De Guzman, Ma. Ediza May P. BSFT 1 Date of Performance: January 20, 2012 Date of Submission: February 17, 2012
ABSTRACT
There were 3 set- up tested during the experiment. Those are the test for carbon and hydrogen, nitrogen, and sulfur. The test for carbon and hydrogen was done using sugar in which, change in its appearance and color is very evident upon heating. The mixture of stock solutions, 6 % NaOH solution and 0.5% cupric sulfate solution was used for nitrogen testing. There was a changed in color when mixed together. The test for sulfur was made using one ml of stock solution, NaOH solution and lead acetate solution. The mixed solution change its appearance and proves its alkalinity.
Qualitative Analysis of Organic Compounds The analysis and identification of unknown organic compounds constitutes a very important aspect of experimental organic chemistry. Analytical chemistry is the study of the separation, identification, and quantification of the chemical components of natural and artificial materials. Qualitative analysis gives an indication of the identity of the chemical species in the sample and quantitative analysis determines the amount of one or more of these components. The separation of components is often performed prior to analysis.
The experiment was done to analyze the type of elements found in an organic compounds.
METHODS
The experiment was conducted by Ma. Ediza May P. de Guzman and Cyril L. Denilla The materials used are Bunsen burner, test tube, test tube holder, water bath, dropper, tripod, sugar, stock solution, NaOH, 0.5 % of Cupric Sulfate and Lead Acetate. PROCEDURES: A. Test for Carbon and Hydrogen B. Test for Nitrogen C. Test for Sulfur
RESULTS The outcome of the tested materials were based on the observation noted after the experiment. In testing the carbon and hydrogen, the sugar in the tin can melted slowly and the more it is subjected to heat, the more it turns into a caramel or brownish color. For Nitrogen, when the stock solution was added by 3 drops of 6%NaOH solution, Theres no change in its appearance but when it was added with 3 drops of 0.5% Cupric Sulfate solution, its color changed to blue. On testing the sulfur, during heating of the solutions it boils and produce bubbles.From a cloudy solution, after heat was applied it became clear appearance and had a little yellowish color. This prove its alkalinity
DISCUSSION
REFERENCES
De Guzman, Ma. Ediza May P. BSFT1 Date of Performance: January 13, 2012 Date of Submission: February 17, 2012
ABSTRACT
The melting and boiling point determination was performed using the set-up of Erlenmeyer, thermometer with attached glass tubing suspended on vegetable oil. The glass tubing was dipped fist on the sulfur powder before it was heated. The same procedure was applied on the other setup. The only thing that differs is the the glass tubing dipped on NaOH. Different temperatures were noted before and after heating.
The experiment was done to determine the boiling point and melting point of the substances used.
METHOD The experiment was conducted by Ma. Ediza May P. de Guzman and Cyril L. Denilla. The materials used are one small test tube, Bunsen Burner, tripod, sample of sulfur powder and NaOH, thermometer, glass tubing, wire gauze, Erlenmeyer flask, capillary tube, vegetable oil, and water bath. PROCEDURES: A. Melting Point Determination
Seal end of capillary tube by heating.
Gently tap the tube to let the sample settle down on the sealed end . By means of rubber band, attach the tube to a thermometer.
Gently tap the tube to let the sample settle down on the sealed end . By means of rubber band, attach the tube to a thermometer. Use vegetable oil for liquid bath with thermometer and the attached tube suspended it.
Heat until bubbles comes out.
Use vegetable oil for liquid bath with thermometer and the attached tube suspended it.
Heat the liquid bath with a temp. that raises 2-3 Celsius per minute.
RESULTS
The outcome of the tested materials were based on the observations noted after the experiment. In determining the melting point, the temperature at the beginning of the melting is 5 Celsius and raises to 125 Celsius when it was totally melted. For the boiling point, the temperature when stream of bubbles came out is 113 Celsius and 105 Celsius is the temperature when the last bubble came out.
DISCUSSION
REFERENCES