Test

BIEN DONG PETROLEUM OPERATING COMPANY
BIEN DONG-1 PROJECT EPCI OF HAI THACH PQP, HAI THACH WHP AND PIPELINES
CONTRACTOR: PETROVIETNAM TECHNICAL SERVICES CORPORATION M & C SUB CONTRACTOR: ALPHA ECC
Alpha ECC Chemical Cleaning Standard Operating Procedure

Document No.: E1001-ALPHAECC-0023
PTSC M&C/ALPHA ECC

REV DATE B1
09-0212
BDPOC
APPROVED BY PTSC REVIEWED BY APPROVED BY
PREPARED BY SUB
APPROVED BY SUB
REVIEWED BY PTSC
NAME SIGN DATE NAME SIGN DATE NAME SIGN DATE NAME SIGN DATE NAME SIGN DATE NAME SIGN DATE Khang T.L 09-0212 Quang P.V 09-0212
PTSC M&C
BIEN DONG PETROLEUM OPERATING COMPANY BIEN DONG-1 PROJECT EPCI OF HAI THACH PQP, HAI THACH WHP AND PIPELINES
BD POC
Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:
Alpha ECC - Standard Procedure for Chemical Cleaning
Page 2 of 20
REVISION RECORD SHEET No. Rev. No. 1 B1 Content of revision Issued for Review Date of Revision 09-02-2012
PTSC M&C
BD POC
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TABLE OF CONTENTS
SECTION DESCRIPTION
1.0 2.0 3.0 4.0 5.0
PAGE
PURPOSE ..4 SCOPE... .4 REFERENCE. .5 DEFINITIONS.. ..5 PROCEDURE 6 5.1 General Requirement 5.2 Documentation 5.3 Chemical cleaning equipment and connection work 5.4 Preparation for chemical cleaning 5.5 Chemical cleaning steps 5.6 Specific steps for leak test & water flushing 5.7 Specific steps for degreasing 5.8 Specific steps for pickling with acid 5.9 Specific steps for passivation/ neutralization 5.10 Nitrogen purging and preservation 6 6 7 8 9 10 12 14 16 18
6.0 7.0
INSPECTION..19 SPECIAL REQUIREMENT...19 7.1 Disposal of waste liquids 7.2 Safety requirement for chemical cleaning 19 19
8.0
RECORD .20 APPENDICES Appendix 1: Chemicals - MSDS and Data Sheets. Appendix 2: Cleaning Equipment Layout Diagram Appendix 3: Reporting Forms Appendix 4 : Organizational Chart
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1.0 PURPOSE
This procedure covers the methods of cleaning and protection of the internal surfaces of steel offshore piping systems to acceptable levels of cleanliness for a successfully start-up and operation. It will only be used for piping systems, specified by project specifications and identified on AFC (approved for construction) drawings for chemical cleaning.
2.0 SCOPE
This procedure includes the preparation and execution of chemical cleaning (leak test & water flushing, degreasing, acid pickling, neutralization / passivation, and nitrogen blanket application) to the internal surface of carbon or stainless steel piping systems to remove loose scale, rust, foreign matter, grease, etc. During the chemical cleaning operations, care shall be taken to prevent direct contact of chemicals with items that are identified on the isometric drawings for chemical cleaning: Piping systems with copper alloy materials, Vessels, Pumps, All bolted/screwed valves and instruments.
The chemical cleaning process shall be accomplished by using chemical agents (degreasing, pickling, neutralization and passivation agents) in the system and circulating the chemical solutions for specified periods of time. It also addresses environment regulation compliance and personnel safety aspects of the work to be done.
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3.0 REFERENCE
ISO 4406:1999: ANSI / ASME B3l.3-2010: ASTM A380 - 96: Hydraulic fluid power - Fluids - Method for coding the level of contamination by solid particles Code for Pressure Piping - Process Piping Standard Practice for Cleaning, Descaling, and Passivation of Stainless Steel Parts, Equipment, and Systems. ASTM Committee A-1 on Steel, Stainless Steel, and Related Alloys Standard Practice for Chemical Passivating Treatments for Stainless Steel.
ASTM A 967-05:
4.0 DEFINITIONS
BD POC: PTSC: ALPHA ECC: P&ID: BIEN DONG PETROLEUM OPERATING COMPANY PETROLEUM TECHNICAL SERVICES COMPANY. SOUTHERN PETROLEUM CONSTRUCTION J.S COMPANY PIPING AND INSTRUMENTATION DIAGRAM
PTSC M&C
BD POC
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5.0 PROCEDURE 5.1 Gen eral Requirements

5.1.1. 5.1.2. Lines to be chemical cleaned shall be clearly identified on the P & IDs or isometric drawings, and Line Index, and submitted to BD POC representativ for approval. e Systems to be treated shall have been hydrostatically tested (water) which has accepted by BD POC. 5.1.3. during the 5.1.4. All supports shall be installed ready to receive variable loading and expansion cleaning process. Inline components such as orifice plates, check valve, control valves, flow meter elements and relief valves shall be removed and replaced with temporary spools (supplied by the client). All removed equipment shall be shown on each test pack and highlighted on The supply inlet into the system shall be fitted with a temporary isolation valve resistance type) for safety purposes.
been
5.1.5. drawings. 5.1.6. (chemical
5.1.7. The systems to be cleaned shall have high and low point vents and drains installed. The system filling point shall be the lowest point in the system. A high point vent shall be utilized as secondary return line and vent. 5.1.8. exceed 5.1.9. end Maximum temperature used during the operations of chemical cleaning shall not maximum design temperature for the systems as listed in the Line Index. Acceptance criteria for chemical cleaning shall be according to ISO 4406:1999. The results shall be a clean surface. For all synthetic lube oil and mineral lube oil piping systems, ISO 4406:1999 grade 17/15/12 (equivalent to NAS 1638 class 6) shall be the acceptance criteria. Acceptance criteria for all compressed gas piping systems shall be ISO 4406:1999 grade 17/15/12 (equivalent to NAS 1638 class 6).
5.2
Documentation
5.2.1. The compliance to specified ISO 4406:1999 requirements shall be documented.
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5.3
Chemical cleaning equipment and connection work

