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  • Metallographic Etchants

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    The following table lists the most commonly used etchants. Ammonia Hydrogen Peroxide (3%) DI Water mix Ammonia and water before adding peroxide. Must be used fresh. Excellent for aluminum and titanium alloys. Marble's Reagent CuSO4 Hydrochloric acid immersion etching at 20 degrees celcius.

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    The following table lists the most commonly used etchants. Ammonia Hydrogen Peroxide (3%) DI Water mix Ammonia and water before adding peroxide. Must be used fresh. Excellent for aluminum and titanium alloys. Marble's Reagent CuSO4 Hydrochloric acid immersion etching at 20 degrees celcius.

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    Attribution Non-Commercial (BY-NC)
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    536 tayangan2 halaman

    Metallographic Etchants

    Diunggah oleh

    turorama
    The following table lists the most commonly used etchants. Ammonia Hydrogen Peroxide (3%) DI Water mix Ammonia and water before adding peroxide. Must be used fresh. Excellent for aluminum and titanium alloys. Marble's Reagent CuSO4 Hydrochloric acid immersion etching at 20 degrees celcius.

    Hak Cipta:

    Attribution Non-Commercial (BY-NC)
    Unduh sebagai PDF, TXT atau baca online dari Scribd
    Tandai sebagai konten tidak pantas
    dari 2

    Metallographic Etchants

    Metallographic Etchants
    | Home | Consumables | MSDS | Procedures | Equipment | Etchants | Contact us |

    Metallographic Etchants
    Ordering on-line

    COMMON ETCHANTS

    CAUTION:Safety is very important when etching. Be sure to wear the appropriate protective clothing and Technical information observe all WARNINGS on chemical manufacuters MSDS. Also review the COMMENTS and CONDITIONS Section for each etchant.
    MSDS sheets Brochures and catalogs

    Recommended Etchants
    Aluminum alloys Brasses and Bronzes Cast Iron Copper alloys Low carbon steel High carbon steel Stainless steel Tin alloys Zinc alloys Ceramics

    Metallography Support

    Consumables Lab Equipment Brochures Applications Support Procedures Metallography basics

    The following table lists the most commonly used etchants

    Etchant

    Composition

    Conc.

    Conditions

    Comments

    ASTM No. 30

    Ammonia Hydrogen Peroxide (3%) DI Water

    62.5 ml 125 ml 62.5 ml

    Mix Ammonia and water before adding peroxide. Must be used fresh. Swab 5-45 seconds

    For etching copper, copper alloys and copper-silver alloys.

    Kalling's No. 2

    CuCl2 Hydrochloric acid Ethanol

    5 grams 100 ml 100 ml

    Immersion etching at 20 degrees Celcius

    For etching duplex stainless steels and Ni-Cu alloys and superalloys.

    Kellers Etch

    Distilled water Nitric acid Hydrochloric acid Hydrofluoric acid

    190 ml 5 ml 3 ml 2 ml

    10-30 second immersion. Use only fresh etchant

    Excellent for aluminum and titanium alloys.

    Klemm's Reagent

    Sodium thiosulfate solution Potassium metabisulfite

    250 ml Saturated 5 grams

    Etch for a few seconds to minutes

    For etching alpha-beta brass, bonze, tin, cast iron phosphides, ferrite, martensite, retained austenite, zinc and steel temper embrittlement.

    Krolls Reagent

    Distilled water Nitric acid Hydrofluoric acid

    92 ml 6 ml 2 ml

    Swab specimen up to 20 seconds

    Excellent for titanium and alloys.

    Nital

    Ethanol Nitric acid

    100 ml 1-10 ml

    Immersion up to a few minutes.

    Most common etchant for Fe, carbon and alloys steels and cast iron - Immerse sample up from seconds to minutes; Mn-Fe, MnNi, Mn-Cu, Mn-Co alloys.

    http://www.metallographic.com/Etchants/Etchants.htm[01.08.2011 11:38:59]

    Metallographic Etchants

    Marble's Reagent

    CuSO4 Hydrochloric acid Water

    10 grams 50 ml 50 ml

    Immerse or swab for 5-60 seconds.

    For etching Ni, Ni-Cu and Ni-Fe alloys and superalloys. Add a few drops of H2SO4 to increase activity.

    Murakami's

    K3Fe(CN)6 KOH Water

    10 grams 10 grams 100 ml

    Pre-mix KOH and water before adding K3Fe(CN)6

    Cr and alloys (use fresh and immerse); iron and steels reveals carbides; Mo and alloys uses fresh and immerse; Ni-Cu alloys for alpha phases use at 75 Celcius; W and alloys use fresh and immerse; WC-Co and complex sintered carbides.

    Picral

    Ethanol Picric acid

    100 ml 2-4 grams

    Seconds to minutes Do not let etchant crystallize or dry explosive

    Recommended for microstructures containing ferrite, carbide, pearlite, martensite and bainite. Also useful for magnetic alloys, cast iron, high alloy stainless steels and magnesium.

    Vilellas Reagent

    Picric Acid Hydrochloric acid Ethanol

    1 gram 5 ml 100 ml

    Seconds to minutes

    Good for ferrite-carbide structures (tempered martensite) in iron and steel

    Guide to Acid Concentrations


    Acid / Base
    Nitric (HNO 3 ) Hydrofluoric (HF) Hydrochloric (HCl) Ammonium Hydroxide (NH4 OH)

    Specific gravity
    1.4 -

    Concentration
    68-70% 40% 37-38% 35%

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    http://www.metallographic.com/Etchants/Etchants.htm[01.08.2011 11:38:59]

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