31/08/2008

Doc. No.
GLAUBER SALT (SODIUM SULPHATE) WIL/RUGS/SOP-C000
P/No. 1 Of

2. Chemical: - Erichrome Black T Indicator (0.1 Grams dissolved in 100 ml of
water), Ammonia Buffer Solution, and 0.02 N EDTA solution.
3. Procedure : -
1. Take 5.00 grams of Glauber’s Salt (Sodium Sulphate)
sample into a volumetric flask and make it volume to
100 ml.
add 2/3 drops of Indicator Solution, and 1.00 ml of
Ammonia buffer solution.
3. Titrate it against 0.02 N EDTA solution from burette.
4. End Point: - Wine red to greenish
Calculation Part: -3
Hardness of Glauber’s salt in 50gpl of ppm.

=Burette Reading (B.R) X 40
STD Hardness in 50gpl Of Glauber’s salt = Not more than 50 ppm

Limited
ISSUE :- 31/08/2008

Doc. No.
TOTAL HARDNESS OF WATER WIL/RUGS/SOP-C000
P/No. 1 Of

2. Chemical: - Erichrome Black T Indicator (0.1 Grams dissolved in 100 ml of
water), Ammonia Buffer Solution, and 0.02 N EDTA solution.
3. Procedure : -
1. Take 25 ml of tap water in a conical flask and
add 2/3 drops of Indicator Solution, and 1.00 ml of
Ammonia buffer solution.
3. Titrate it against 0.02 N EDTA solution from burette.
4. End Point: - Wine red to greenish.
5. Note down the burette reading as “x”.
Calculation Part=
Total Hardness = B.R. [“x”] X 40
Limit : Not More Than 10 ppm.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED BLEACH SAFE TEST

(WASHING AS PER AATCC-150 ADDING CHEMICALS AS
Doc. No.
WIL/RUGS/SOP-P0001
PER INHOUSE METHOD)
P/No. 1 Of

Conditioning Racks
2. Chemical: - Sodium Hypochlorite solution ( NaOCl) of 10
gpl available chlorine & AATCC WOB Detergent,
3. Specimen Size: - Full Rug
4. Test Procedure:
(1) Take the sample Rug to be tested & weigh the sample
and enough ballast to make a 1.8 ± 0.1 kg or 3.6 ± 0.1 kg as
per suitable weight.
(2) Put the sample ( with ballast load) washing machine.
(4) Add 1.5 oz (42.5 gm) Sodium Hypo Chlorite & 1.5 oz
(42.5 gm) of AATCC WOB detergent powder.
(5) Start the washing machine and complete the
washing cycle.
it.
(9) Repeat the same for 3 times
Evaluation: Evaluate the color change with grey scale.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED TESTING METHOD FOR HYDROGEN PEROXIDE

Doc. No.
WIL/RUGS/SOP-C000
P/No. 1 Of

2. Chemical: - Hydrogen Peroxide(H2O2),20 % Sulphuric Acid (H2SO4),
Potassium Permanganate sol.n(KMnO4)
3. Procedure : -
1. Take 1.00 grams of Hydrogen Peroxide sample into a
Add 20 ml of 20 % Sulphuric Acid Solution.
3. Titrate it against 0.1 N KMnO4 solutions from burette.
4. End Point: - colorless to red
Calculation Part: -
STD % Purity Of Hydrogen Peroxide=48 % & above.

Limited
ISSUE :- 31/08/2008
INDIA LIMITED TESTING METHOD FOR HYDROGEN PEROXIDE

Doc. No.
WIL/RUGS/SOP-C000
P/No. 1 Of

2. Chemical: - Hydrogen Peroxide(H2O2),20 % Sulphuric Acid (H2SO4),
Potassium Permanganate sol.n(KMnO4)
3. Procedure : -
1. Take 1.00 grams of Hydrogen Peroxide sample into a
Add 20 ml of 20 % Sulphuric Acid Solution.
3. Titrate it against 0.1 N KMnO4 solutions from burette.
4. End Point: - colorless to red
Calculation Part: -
STD % Purity Of Hydrogen Peroxide=48 % & above.
Peroxide indicator: 5 % Pottassium Tittanium Oxalate

0.1% H2SO4 (10 %)
Make it 100 ml with water.
Take 1 ml of bleaching liquor add 2-3 drops of above prepare indicator.
Observation:
Solution becomes yellow- peroxide present
Colorless solution- Peroxide NIL

Limited
ISSUE :- 31/08/2008

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WELSPUN WORK INSTRUCTION MANUAL

INDIA LIMITED INDEX

PREPARED BY : - Welspun India AUTHORISED BY : -

1) Apparatus:- Crock meter, White cotton cloth, Grey scale for

(1) Fix the test specimen in the insert of crock meter.