The table of equipment / instruments listed below is indicative only. The actual equipment shall be determined during the project phase and approved by PTSC and BD POC. As a minimum, the following equipment/instruments shall be used to facilitate testing:
No 1.
2.
3.
4.
5. 6. 7. 8. 9.
Equipment Chemical circulating tank 5000 liters Material: Composite Volume: 5m3 protection framework and gutters to collect chemicals Chemical batching tank 500 liters Material: Plastic corrosion-resistant Volume: 0.5m3 Protection framework and gutters to collect chemicals Chemical pumping station - Sandpiper Model S1F - Working pressure : 7 bar - Flow: 50 m3/h Include 05 diaphragm pump Waste water pumping station - Sandpiper Model S1F - Working pressure : 7 bar - Flow: 10 m3/h Include 02 diaphragm pumps pH measurement Hose connection QME R1AT " Material: Rubber with steel mesh Pressure max: 80 bar Flexible hose, corrosion-resistant Laser Particle Analyzer LasPaCII-P / or equivalent Thermometer
Qty 03
Original NAACO Vit nam NAACO Vit nam USA
Remakes
06
02
01
USA
02
Japan QME Flex Italia Technology
meters 01 01 01
Stauff, Germany
10. Pressure gauge for nitrogen
Connection work shall be as follows: Connection and bypass have to implement how to make sure cleaning chemical will not contact with all the equipment (or instrument) were installed on the piping system. (control valve, cylinder, pump, sensor) Typical layout diagram of the flushing equipment system is enclosed in Appendix 2.
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5.4 Preparation for chemical cleaning

As a minimum, the following technical aspects shall be checked for completion before commencement of the chemical operations: Flushing equipment chemically cleaned, System drained and dry before chemical cleaning, Marked up drawings (P&IDs) attached, System equipment bypassed and blinded, Analysis certificate copy attached, System/equipment labeled, Preservation carried out, System/equipment reinstated, System/equipment blinded off. As a minimum, the following safety aspects shall be addressed for completion before commencement of the chemical operations: In preparation position, tank chemical containers are placed absorbent pads lined with chemicals, chemical equipment collection when the problem occurred: a. Chemical cleaning acid, b. Tank fresh water tap emergency exhaust. c. Acid absorbent plate. At work site, MSDS of all chemicals to be used , and a portable eye wash station shall be located and available at all time in the zone of utilization. Personal Protective Equipment (PPE) for operators: a. Corrosion- resistant clothing b. Gas mask c. Face seal d. Rubber gloves. 2. Leak check and accident prevention: a. Upon completion of the temporary installation, the system shall be water tested to check for leaks The test pressure shall be maximum pump head discharge pressure with continuous flow. b. PTSC Safety officer shall witness the testing of the temporary facilities. c. Upon satisfactory completion of the test, PTSC Safety Officer will endorse the permit to work with corrosive material.
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5.5 Chemical cleaning steps

5.5.1 Main steps
Main steps of chemical cleaning are shown below: 1 LEAK TEST & WATER FLUSHING 2 DEGREASING WITH ALKALINE
WATER RINSING
PICKLING WITH ACID
WATER RINSING
PASSIVATION/ NEUTRALIZATION
WATER FLUSHING
5.5.2 Brief description of the process Brief description of the process
DRYING / NITROGEN PURGING
See Appendix 2 for a typical layout diagram for connecting a test pack with the chemical cleaning equipment system. DRYING / NITROGEN BLANKET PPLICATION: a nitrogen blanket shall be applied to all chemically cleaned lines and shall be kept at a positive nitrogen pressure until ready for start-up. This positive pressure shall be 10 psig.
PTSC M&C
BD POC
Document No.: E1001-ALPHAECC-0023 Revision No.: B1
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5.6 Specific steps for LEAK TEST & WATER FLUSHING

1-1 LEAK TEST & WATER FLUSHING
1-2
CLEANING CIRCUIT FILLING
1-3
CIRCULATION LEAK TEST
NO
1-4
WATER FLUSHING COMPLETE/ PUMP STRAINER CLEAN ? YES
a. Flow velocity check b. Leakage check
1-5
PREPARE FOR DEGREASING STEP 2
5.6.1 Leak test & water flushing control parameters

Circulation leak check: Flow velocity check: checking / recording leakage at cleaning system connection points. 90 - 150 cm/s
5.6.2 Leak test & water flushing acceptance criteria

Leakage: no leakage at system connection points at the end of Step 1 LEAK TEST & WATER FLUSHING.
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5.6.3 Leak test & water flushing description - Step 1

LEAK TEST & WATER FLUSHING is the first step in preparation for chemical cleaning, to ensure that the system to be treated is leak free after water flushing and prior to degreasing. It will also removes heavy deposits of oils, greases, soils or foreign matter other than mill scale, rust, or rust scale from internal surfaces of the piping system. This pre-cleaning shall be carried out by circulation method, using tap (potable) water. See Appendix 2 for typical layout of the system. During Step 1, no chemical shall be injected into the system. Piping to be cleaned will be disconnected or blanked off from mechanical equipment to prevent circulation of chemicals through bearings, cylinders, oil filter cartridges, instruments, screens and filters. Valves and equipment may be included in the circulation system, provided that their materials are resistant to chemical solutions involved and prior approval by customer (PTSC & BD POC) is obtained.
During flushing, the system shall be packed with the water and no air shall be present in high points. Use naked eyes to check connection points in the circulation system and look for water leakage (step 1-3). The work shall be immediately suspended to correct any found leaking point. Soap water, dry cloth or similar aids may be used from outside connection points to assist leakage detection. During the flushing operation, if any leak is observed, remedial action shall be taken to stop the leak and flushing shall be continued until the visual inspection of outlet water indicates it has the same appearance of inlet water. During flushing, water flow velocity shall be kept within the range of 90 to 150 cm/s (3 to 4 ft/s), prefererably at 150 cm/s.
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5.7 Specific steps for DEGREASING

LEAK TEST & WATER FLUSHING COMPLETE
2-1 FLUSHING CIRCUIT WITH WATER 2-2 WATER CIRCULATION (40 - 60 oC) 2-3 ALKALINE CLEAN WITH CIRCULATION OF ALCA SOLUTION FOR 4 HOURS (MAX.) NO 2-4 ALKALINE CLEANNING COMPLETE ? ALL PARAMETERS STABLE ? YES 2-5 NEUTRALIZE pH TO 7- 9. (ADD ALCA) 2-6 DRAIN OUT. SEND TO NEUTRALIZED TANK a. pH check b. Wipe test c. Temperature check d. Flow velocity check
2-7 RINSING WITH WATER
a. pH check < 8.5
2-8 PREPARE TO PICKLE WITH ACID STEP 3
5.7.1 Degreasing control parameters

