DAFTAR PUSTAKA

Ade, Ryane, dkk. 2014. Penggunaan Teknologi Plasma Dalam Mengurangi Kandungan
BOD dan Warna pada Limbah Cair Indutri Minuman Ringan. Jurusan Teknik
Lingkungan dan Teknik Elektro Fakultas Teknik Universitas Diponegoro.
Semarang.

Araujo DM., Yoshida MI., Stapelfeldt F. and Ambiental E. 2009. Estudos

comparativos entre carvão ativado e resina de troca iônica para adsorção de
ouro ,cobre e ferro. R Esc Minas 62: 463-468.

Aritonang, B dan Hestina. 2018. Daya Adsorpsi Karbon Aktif dari Cangkang Kemiri
Terhadap Kadar Bilangan Peroksida pada Minyak Goreng Bekas. Jurnal Kimia
Saintek dan Pendidikan. Vol. 2, No. 1, hh. 21-30

Baker, F.S., et al. 1997. Activated carbon. Encyclopedia of separation technology. John
Wiley and Sons, New York.

Djatmiko, B., S. Ketaren dan S. Setyahartini. 1985. Pengolahan Arang dan

Kegunaannya. Agroindustri Press, Jurusan Teknologi Industri Pertanian,
FATETA-IPB, Bogor.

Faradina, E. dan Setiawati, N., 2010. Regenerasi Minyak Jelantah Dengan Proses
Bleaching Menggunakan Adsorben Arang Aktif. Laporan Penelitian Program
StudiTeknik Kimia. Universitas Lambung Mangkurat, Banjarbaru.

Ginting, Radhwa Yumna. 2020. Produksi Biochar Dari Limbah Kulit Biji Mete Dengan
Metode Microwave Pirolisis. Skripsi. Universitas Hasanuddin. Makassar.

Hamdila, J.D. 2012. Pengaruh Variasi Massa Terhadap Karakteristik Fungsionalitas

dan Termal Komposit MgO-SiO2 Berbasis Silika Sekam Padi Sebagai Katalis.
Skripsi. Universitas Lampung. Bandar Lampung.

57
Harsanti, D. 2010. Sintesis dan Karakteristik Boron Karbida dari Asam Borat, Asam
Sitrat dan Karbon Aktif. Jurnal Sains dan Teknologi Modifikasi Cuaca. 11(1) :
29-40.

Hassan, M. Y., Hussein, M. A., dan Osman, H. I. (2010). Determination of Fuel

Properties and Enginne Performance of Ethanol/Gasolibe Blends for Spark
Ignition Engine. Khartoum: University of Khartoum.

Idham, D.S. 2008. Parameter-Parameter Dalam Analisa Batubara, Makassar.

Kim, I.K. Hong, I.S. Choi and C.H. Kim, Journal of Ind. and Eng. Chemistry, 2 (2)
1996) 116-121.

Klancnik, Grega, Jožef Medved, dan Primož Mrvar. 2010. Differential thermal analysis
(DTA) and differential scanning calorimetry (DSC) as a method of material
investigation. Materials and Geoenvironment. 57(1): 127-142

Konuma. (1992). Film Deposisition by Plasma Techniques. USA: Spirnger-Verlag.

M.B, Sweatman dan N.Quirke.2001. Characterization of Porous Materials by Gas

Adsorption: Comparison of Nitrogen at 77 K and Carbon Dioxide at 298 K for
Activated Carbon, 5011-5020.

Monika, I., Sumaryono, Suprapto, S., Rahayu, A., dan Margono, B. (2009). Optimasi
proses dan uji coba pemanfaatan karbon aktif batu bara. Laporan Akhir. Pusat
Penelitian dan Pengembangan Teknologi Mineral dan Batu Bara, Bandung.

Naftali, C. dan Wamea, A.P. (2015). Prarancangan pabrik karbon aktif grade industri
dari tempurung kelapa. Skripsi Sarjana. Fakultas Teknik. Universitas Gadjah
Mada. Yogyakarta.

Novie. 2014. Coal Proximate and Ultimate Analysis, Jakarta.

