Beamlines 2009/2010 and future

Harry Westfahl Junior Vice-diretor Cientfico LNLS

LNLS Beamlines

16 Beamlines + 2 planned

UV and Soft X-ray (4) X-Ray Fluorescence and Absorption (4) X-Ray Diffraction (4) X-Ray Scattering (2) and Macromolecular Crystallography (2) X-Ray tomography (Talbot interferometer) + Infrared/AFM planned for 2012

LNLS Beamlines

Instrumentation Highlights

PGM, our first undulator beamline operating for users XDS at the SC wiggler will open for users 1st sem. of 2012 Refurbishing/remodeling of the optics of 3 beamlines (SXS, SAXS1, SGM) Several new detection systems installed (Pilatus, multi-channel analyzers, etc..) Several new end-stations for in-situ and high throughput experiments (XMCD, SC magnet, Gleeble, MX robot, etc..) LabWeb: Prototype for remote beamline operation over the web (XRD, SAXS) New control/data acquisition system under evaluation (EPICS) to replace the in-house system which is now obsolete
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Instrumentation planning ( 2 years )

2 new beamlines (tomography and infrared) Control and data acquisition refurbishing (EPICS) and LabWeb will merge into LabWeb II (2.6 M R$ from PETROBRAS) Time resolved SAXS (msec): Rheo-SAXS (PETROBRAS) and Stoppedflow, Electric Field XAFS: micro X-Ray Fluorescence, High Pressures Phase retarder (polarization)

EUV: SGM extension, mirror replacement on TGM XRD: 2 new diffractometers (FAPESP) MX: Refurbishing and realignment
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Industrial Projects
PETROBRAS: Catalysis, Gleeble, Drag reduction BRASKEM: Ultra-small creep fibers Rhodia (future): Catalysis Vale (future): Tomography of minerals UNILEVER (future): Nano-structured soaps Cosmetics network: Nano-structured cosmetics

LNLS Beamlines

UV and Soft X-Rays Beamlines

Beamline TGM SGM

Monochromator Toroidal Grating

Energy Range 12-300 eV

Applications Surface, Atomic and Molecular Physics; Time-of-Flight Surface and Interfaces. Atomic and Molecular Physics Surface and Interfaces. Atomic and Molecular Physics, X-ray Magnetic Dichroism Photoabsorption and photoemission spectroscopy

Spherical Grating 100-1200 eV

PGM

Planar Grating

100-1200 eV

SXS

Double crystal

1-6 keV

LNLS Beamlines

Research

Researcher Post-Doc 2s 2011

2s 2011

Instrumentation

Instr. Supervisor Scientific Assistant Technician Trainee

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SGM and TGM

UV and Soft X-Rays Beamlines

SGM:
Remodeled optics with new mirrors in Silicon substrate (ordered) and longer focal distance Improved stability, flux and resolution and better vaccum (additional pump)

TGM:

New mirrors (same optics) ordered with Silicon substrate Improved stability

LNLS Beamlines

PGM (90-1200 eV)

Open for users - first results of photoemission on liquids (only 5 exp. in the world) - nanosciences, nanomagnetism

1. 2. 3. 4.

Very stable, reliable Resolution > 8000 Easy change of polarization Very quick change of the gap of the undulator

LNLS Beamlines

X-Ray Absorption and Fluorescence Beamlines

Beamline Monochromator XRF XAFS1 XAFS2 DXAS White beam or double crystal Channel cut Focusing Double crystal One single-bent crystal

Energy Range 5-25 keV 3-25 keV 4-17 keV 5-12 keV

Applications Environment and Geochemistry, Biophysics and Agriculture Materials Science, thin films and diluted systems Materials Science, thin films and diluted systems Materials Science, In-situ Studies, Magnetic Dichroism

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Research

Researcher Post-Doc
Instrumentation

Instr. Supervisor Scientific Assistant Technician Trainee

LNLS Beamlines
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FAX Highlights
X-Ray Fluorescence and Absorption Beamlines

Micro X-Ray Fluorescence

Diamond /4 plate for XMCD

High Pressures @ 150 GPa

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X-Ray Diffraction

Beamline XRD1 XRD2 XPD

Monochromator Focusing Double crystal Focusing Double crystal Focusing Double crystal Focusing or Plane Double crystal

Energy Range 5-15 keV 5-15 keV 5-15 keV

Applications Single crystal diffraction, Multiple Beam Diffraction Magnetic Scattering, Grazing Incidence, Nanostructures Power Diffraction Studies in Materials Science Materials Science

SCW

5-30 keV

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Research

Researcher Post-Doc
Instrumentation

Instr. Supervisor Scientific Assistant Technician Trainee

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XRD Highlights
X-Ray Fluorescence and Absorption Beamlines

Planning:
6-circle diffractometer with goniometric tower for Atomic Layer Deposition (FAPESP) in situ
Multiple diffraction, Bragg Surface

Heavy-duty 2-circle diffractometer with an ensemble of Si microstrip (Mythen 1k) detectors

Powder diffraction for Sirius

Start operating XDS for users (joint management with FAX group)

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X-Ray Scattering and Macromolecular Crystallography

Beamline MX1 MX2 SAXS1 SAXS2

Monochromator One single-bent crystal Focusing Double crystal Toroidal Multilayer One single-bent crystal

Energy Range 6-12 keV 5-15 keV 6-12 keV 6-12 keV

Applications Structural Molecular Biology Structural Molecular Biology using MAD technique Dynamics of soft materials Glasses and Nanocrystals, Polymers and Molecular Biology

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Research

Researcher Post-Doc
Instrumentation

LNBio

Instr. Supervisor Scientific Assistant Technician Trainee

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SAXS Highlights
X-Ray Scattering

Time Resolved SAXS (200 Hz) with 10ph/s

Rheo-SAXS, Stopped flow, etc..

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