Temperature: Flow velocity: Circulation period: pH: 40 - 60 oC 90 - 150 cm/s 4 hours 7 - 9.
5.7.2 Degreasing acceptance criteria

Cleanliness: pH < 8.5 (steps 2-7 only).
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5.7.3 Degreasing description - Step 2

DEGREASING WITH ALKALINE is the second step of chemical cleaning, to ensure that any remaining oil, or grease in the internal of the piping system (the test pack) is cleaned before Step 3 is commenced. All particles are further removed. The chemical used for degreasing has a mild foaming action, adapted to circulation treatment. After flushing the system and chemical bath tank with normal tap water (for carbon piping systems) or clean water of max. 20 ppm of chloride (for stainless steel piping systems), the temperature of the circulation water shall be raised by exchanging heat with a hot oil circuit to 40 - 60oC. This temperature shall be maintained throughout the treating process. Degreasing chemical shall be mixed into chemical tank (5 - 7%) and circulated through the system to remove grease and oil. Degreasing chemical: ALCA is a mixture of 10 - 25% potassium hydroxide (KOH), 2.5 - 10% diethanolamide of fat acids, 2.5 - 10% trisodium phosphate (MSDS and Data Sheets attached in Appendix) Treating duration shall be 2 - 4 hours A sample of the degreasing solution sample shall be tested every 30 minutes at the entrance and exit of the system. PTSC and BD POC representative(s) shall witness the analysis. Visual check: examination will be done by white light or using ultraviolet instrument and supplemented by wipe measure. The solvent will illuminate if it contains oil or grease (with ultraviolet).
Step 2-5: neutralization to achieve pH 7 - 9 shall be by adding ALCA. Wipes will be kept as an evidence of the progress of the degreasing step. When the wipe test shows no traces of oil, the degreasing process is deemed completed.
PTSC M&C
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5.8 Specific steps for PICKLING WITH ACID

DEGREASING COMPLETE
3-1 FILLING CIRCUIT WITH WATER a. Temperature check c. Leak check
3-2 HOT WATER CIRCULATION (40 - 50 oC) 3-3 ACIDS + INHIBITOR FEED (ADD ARA 400). CIRCULATION (40 - 50 oC) UNTIL IRON STABLE NO 3-4 PICKLING COMPLETE ? ALL PARAMETERS STABLE ? YES 3-5 NEUTRALIZE pH TO 7-9 (ADD ALCA) 3-6 DRAIN OUT. SEND TO NEUTRALIZED TANK
a. Cleanliness check, acc. to ISO 4406:1999 b. pH check c. Fe ++ion check (+/- 10% Fe ion readings after 3 consecutive readings means iron removal is completed)
3-7 RINSING WITH WATER
a. Cleanliness check, ISO 4406:1999 b. pH check 7-9
3-8 PREPARE TO PASSIVATION STEP 4
5.8.1 Pickling control parameters

Cleanliness: Temperature: Flow velocity: Fe ion content: pH: checking / recording in accordance with ISO 4406:1999 (steps 3-4 only) 40 - 50 oC 90 - 150 cm/s 600 - 2500 ppm (step 3-4) 3.5 - 4.5 (steps 3-4); 7 - 9 (step 3-7)
5.8.2 Pickling acceptance criteria

Cleanliness: Code 17/15/12, ISO 4406:1999 (equiv. NAS 1638 class 6) for the piping systems (step 3-7 only).
PTSC M&C
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5.8.3 Pickling description - Step 3

PICKLING WITH ACID is the third step of chemical cleaning, to ensure cleaning of rust and scale without causing any damage to the circuit and specially valves, more sensitive to acid than the pipes. Prior to adding acid cleaning chemical, heated water shall be circulated (steps 3-1 and 3-2) in the system to re-check for any leakage on the flanges, temporary bypass hook-ups and all hose connections. All solutions during the recirculation sequence shall be filtered. Full flow filters or equipment shall be equipped with corrosion-resistant screens capable of removing particles that are 4 micrometers or more in diameter. Acid chemical must be tested on samples of pipes to see effectiveness of cleaning and protective against further corrosion. Carbon steel piping systems: The chosen pickling product is ARA 400 (MSDS and Manufacturer Data Sheets attached in Appendix 1). ARA 400 consists of 2% glycolic acid, 2.5% citric acid, and 40% phosphoric acid. This product has a mild corrosive action, enough to remove remaining rust and scale without damaging pipe internal part. It also include a corrosion inhibitor (0.5%) and 1% non-ionic surfactant in order to ease the effect of the acids. Water used for Step 3 shall be clean tap water. Acid concentration is maintained from 5 to 7%. Neutralization to pH 7 - 9 shall be by adding ALCA (Step 3-5) of 2% concentration. Stainless steel piping systems: ARA 400 is also chosen for pickling of the stainless piping systems. Water used for Step 3 shall be clean de-mineralized water containing maximum 20 ppm of chloride. The acid concentration is maintained from 7 to 20%. Neutralization to pH 7 - 9 shall be by adding ALCA of 2% concentration (Step 3-5). Treating duration: 4 hours for carbon steel piping systems; 2 hours for stainless steel piping systems. Check frequency (Step 3-4): every 30 minutes. A sample coupon shall be placed inside the chemical mixing bath tank to evaluate the effectiveness of the cleaning process. Sample coupons shall be inspected after completion of each stage of the cleaning process. 1. The descaling solution sample shall be analyzed every hour. PTSC and BD POC representative shall witness the analysis process. 2. Check sample coupon effectiveness of cleaning. Wipes will be introduced at key areas in order to verify effectiveness of the descaling and de-rusted process. After one hour, 1 hour and half, two hours, three and four if necessary. Inspection of the test pack at the end of pickling process (Step 3-7) should look for the following indication of acceptance criteria for cleanliness at location of re-entry into pickling tank: cleanliness of 17/15/12 scale, ISO 4406:1999 (equiv. NAS 1638 class 6) for the treated piping systems. To confirm the effectiveness of the cleaning, the first test pack will be chemically cleaned with a pipe coupon installed (representing the actual pipe of the test pack). At step 3-7, this coupon will be removed from the cleaning circuit for checking of internal surface cleanliness. Important note: If iron content difference between beginning and during the pickling process (when testing is carried out, Step 3-4) exceeds 5,000 ppm (or 5,000 mg/L), the pickling shall immediately be stopped and the acid mixture be drained from the system followed by proper rinsing until pH of 7 - 8 is reached. Then the type and concentration of acids and inhibitor shall be changed. Approval of the change by customer representative shall be obtained prior to resumption of acid pickling. This situation rarely happens in practice with new piping systems.
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5.9 Specific steps for passivation/ neutralization
PICKLING COMPLETE
4-1 FILLING CIRCUIT WITH WATER 4-2 HOT WATER CIRCULATION (40 - 50 oC) a. Temperature check b. Flow velocity check
4-3 ADD ALCA TO PASSIVATE
a. pH check a. pH check b. Temperature check
4-4 PASSIVATION COMPLETE. ALL PARAMETERS STABLE 4-5 MAINTAIN PARAMETERS pH > 9.2
a. pH check
4-6 PASSIVATION COMPLETE`
5.9.1 Passivation / Neutralization control parameters