Nur, Muhammad. 2011. Fisika Plasma dan Aplikasinya. Universitas Diponegoro.

Semarang.

58
Nurdin, M.F. 2016. Perancangan Teknologi Sederhana Untuk Membangkitkan
Microwave Plasma Dalam Cairan. Jurusan Mesin, Fakultas Teknik, Universitas
Hasanuddin.

Pari, G. 1996. Kualitas arang aktif dari 5 Jenis Kayu. Buletin Penelitian Hasil Hutan
Vol. 14 No. 2 : 60 – 68.

Perwira, G, 2014. Analisis Luas Permukaan Arang Aktif Dengan Menggunakan

Metode BET (SAA). Semarang.

Potter F. dan Christopher. 2010. Fisika Modern Di Sekitar Kita. P.T. Indeks Jakarta

Putra, A.E.E. 2013. Produksi Hidrogen Melalui Dekomposisi Metana Dengan High
Frequency Plasma. Jurusan Teknik Mesin. Universitas Hasanuddin. Makassar.

Rodriguez-Reinoso F., Molina-Sabio M. and Munecas MA. 1992. Effect of

microporosity and oxygen surface groups of activated carbon in the adsorption
of molecules of different polarity. J Phys Chem 96: 2707-2713.

Schecter,I.barzilai,I.L.,anda Bulatov,V. (1997). Online Remote Prediction of Gasoline

Properties by Combined Optical Method, Ana.Chim.Acta, 339. Hal 193-199.

Sembiring, dkk. 2003. Arang Aktif (Pengenalan dan Proses Pembuatan).

Sing, K.S.W., Everett, D.H., Haul, R.A.W., Moscou, L., Pierotti, R.A., Rouquerol, J.,
and Siemieniewska, T., (1985), Reporting Physisorption Data for Gas Solid
Systems with Special Reference to the Determination of Surface Area and
Porosity, Pure & Appl. Chem., Vol. 57, No. 4, pp. 603-619.

Subama, E. 2010. Pengsruh Penambahan 20% Berat Fly Ash Terhadap Sifat Fisis
Keramik Tradisional Berbasis Mineral Lempung Dengan Suhu Penyinteran
1100oC. Skripsi. Universitas Lampung. Bandar Lampung.

59
Sudirjo, M. 2006. Pembuatan Karbon Aktif dari Kulit Kacang Tanah (Arachis
hypogeae) dengan Aktivator Asam Sulfat, Skripsi, Universitas Diponegoro,
Semarang.

Sudrajat dan S. Soleh, 1994, “Petunjuk teknis pembuatan arang aktif”, Puslitbang Hasil
Hutan dan Sosial Ekonomi kehutanan, Bogor.

Suherman. 2009. Karakteristik Fungsionalitas dan Termal Bahan Keramik Cordierite

(Mg2Al4Si5O18) Berbasis Silika Sekam Padi Akibat Perlakuan Kalsinasi.
Skripsi. Universitas Lampung. Bandar Lampung.

Surya, Y. 2010. Oven Microwave, (online), (http://soerya.surabaya.go.id, diakses

tanggal 08 September 2020).

Sutanto, H., Subagio, A., Supriyanto, E., Arifin, P., Budiman, M., Sukirno, dan
Barmawi, M. 2005. Pengaruh Laju Alir Gas Nitrogen Terhadap Intensitas Emisi
Optik Plasma Nitrogen Yang Dibangkitkan Oleh Gelombang Mikro 2,45 Ghz
Dengan Metoda Optical Emission Spectroscopy. Vol. 7: 22-28. ISSN 1411-
1349.

Syaifullah, Arief. 2019. Analisis Pengaruh Variasi Volume Oksigen Terhadap Nilai
Kalori Bahan Bakar Gasoline Menggunakan Alat Kalorimeter Bom. Skripsi.
Universitas Hasanuddin. Makassar.

Tanaka, K., Yosiaki, K., Tetsuro S., Fumiko, H. and Katsuko, K. (2008). Quantitation
of Curcuminoids in Curcuma Rhizome by Near-Infrared Spectroscopic
Analysis. Journal of Agriculture and Food Chemistry. Vol 8 No 56. Hal 8787-
8792.