(1) Fix the test specimen in the insert of crock meter.

Evaluation: Evaluation the rating with Grey scale for staining.

PREPARED BY : - Welspun India AUTHORISED BY : -

WELSPUN WORK INSTRUCTION MANUAL

INDIA LIMITED COLOCOLOR FASTNESS TO RUBBING

1) Apparatus :- Crockmeter,cotton rubbing cloth,grey scale for staining

(1) Fix the test specimen (Fabric/Yarn) on Crock meter by

(1) Fix the test specimen (Fabric/Yarn) on Crock meter by

PREPARED BY : - Welspun India AUTHORISED BY : -

WELSPUN WORK INSTRUCTION MANUAL

ISO 105/C06 (C2S)

1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre, Grey Scale

(1) Prepare 4 g/l ECE Detergent + 1 g/l Sodium Perborate

PREPARED BY : - Welspun India AUTHORISED BY : -

WELSPUN WORK INSTRUCTION MANUAL

COLOR FASTNESS TO WASHING

1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre No -10, Grey

(1) Prepare 1.5 g/l Detergent (WOB) Solution.

PREPARED BY : - Welspun India AUTHORISED BY : -

INDIA LIMITED COLOR FASTNESS TO WASHING

1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre No -10, Grey

(1) Prepare 1.5 g/l Detergent (WOB) Solution.

PREPARED BY : - Welspun India AUTHORISED BY : -

WELSPUN WORK INSTRUCTION MANUAL

INDIA LIMITED DOMESTIC WASHING AND DRYING PROCEDURE

1. Apparatus :- Automatic Washing M/c(Front/Top Loading),Tumble dryer,

Evaluation : Evaluate the shrinkage lengthwise, widthwise and border wise

% Shrinkage = (Original Dimension – Washed Dimension) x100

PREPARED BY : - Welspun India AUTHORISED BY : -

WELSPUN WORK INSTRUCTION MANUAL

INDIA LIMITED DOMESTIC WASHING AND DRYING PROCEDURE

1. Apparatus :- Automatic Washing M/c(Top Loading),Tumble dryer,

Evaluation : Evaluate the shrinkage lengthwise, widthwise and border wise

% Shrinkage = (Original Dimension – Washed Dimension) x100

PREPARED BY : - Welspun India AUTHORISED BY : -

WELSPUN WORK INSTRUCTION MANUAL

INDIA LIMITED DIMENTIONAL CHANGE OF FABRIC

1. Apparatus :- Automatic Washing M/c(Top Loading),Tumble dryer,

% Shrinkage = (Original Dimension – Washed Dimension) x100

PREPARED BY : - Welspun India AUTHORISED BY : -

WELSPUN WORK INSTRUCTION MANUAL

INDIA LIMITED COLOR FASTNESS TO WASHING

1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre, Grey Scale

(1) Prepare 5 g/l ECE Detergent + 2 g/l Soda Ash

PREPARED BY : - Welspun India AUTHORISED BY : -

INDIA LIMITED COLOR FASTNESS TO CHLORINATED WATER

1. Apparatus :- Laundrometer,Steel balls,Steel beakers,Maultifibre, Grey Scale

(1) Prepare solution from sodium hypo chlorite 20mg/l,

WELSPUN WORK INSTRUCTION MANUAL

INDIA LIMITED COLOR FASTNESS TO

1. Apparatus :- Cylinder, Grey Scale for staining , Grey scale for

2. Chemical: - Sodium Hypochlorite, Calcium Chloride, Magnesium

INDIA LIMITED ABSORBENCY BY DROP METHOD

1. Apparatus :- Embroidery Hoop (6 Inch) or more diameter, Burette, Stopwatch

(1) Specimen condition at 65 + 2% Relative Humidity.

PREPARED BY : - Welspun India AUTHORISED BY : -

INDIA LIMITED COLOUR FASTNESS TO LIGHT

ISO 105 B01 WIL/RUGS/SOP-P000