Temperature: Flow velocity: pH: Circulation time: 40 - 50 oC (Step 4-2) 90 - 150 cm/s 9 - 10 (Step 4-3) 4 hours
5.9.2 Passivation / Neutralization acceptance criteria

pH: > 9.2 (Step 4-5)
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5.9.3 Passivation / Neutralization description - Step 4

PASSIVATION / NEUTRALIZATION is the fourth step of chemical cleaning, to ensure: 1. That traces of chemicals used in previous steps are removed from internal surface of carbon steel piping systems, or 2. That a passive protective layer of chromium oxide is re-created on the internal surface of stainless steel piping systems For carbon steel piping systems: ALCA of 2% is used to neutralize the remaining chemicals on the internal surface of the pipes. For stainless steel piping systems: As the passivation chemical, ALCA of 12 - 40% shall be used. This concentration is especially designed to passivate stainless steel.
PTSC M&C
BD POC
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5.10 Nitrogen purging and preservation

Inert gas purging and preservation shall be carried out as follow. The inert gas utilized shall normally be nitrogen. 5.7.1 5.7.2 Isolate the system by closing the identified valves, blinds, etc. These will be identified on system P & ID or isometric drawing. Determine one or more connections to be used for the introduction of nitrogen into the system. Nitrogen (slightly lighter than air) should be introduced at a lower elevation to promote mixing with the air. Multiple injection locations should be considered for complex systems. Introduce nitrogen into the system and pressure the system to approximately 50 psig.
5.7.3 This
pressure should be maintained for one to three hours to allow mixing of the inert gas and air to take place. 5.7.4 Open one or more blow down valves to depressurize the system to ambient conditions. Blow down valves should also be located at low points in the system to promote the removal of free water and stratified air. Blow down valve locations should be different from pressurization locations if possible. Repressure the system to 10 psig. Isolate and seal the system.
5.7.5
5.7.6 Periodically monitor the system pressure. A positive system pressure should be maintained. Repressure the system if necessary. 5.7.7 the 5.7.8 tag. PTSC / BD POC Representative shall witness the purging process and daily to ensure positive system pressure is maintained. Preservation lines which contain preservation Nitrogen shall be identified with warning
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BD POC
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6.0 INSPECTION
6.10 6.11 The sample coupons will be the inspected to evaluate the effectiveness of the chemical. The pipe opens ends, where treatment accessible shall be visually inspected and the pipe internal surfaces checked to ensure they are free from any trace of contamination. Disposal of waste liquids
The waste liquids used shall be treated in accordance with the environmental onlywaste water with a pH 69 may be disposed to the designated drain pit. Connect the neutralization pump outlet to the waste discharge outlet. Inject the neutralization chemical into waste chemical discharge line to mix with the chemical before discharge to drain pit. will be 7.1.4 Monitor the pH value and adjust the pH value to 7 at discharge point. The pH value witnessed by PTSC Safety officer.
7.0 SPECIAL REQUIREMENT

7.1
7.1.1 regulations 7.1.2 waste 7.1.3
7.2
Safety requirement for chemical cleaning

The cleaning area shall be barricaded off to unauthorized personnel and a warning "DangerChemical Cleaning In ProgressKeep Out" must be displayed at all the area of operations.
7.2.1 notice approaches to 7.2.2
any
Cleaning personnel must know how to stop cleaning operations immediately in case of emergency.
7.2.3 7.2.4
Cleaning agents, inhibitors and other chemicals shall be transported in closed marked containers. All personnel engaged in chemical cleaning shall wear, as appropriate, protective goggles, boots, chemically resistant suit, a face mask and suitable respiratory A supply of eye wash solution shall be available in a prominentlydisplayed cabinet. A supply of running water shall be available for immediate use. Arrangements for the safe and legal disposal of cleaning agents shall be made. The cleaning circuit shall be tested for leaks before any cleaning agent is introduced. Before any chemical is introduced into the cleaning circuit, an adequate supply of neutralizing agent, where appropriate, shall be at hand for emergency use.
gloves,
protection. . 7.2.5 7.2.6 7.2.7 7.2.8 7.2.9
7.2.10 Provisions for complete draining of equipment must be provided. 7.2.11 Deadleg which would prevent neutralization must be catered for before introduction of cleaning fluid.
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8.0 RECORD
8.1 A Chemical cleaning package identifying the piping system to be chemically treated shall contain the following:
Marked up P & IDs / isometrics identifying the boundary limit of the systems to be All or blinds, fill and drain points shall be identified.
8.1.1 treated.
8.2
The Chemical Cleaning Report shall be made up as follow:

8.2.1 8.2.2 8.2.3 8.2.4 8.2.5 Leak Test & Water Flushing Records. Degreasing Records. Acid Pickling Records. Neutralization / Passivation Records. Nitrogen Blanket Pressure Check Record.
APPENDIX 1
CHEMICALS MSDS & DATA SHEETS
MATERIAL SAFETY DATA SHEET
Page : 1 Revision nr : 3 Date : 1 / 26 / 2009 Supersedes : 12 / 7 / 2007
ALCA
11.033
C - Corrosive
1. Identification of the product and the company

Trade name Type of productf Company identification : ALCA : Streamlining for cleanings heavy scheme it in high pressure. See product bulletin for detailed information. : Socit Caral B.P. N 452 F-27204 VERNON CEDEX France Tel : +33 (0) 2 32 52 42 60 - Fax: +33 (0) 2 32 52 26 74 Mail : fds@caral.fr
2. Hazards identification
Risk Phrases : Causes severe burns.
3. Information on ingredients
This product is considered to be hazardous and contains hazardous components.
Substance name Value(s) CAS nr 1310-58-3 ----7601-54-9 61789-30-8 6419-19-8 EINECS nr 215-181-3 ----231-509-8 263-049-9 229-146-5 EC index 019-002-00-8 ----E 339 III --------Classification Xn; R22 C; R35 Xi; R38-41 Xi; R36/38 Xi; R36/38 Xi; R36/38
Potassium hydroxide Dithanolamide d'acides gras Trisodium phosphate, 12 H2O Potassium cocoate Nitrilotrimethylenetris(phosphonic acid)
: : : : :
10 to 25 % 2.5 to 10 % 2.5 to 10 % < 2.5 % < 2.5 %
Other informationf
: Free from ethoxylate nonylphenol.
4. First aid measures