Tawalbleh, Journal of Applied Science,5(3)(2005)482-487

Thermo Nicolet. (2001). Introduction to FTIR Spectrometry. Thermo Nicolet Inc:

Madison, USA.

60
LAMPIRAN

61
62
63
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St3_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID sebelum plasma_2 Weight 0,532 g
Description
Analysis
Data ID {485a20d1-f779-471a-ac5c-365952dd4ff1}
Operator operator Date 2020.11.23 Duration 119,45 min
Instrument St 3 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,2225 °C Void Volume Mode NOVA mode Cell ID 31
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Thickness Method deBoer
P-tags below 0.35 ignored Moving Pt. Average off
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K

BJH Pore Size Distribution Adsorption results

Surface Area 0 m²/g
Pore Volume 0 cc/g
Pore radius Dv(r) 1.62179 nm

Table- BJH Pore Size Distribution Adsorption

radius Pore Volume Pore Surf. dV(r) dS(r) dV(log r) dS(log r)
nm cc/g Area cc/nm/g m²/nm/g cc/g m²/g
m²/g
1.62179 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.78392 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.97587 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.20509 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.46152 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.76770 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.15733 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.66175 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
4.33112 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
5.29721 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
6.77073 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
9.40447 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127113532047-02478} Page 1 of 1

64
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St3_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID sebelum plasma_2 Weight 0,532 g
Description
Analysis
Data ID {485a20d1-f779-471a-ac5c-365952dd4ff1}
Operator operator Date 2020.11.23 Duration 119,45 min
Instrument St 3 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,2225 °C Void Volume Mode NOVA mode Cell ID 31
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Thickness Method deBoer
P-tags below 0.35 ignored Moving Pt. Average off
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K

BJH Pore Size Distribution Desorption results

Surface Area 0 m²/g
Pore Volume 0 cc/g
Pore radius Dv(r) 1.62649 nm

Table- BJH Pore Size Distribution Desorption

radius Pore Volume Pore Surf. dV(r) dS(r) dV(log r) dS(log r)
nm cc/g Area cc/nm/g m²/nm/g cc/g m²/g
m²/g
1.62649 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.77874 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.95353 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.15397 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.39252 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.66575 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.98100 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.39366 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.92243 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
4.61204 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
5.56010 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
7.04074 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
9.67852 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127113549656-02533} Page 1 of 1

65
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St3_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID sebelum plasma_2 Weight 0,532 g
Description
Analysis
Data ID {485a20d1-f779-471a-ac5c-365952dd4ff1}
Operator operator Date 2020.11.23 Duration 119,45 min
Instrument St 3 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,2225 °C Void Volume Mode NOVA mode Cell ID 31
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Table - Isotherm Isotherm
Relative Pressure, P/Po Volume Adsorbed
@STP
cc/g
0.0254686 -0.018788
0.0709092 -0.0856479
0.112909 -0.143724
0.156984 -0.219312
0.201798 -0.318773
0.248359 -0.414472
0.289117 -0.492154
0.334095 -0.575396
0.380045 -0.666648
0.423590 -0.742406
0.465227 -0.822907
0.511691 -0.912953
0.556166 -0.998652
0.597830 -1.08329
0.641356 -1.16831
0.685683 -1.26177
0.730189 -1.34762
0.773968 -1.43474
0.819398 -1.52139
0.862529 -1.60957
0.906952 -1.69930
0.950525 -1.76417
0.908959 -1.69762
0.868116 -1.62782
0.826286 -1.55104
0.787548 -1.48800
0.746914 -1.40837
0.707345 -1.34793
0.664482 -1.26977
0.625842 -1.20110
0.587197 -1.13786
0.545079 -1.06218
0.504052 -1.00103
0.463631 -0.938866
0.422665 -0.873427
0.383842 -0.817815
0.342591 -0.749353
0.302224 -0.693682
0.262342 -0.632289
0.220378 -0.566931
0.180423 -0.500662
0.138938 -0.425765
0.0997997 -0.397122