- Skin contact - Eye contactf - Ingestion : Take off contaminated clothing. Immediately flush the contact area with plenty of water. If soreness persists or if contamination is wide, consult a doctor. : Rinse immediately with plenty of water. Contact ophthalmologist immediately. : Rinse mouth. Do not neither get to drink nor induce vomiting. Notify immedialtely a doctor. If possible show this sheet, if not available show packaging or label.
5. Fire - fighting measures

Flammable class If product is involved in a fire : Not flammable. : All extinguishing media can be used. Do not enter fire area without proper protective equipment, including respiratory protection. Collect extinguishing water, do not drain it off in sewer pipe or natural waterways.
Socit Caral
B.P. N 452 F-27204 VERNON CEDEX France Tel : +33 (0) 2 32 52 42 60 - Fax: +33 (0) 2 32 52 26 74 Mail : fds@caral.fr
ALCA
11.033
6. Accidental release measures

Personal precautions Environmental precautions After spillage and/or leakage Cleaning method : Wear suitable personal protection equipment. : Prevent entry to sewers and public waters. Notify authorities if product enters sewers or public waters. : Mop up liquid with inert absobent material and dipose of contaminated material as waste in accordance with 13. : Finish by flushing residue with large amount of water. If necessary, neutralize with diluted acidic aqueous solution.
7. Handling and storage

Handling Storage : Inform personnel of product risks and cares to be enforced. Avoid skin or eyes contacts. Do not smoke, drink or eat during the use. Beware of dripping and spilling which can make the ground sliding. : Store in dry, cool, well-ventilated area. Store well away from strong Acids Locales floor should be waterprof and should constitute a retention basin in order to hold down possible outflow. : Polyethylene
Wrapping material
8. Exposure controls / personal protection

Personal protection
- Hand protection - Eye protection - Others Industrial hygiene
: : : :
Occupational Exposure Limits
Use rubber gloves. Safety glasses. Protection clothes Emergency eye wash fountains and safety showers should be available in the immediate vicinity of any potential exposure. Local exhaust and general ventilation must be adequate to meet exposure standards. : Potassium hydroxide : VLE [mg/m3] : 2 (2-methoxymethylethoxy)propanol : VME [mg/m3] : 308
8 =@
9. Physical and chemical properties

Physical state Colour Odour pH value (concentrated product) pH value in distilled water Initial boiling point [C] Density Solubility in water Flash point [C] : : : : : : : : : Liquid Dark Odourless 14 solution 10% : 13,3 100 1.20 Complete Not applicable.
10. Stability and reactivity

Stability Risk of violent reactions Materials to avoidf : Stabile product in normal use and storage conditions. : In case of mixing with Strong acids . : Aluminium (Al) - Attack with clearing of inflammable gaseous hydrogen.
Socit Caral
ALCA
11.033
11. Toxicological information

On product - Skin contact - Eye contactf aftereffects). - Fortuitous ingestion : Risk of serious local caustic injuries if decontamination is not quickly done. : Oculomotor attacks can be particularly serious (iritis, glaucoma, or even of disabling : Can lead to hepato-digestive reaches and serious respiratory problems.
12. Ecological information

On product On ingredients : Contained phosphate ions (less than 5 %) capable of developping enrichment of water. : Surfactant(s) easily biodegradable, according to CE regulation n648/2004. Potassium hydroxide : CL50-fish [mg/l] : 80 Nitrilotrimethylenetris(phosphonic acid) : CL50-fish [mg/l] : > 250
13. Disposal considerations

Disposal : Dispose in a safe manner in accordance with local/national regulations. Avoid release to the environment. Before waste pipe disposal, neutralise effluents at 5.5<pH<8.5.
14. Transport information

Hazard Label(s)
Shipping name - UN No. - H.I. nr : - ADR/RID Other
UN1814 HYDROXYDE DE POTASSIUM EN SOLUTION, 8, II 1814 : 80 Group : II : Class : 8 LQ 22 : : :
15. Regulatory information

Labelling Symbol(s) Contains R Phrase(s) S Phrase(s) : : : : : According to working laws. C-Corrosive. Potassium hydroxide R35 : Causes severe burns. S26 : In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S27 : Take off immediately all contaminated clothing. S36/37/39 : Wear suitable protective clothing, gloves and eye/face protection. S45 : In case of accident or if you feel unwell, seek medical advice immediately ( show the label when possible).
16. Other information

Text of R-Phrases in 2 : R22 : Harmful if swallowed. R35 : Causes severe burns. R36/38 : Irritating to eyes and skin. R38 : Irritating to skin. R41 : Risk of serious damage to eyes.
Socit Caral
ALCA
11.033
16. Other information (continued)

Revision date : All section were verified at emission date of this document.
The contents and format of this MSDS are in accordance with EEC Commission Directive 2001/58/EC. DISCLAIMER OF LIABILITY The information in this MSDS was obtained from sources which we believe are reliable. However, the information is provided without any warranty, express or implied, regarding its correctness. The conditions or methods of handling, storage, use or disposal of the product are beyond our control and may be beyond our knowledge. For this and other reasons, we do not assume responsibility and expressly disclaim liability for loss, damage or expense arising out of or in any way connected with the handling, storage, use or disposal of the product. This MSDS was prepared and is to be used only for this product. If the product is used as a component in another product, this MSDS information may not be applicable.
End of document
Socit Caral
TECHNICAL DATASHEET
ALCA
DEGREASER FOR HIGH PRESSURE HEAVY CLEANING REF. 11.033
DESCRIPTION ALCA is a degreaser for heavy cleaning jobs with high pressure machine. ALCA contains powerful alcalin detergents that eliminates mudd,oil,grease ALCA , over-active, shows an economical dosing. It contains an anti-limescale agent that prevents scaling of the device and chalky deposits on treated surfaces. ALCA contains also a corrosion inhibitor that temporarily protects iron during and after cleaning. ALCA is a bit foaming and is easily rinsed. MAIN SCOPE OF APPLICATION All heavy work with high pressure : engines, frames. Degreaser of steel and iron metal sheet before painting Degreasing of floors of garages and workshops Neutralizes acids PROCEDURE OF USE Pour ALCA in the product tank and adjust flow and pressure in order to have a 2% concentration at the hose or nozzle. After the cleaning operation, rinse with all with water. ALCA suits all high pressure cleaners :cold or hot water, or even steam. PHYSICO-CHEMICAL PROPERTIES aspect : smell : density at 20C : pH at 2%:
dark blue liquid none 1,2 12,5
Not flammable Bio degradable surfactants by over 90% Contains caustic potassium Nonylphenol ethoxyle free
CARAL Manufacturing in La chapelle Ranville BP452 27204 Vernon cedex FRANCE Tel +33 232 524 260 fax +33 232 522 674 website : www.caral.fr email : caral@caral.fr
04/02
Page : 1
Revision nr : 1 Date : 12 / 21 / 2011 Supersedes : 0 / 0 / 0
ARA 400
VIETNAM-2
1.
Identification of the substance/mixture and of the company/undertaking Product identifier

: ARA 400 : For professional use only.
: rust cleaner/descaler
1.1.
Trade name Use
1.2. 1.3.
Relevant identified uses of the substance or mixture and uses advised against Details of the supplier of the safety data sheet
: Socit Caral 5 rue du fond du val F-27600 SAINT PIERRE LA GARENNE France Tel : +33 (0) 2 32 52 42 60 - Fax: +33 (0) 2 32 52 26 74
: Centre anti- poison ORFILA 01 45 42 59 59
Type of product Company identification
1.4. Emergency telephone number

Emergency phone nr
2.
Hazards identification Classification of the substance or mixture

or EC 1999/45 : C; R34
2.1.
Classification EC 67/548
Hazard Class and Category Code Regulation EC 1272/2008 (CLP) Health hazards : Skin corrosion - Category 1B - Danger (CLP : Skin Corr. 1B) Serious eye damage - Category 1 - Danger
2.2. Label elements

Labelling EC 67/548 or EC 1999/45
Symbol(s)
R Phrase(s) S Phrase(s)
: C-Corrosive. : R34 : Causes burns. : S26 : In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 : Wear suitable protective clothing, gloves and eye/face protection. S45 : In case of accident or if you feel unwell, seek medical advice immediately ( show the label when possible).
2.3.
Other hazards
None under normal conditions.
3.
Composition/information on ingredients
: :
Value(s) <1%
Substance name
TENSIO ACTIF NON IONIQUE Phosphoric acid %
CAS nr 68439-46-3
EINECS nr -----
EC index -----
REACH
-----
Classification
Xn; R22 Xi; R41 C; R34 Skin Corr. 1B
< 35 %
7664-38-2
231-633-2
015-011-00-6
-----
Socit Caral
5 rue du fond du val F-27600 SAINT PIERRE LA GARENNE France
Tel : +33 (0) 2 32 52 42 60 - Fax: +33 (0) 2 32 52 26 74
Page : 2
Revision nr : 1 Date : 12 / 21 / 2011 Supersedes : 0 / 0 / 0
ARA 400
VIETNAM-2
3.
Composition/information on ingredients (continued)

Value(s) CAS nr 79-14-1 79-14-1
EINECS nr
Substance name
EC index ---------
REACH ---------
Classification
Xi; R36/37/38
ACIDE HYDROXYACETIQUE ACIDE CITRIC
: :
<5% <5%
---------
Xi; R36/37/38
4.
First aid measures Description of first aid measures

: In case of doubt, or lasting symptoms, call the doctor. : Take off contaminated clothing. Wash with a lot of water for 15 minutes. If soreness persists or if contamination is wide, consult a doctor. : Rinse immediately and abundantly with water by separating anat eyelids during 15 minutes at least. Consult specialist.
4.1.
General case - Skin contact - Eye contact
4.2. 4.3.
Most important symptoms and effects, both acute and delayed Indication of any immediate medical attention and special treatment needed
: Assure fresh air breathing. Allow the victim to rest. : Don't give a drink neither try to sicken. Warn immediately a doctor. If possible show this sheet, if not available show packaging or label.
No data available.
- massive inhalation - accidental ingestion
5. Fire-fighting measures 5.1. Extinguishing media

: All extinguishing media can be used.
Extinguishing media
5.2.
Special hazards arising from the substance or mixture

: Intervening parties will wear self-contained and insulating respiratory protection. Collect extinguishing water, do not drain it off in sewer pipe or natural waterways.
If product is involved in a fire
5.3.
Advice for fire-fighters

: Not flammable.
Flammable class
6.
Accidental release measures Personal precautions, protective equipment and emergency procedures
: Wear recommended personal protective equipment.
6.1.
Personal precautions
6.2.
Environmental precautions
: Prevent entry to sewers and public waters. Notify authorities if product enters sewers or public waters.
Environmental precautions
Socit Caral
5 rue du fond du val F-27600 SAINT PIERRE LA GARENNE France Tel : +33 (0) 2 32 52 42 60 - Fax: +33 (0) 2 32 52 26 74
6.3. Methods and material for containment and cleaning up

After spillage and/or leakage : Mop up liquid with inert absobent material and dipose of contaminated material in containers specially alloted for this purpose, before later destruction. Cleaning method : Finish by flushing residue with large amount of water. If necessary, neutralize withdi luted basic aqueous solution. In case of important sloughing : Dike for recovery or absorb with appropriate material.
6.4. Reference to other sections

No data available.
7. Handling and storage
7.1. Precautions for safe handling

Handling : Inform personnel of product risks and cares to be enforced. Avoid skin or eyes contacts. Do not smoke, drink or eat during the use.
7.2. Conditions for safe storage, including any incompatibilities
Storage : Close cover tightly after use. Store well away from strong Alkaline . Store in dry, cool, well-ventilated area. Locales floor should be waterprof and should constitute a retention basin in order to hold down possible outflow. Wrapping material : Polyethylene
7.3. Specific end use(s)

No data available.
8. Exposure controls / personal protection
8.1. Control parameters