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127113426963-02262} Page 1 of 1

66
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St3_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID sebelum plasma_2 Weight 0,532 g
Description
Analysis
Data ID {485a20d1-f779-471a-ac5c-365952dd4ff1}
Operator operator Date 2020.11.23 Duration 119,45 min
Instrument St 3 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,2225 °C Void Volume Mode NOVA mode Cell ID 31
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K

BET Multi-point BET results

Isotherm Branch Adsorption
Slope 1281.35
Intercept -937.725
Correlation coeff., r 0.720785
C constant -0.366443
Surface area 10.1347 m²/g
Table - BET Multi-point BET
Relative Pressure Volume Adsorbed 1 / [ W((P/Po) - 1) ]
@STP
cc/g
0.0254686 -0.018788 -1112.9583
0.0709092 -0.0856479 -712.9803
0.112909 -0.143724 -708.5715
0.156984 -0.219312 -679.3726
0.201798 -0.318773 -634.5593
0.248359 -0.414472 -637.8594
0.289117 -0.492154 -661.1876

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127113507755-02396} Page 1 of 1

67
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St3_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID sebelum plasma_2 Weight 0,532 g
Description
Analysis
Data ID {485a20d1-f779-471a-ac5c-365952dd4ff1}
Operator operator Date 2020.11.23 Duration 119,45 min
Instrument St 3 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,2225 °C Void Volume Mode NOVA mode Cell ID 31
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Temp. Comp yes
Thickness Method deBoer
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K

Total Pore Volume results

Total Pore Volume -2,7356e-003 cc/g
for pores smaller than 20,43 nm (radius)
at relative pressure 0,95052

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127113602312-02576} Page 1 of 1

68
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St4_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID setelah plasma_2 Weight 0,5125 g
Description
Analysis
Data ID {704c9fb5-707c-4875-af7e-5f5de689792e}
Operator operator Date 2020.11.23 Duration 120,783 min
Instrument St 4 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,125 °C Void Volume Mode NOVA mode Cell ID 41
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Thickness Method deBoer
P-tags below 0.35 ignored Moving Pt. Average off
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K

BJH Pore Size Distribution Adsorption results

Surface Area 0 m²/g
Pore Volume 0 cc/g
Pore radius Dv(r) 1.62072 nm

Table- BJH Pore Size Distribution Adsorption

radius Pore Volume Pore Surf. dV(r) dS(r) dV(log r) dS(log r)
nm cc/g Area cc/nm/g m²/nm/g cc/g m²/g
m²/g
1.62072 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.78506 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.97567 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.20004 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.45844 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.77471 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.16267 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.66899 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
4.35296 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
5.29286 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
6.76280 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
9.41210 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127122932895-13058} Page 1 of 1

69
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St4_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID setelah plasma_2 Weight 0,5125 g
Description
Analysis
Data ID {704c9fb5-707c-4875-af7e-5f5de689792e}
Operator operator Date 2020.11.23 Duration 120,783 min
Instrument St 4 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,125 °C Void Volume Mode NOVA mode Cell ID 41
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Thickness Method deBoer
P-tags below 0.35 ignored Moving Pt. Average off
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K

BJH Pore Size Distribution Desorption results

Surface Area 0 m²/g
Pore Volume 0 cc/g
Pore radius Dv(r) 1.62411 nm

Table- BJH Pore Size Distribution Desorption

radius Pore Volume Pore Surf. dV(r) dS(r) dV(log r) dS(log r)
nm cc/g Area cc/nm/g m²/nm/g cc/g m²/g
m²/g
1.62411 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.77786 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
1.95712 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.15581 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.38753 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.65767 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
2.98447 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.39578 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
3.90386 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
4.57065 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
5.54984 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
7.03978 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00
9.54490 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00 0.000000e+00

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127122946963-13104} Page 1 of 1