Occupational Exposure Limits : Phosphoric acid ...% : VME [mg/m3] : 1 Phosphoric acid ...% : VLE [mg/m3] : 2 Phosphoric acid ...% : Persistence and degradability
8.2. Exposure controls
Personal protection - Eye protection : Chemical goggles or face shield with safety glasses.
- Hand protection : Use rubber gloves. - Others : Protection clothes Industrial hygiene : Emergency eye wash fountains and safety showers should be available in the immediate vicinity of any potential exposure. Provide local exhaust or general room ventilation.
9. Physical and chemical properties
9.1. Information on basic physical and chemical properties

Appearance Physical state : Limpid liquid Colour : clear pink Odour Odour : Weak Odour threshold : No data available. pH pH value (concentrated product) : < 2 Melting point / Freezing point Initial boiling point - boiling range Flash point Flash point [C] : Not applicable.
Socit Caral
Evaporation rate : No data available. Flammability : No data available. Explosion limits (lower - upper) : No data available. Vapour pressure : No data available. Vapour density : No data available. Relative density Density : 1.29 Solubility Solubility in water : Complete Partition coefficient : n-octanol / : No data available. water Auto-ignition temperature : No data available. Thermal decomposition : No data available. Viscosity Explosive Properties : No data available. Oxidising properties : No data available.
10. Stability and reactivity

Stabile product in normal use and storage conditions.
10.1 Possibility of hazardous reactions 10.2 Conditions to avoid

Keep away from heat. Protect from freezing.
Risk of violent reactions : In case of mixing with Strong alkalis .
10.3 Incompatible materials

No data available. Materials to avoid : Metals -
10.4 Hazardous decomposition products

No data available.
11. Toxicological information
11.1. Information on toxicological effects

- Inhalation : High level concentrations : Irritation of the respiratory tract and the other mucous membranes. - Skin contact : Risk of serious local caustic injuries if decontamination is not quickly done. - Eye contact : Possibility of incapacitating relapses if decontamination is not quickly done. - Fortuitous ingestion : Mouth, sternum and epigastric pains. Bloody vomitings . May cause burns or irritation of the linings of the mouth, throat, and gastrointestinal tract. Undesirable human health effects
12. Ecological information
12.1. Toxicity
On product : Outflow in waste pipe and waterway must be avoid. On ingredients : Surfactant(s) easily biodegradable, according to CE regulation n648/2004. Phosphoric acid ...% : Persistence and degradability
12.2. Persistence - degradability

No data available. No data available. No data available. No data available. No data available.
12.3. Bioaccumulative potential 12.4. Mobility in soil 12.5. Results of PBT and vPvB assessment 12.6. Other adverse effects Socit Socit Caral 5 rue du fond du val F-27600 SAINT PIERRE LA GARENNE France Tel : +33 (0) 2 32 52 42 60 - Fax: +33 (0) 2 32 52 26 74
13. Disposal considerations
13.1. Waste treatment methods

Disposal : Dispose of this material and its container at hazardous or special waste collection point. Before waste pipe disposal, neutralise effluents at 5.5<pH<8.5. Dispose in a safe manner in accordance with local/national regulations.
14. Transport information
14.1. UN Number
General information - UN No. : 3264
14.2. Proper shipping name

Shipping name : UN3264 LIQUIDE INORGANIQUE CORROSIF, ACIDE, N.S.A., 8, III, (E) - Proper shipping name : UN3264 LIQUIDE INORGANIQUE CORROSIF, ACIDE, N.S.A., 8, III, (E) - Proper shipping name : CORROSIVE LIQUID, ACIDIC, INORGANIC, N.O.S.
14.3. Transport Hazard Classification

Hazard Label(s) : 8 Land transport - ADR/RID : Group : III Class : 8 - H.I. nr : : 80 - ADR Class : 8 Sea transport - IMDG : Class 8 - IMDG-Marine pollution : YES - EMS-Nr : F-A S-B Air transport - ICAO/IATA : Packaging instructions cargo : 820 Packaging instructions passenger: 818 - IATA : 8
14.4. Packing group

- ADR Packing group : III LQ 7 IMO Packing group : III IATA Packing group : III
14.5. Environmental hazards

voir 14.3 voir 14.3
14.6. Special precautions for user

No data available. Other : LQ 7 Not applicable. Not applicable.
14.7. Bulk transport - annex II Marpol 73/78 - IBC
Socit Caral
15. Regulatory information
15.1. Safety, health and environmental regulations/legislation specific for the substance or mixture
Ensure all national/local regulations are observed. Labelling : According to working laws. Labelling Regulation EC 1272/2008 (CLP) Hazard pictograms Signal words : Danger Hazard pictograms code : SGH05 Hazard statements : H314 - Causes severe skin burns and eye damage. Precautionary statements - Prevention : P260 - Do not breathe dust/fume/gas/mist/vapours/spray. P264 - Wash thoroughly after handling. P280 - Wear protective gloves/protective clothing/eye protection/face protection. - Response : P301+P330+P331+P310+P321 - IF SWALLOWED : Rinse mouth. Do NOT induce vomiting. Immediately call a POISON CENTER or doctor. Specific treatment. P303+P361+P352 - IF ON SKIN (or hair) : Remove immediately all contaminated clothing. Wash with plenty of soap and water. P304+P340+P310+P320 - IF INHALED : Remove to fresh air and keep at rest in a position comfortable for breathing. Immediately call a POISON CENTER or doctor. Specific treatment is urgent. P305+P351+P338+P310+P321 - IF IN EYES : Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER or doctor. Specific treatment. P363 - Wash contaminated clothing before reuse. - Storage : P235 - Keep cool. P405 - Store locked up. - Disposal considerations : P501C - Dispose of this material and its container to hazardous or special waste collection point, in accordance with local, regional, national and/or international regulation.
15.2. Chemical Safety Assessment

No data available.
16. Other information

Revision date : All section were verified at emission date of this document. Text of R-Phrases in 3 : R22 : Harmful if swallowed. R34 : Causes burns. R36/37/38 : Irritating to eyes, respiratory system and skin. R41 : Risk of serious damage to eyes. Text of H-Phrases in 3 : H314 - Causes severe skin burns and eye damage. Note : Fiche de Scurit dite selon rglement UE n 453/2 010 du 20/05/2010 modifiant le rglement CE n 1907/2006
EndEnd of document
Socit Caral
TECHNICAL DOCUMENTATION
ARA 400
REF. 11.115 Cleaning STEEL
PRODUCT TYPE ARA 400 is designed for cleaning rust and scale on all kind of steel without mechanical intervention for
process that needs acid. ARA 400 takes effect alone, requiring no laborious and armful operations. It is formulated to clean rust and scale on steel even with high grade carbon. It includes a corrosion inhibitor that temporaly protects sensitive surface. It contains additives for fast and total cleaning of oxides, as well as sequestration of dissolved metal ions. ARA is designed to fit internationnal regulation to protect environment, international standards and U.S National Nitrate
compliance. MAIN APPLICATIONS