70
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St4_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID setelah plasma_2 Weight 0,5125 g
Description
Analysis
Data ID {704c9fb5-707c-4875-af7e-5f5de689792e}
Operator operator Date 2020.11.23 Duration 120,783 min
Instrument St 4 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,125 °C Void Volume Mode NOVA mode Cell ID 41
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Table - Isotherm Isotherm
Relative Pressure, P/Po Volume Adsorbed
@STP
cc/g
0.0261003 -0.0752764
0.0685516 -0.163290
0.116391 -0.252361
0.158881 -0.349849
0.200801 -0.461977
0.247115 -0.575643
0.292355 -0.684384
0.333470 -0.775125
0.379069 -0.884135
0.423898 -0.982660
0.465482 -1.07918
0.511394 -1.18893
0.554710 -1.28762
0.598178 -1.39137
0.642674 -1.49320
0.685606 -1.59734
0.731219 -1.69390
0.775328 -1.80107
0.818225 -1.89386
0.862922 -1.99325
0.906900 -2.09392
0.950716 -2.16370
0.907005 -2.09183
0.867463 -2.01761
0.827329 -1.93852
0.785100 -1.86242
0.745331 -1.79113
0.706494 -1.72091
0.665999 -1.64698
0.624837 -1.56940
0.586002 -1.50859
0.544740 -1.43310
0.505199 -1.37588
0.463998 -1.30779
0.421783 -1.24387
0.383424 -1.19099
0.341836 -1.12481
0.300921 -1.06861
0.260871 -1.01278
0.220990 -0.951404
0.181303 -0.889236
0.139196 -0.820698
0.099956 -0.794922

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127122845876-12905} Page 1 of 1

71
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St4_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID setelah plasma_2 Weight 0,5125 g
Description
Analysis
Data ID {704c9fb5-707c-4875-af7e-5f5de689792e}
Operator operator Date 2020.11.23 Duration 120,783 min
Instrument St 4 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,125 °C Void Volume Mode NOVA mode Cell ID 41
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K
BET Multi-point BET results
Isotherm Branch Adsorption
Slope -648.348
Intercept -307.096
Correlation coeff., r 0.92946 C
constant 3.11123
Surface area 0 m²/g

Table - BET Multi-point BET

Relative Pressure Volume Adsorbed 1 / [ W((P/Po) - 1) ]
@STP
cc/g
0.0261003 -0.0752764 -284.8538
0.0685516 -0.163290 -360.6204
0.116391 -0.252361 -417.6254
0.158881 -0.349849 -431.9996
0.200801 -0.461977 -435.1515
0.247115 -0.575643 -456.2117
0.292355 -0.684384 -482.9992

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127122901843-12957} Page 1 of 1

72
 INSTITUT TEKNOLOGI BANDUNG
Quantachr ome T ouchWin v1 .2
Report date: Jum Nov 27 2020 Operator: operator
Filename: 44 Pts Full isotherm - St4_20201123_134559.qcuPhysIso

Analysis Information
Sample
ID setelah plasma_2 Weight 0,5125 g
Description
Analysis
Data ID {704c9fb5-707c-4875-af7e-5f5de689792e}
Operator operator Date 2020.11.23 Duration 120,783 min
Instrument St 4 on NOVA touch 4LX [s/n:17018063001] Firmware 1.04
Comments
Ambient Temp. 39,125 °C Void Volume Mode NOVA mode Cell ID 41
Cell Type 12mm with rod Thermal Delay 600 sec Po Mode Continuous
Adsorbate
Name Nitrogen Molecular Weight 28,013 g/mol Cross Section Area 16,2 Ų/mol
Non-ideality 6,58e-005 1/torr Bath Temperature 77,35 K
Degas information
Type Vacuum Degassing
Operator
Description

Data Reduction Parameters

Thermal Transpiration no
Temp. Comp yes
Thickness Method deBoer
Adsorbate Model
Name Nitrogen Molecular Weight 28,0134 g Cross Section Area 16,2 Ų/molec
Bath Temperature 77,35 K

Total Pore Volume results

Total Pore Volume -3,3552e-003 cc/g
for pores smaller than 20,51 nm (radius)
at relative pressure 0,95072

Quantachrome TouchWin™ v1.2 {Report ID: QC20201127123014158-13196} Page 1 of 1

73