Steel cleaning, rust removal, descaling.
INSTRUCTIONS FOR USE Dilute ARA 400 in water from 5 % to about 20% then spray on and wait till rust and scale has disapear.
Renew operation if necessary. Rinse with clear water in order to neutralize PH. By diping, dilution of 7% is normally enough. Visual evalutaion should be done every 15 minutes in order to guaranty good results. Rinse.
PHYSICAL CHEMICAL PROPERTIES

aspect odour at 20C pH at 20 % active ingredient content surface stress at 20 C : pink liquid : mild density : 1.29 : approx. 1.5 : 60% : 31 dynes/cm (at 20 % in hard water)
non-flammable - Surface-active agents biodegradable at over 90% contain phosphoric acid. exempt from hydro-fluoric, hydrochloric and nitric acid approved for food contact (bylaw of 08/09/99) FREE OF NONYLPHENOLS OR OCTYLPHENOL ETHOXYLATES
Q - Caral is the Trademark of Avco Caral Co., Ltd. All rights reserved. Office: 28Phan Liem Street, Dakao Ward, District 1, HoChiMinh City Tel: 08.38208940 - Fax: 08.38208943 - Email: cs@qcaral.com.vn Factory: Avco Vietnam - Road No.2, Nhon Trach I IP, Nhon Trach Dist, Dong Nai Province. Tel: (84) 613 569 711/12 - Fax: (84) 613 569 713
APPENDIX 2
CLEANING EQUIPMENT LAYOUT DIAGRAM
4 -
C
cD nE
a E E E
LL
T0
c
E a'
a
w( w w !V n !u q
APPENDIX 3
REPORT FORMS (RECORDS)
LEAK TEST & WATER FLUSHING RECORD

Project Name BIEN DONG-1 Project - EPCI of Hai Thach PQP, Hai Thach WHP and Pipelines Client PTSC M&C / BIEN DONG POC Job Number Drawing number Test Pack Number
1. TOTAL WATER VOLUME LITERS
Report number Date

Page of
PIPE MATERIAL: CS
SS
(TICK IF APPLICABLE)
2. RECORD ON EVERY 30 MINUTES OF CIRCULATION FOR TWO HOURS, EXCLUDING LEAKAGE CORRECTION TIME, IF ANY.
No.
HOURS/MINUTES
FLOW VELOCITY [CM/S]]
LEAKAGE [Y/N]
REMARKS
Prepared By:
ALPHA ECC Name: Signature: Date:
Witnessed By
PTSC M&C
Witnessed By
Approved by
BIEN DONG POC
DEGREASING RECORD
Project Name BIEN DONG-1 Project - EPCI of Hai Thach PQP, Hai Thach WHP and Pipelines ClentPTSC M&C / BIEN DONG POCi Job Number Drawing number Test Pack Number
1. TOTAL WATER VOLUME 2. ALCA CHEMICAL WEIGHT LITERS KGS
Report number Date

Page of
PIPE MATERIAL: CS PIPE MATERIAL: SS
(TICK IF APPLICABLE) (TICK IF APPLICABLE)
3. RECORD ON EVERY 30 MINUTES OF CIRCULATION OF THE DEGREASING SOLUTION No. HOURS/MINUTES TEMPERATURE [ C]
o
FLOW VELOCITY [CM/S]]
ALKALINITY [pH]
OIL TRACE BY WIPE TEST [Y/N]
REMARKS
4. LAST pH (step 2-7) AT RINSING WITH WATER IS:
Prepared By:
Witnessed By
PTSC M&C
Witnessed By
Approved by
BIEN DONG POC
ACID PICKLING RECORD

Project Name BIEN DONG-1 Project - EPCI of Hai Thach PQP, Hai Thach WHP and Pipelines Client PTSC M&C / BIEN DONG POC Report number Job Number Date Drawing number Test Pack Number
1. TOTAL WATER VOLUME 2. ARA 400 CHEMICAL WEIGHT LITERS KGS Page of
3. RECORD ON EVERY 30 MINUTES OF CIRCULATION OF THE PICKLING SOLUTION No. HOURS/MINUTES TEMPERATURE [oC] FLOW VELOCITY [CM/S]] ALKALINITY [pH] Fe IONS [ppm[ ISO 4406:1999 CODE / / / / / / / / / / / / / / / / REMARKS
4. LAST ISO 4406:1999 CODE AT RINSING WITH WATER (Step 3-7) IS:
Prepared By:
Witnessed By
PTSC M&C
Witnessed By
Approved by
BIEN DONG POC
NEUTRALIZATION / PASSIVATION RECORD

Project Name BIEN DONG-1 Project - EPCI of Hai Thach PQP, Hai Thach WHP and Pipelines Client PTSC M&C / BIEN DONG POC Report number Job Number Date Drawing number Test Pack Number
1. TOTAL WATER VOLUME 2. ARA 400 CHEMICAL WEIGHT LITERS KGS Page of
3. RECORD ON EVERY 30 MINUTES OF CIRCULATION OF THE NEUTRALIZATION / PASSIVATION SOLUTION No. HOURS/MINUTES TEMPERATURE [ C] FLOW VELOCITY [CM/S]]
o
ALKALINITY [pH]
REMARKS
4. LAST pH AT MAINTAIN PARAMETERS (Step 4-5) IS:
Prepared By:
Witnessed By
PTSC M&C
Witnessed By
Approved by
BIEN DONG POC
NITROGEN BLANKET PRESSURE CHECK RECORD

Project Name BIEN DONG-1 Project - EPCI of Hai Thach PQP, Hai Thach WHP and Pipelines Client PTSC M&C / BIEN DONG POC Report number Job Number Date
Page of
No.
TEST PACK No.
LINE No.
DATE
PRESSURE [PSIG]
CHECKED BY PTSC M& C (SIGNED)
CHECKED BY BD POC (SIGNED)
REMARKS
Prepared By:
Witnessed By
PTSC M&C
Witnessed By
Approved by
BIEN DONG POC
APPENDIX 4
ORGANIZATIONAL CHART
BIEN DONG PETROLEUM OPERATING COMPANY - BIEN DONG-1 PROJECT EPCI OF HAI THACH PQP, HAI THACH WHP AND PIPELINES PTSC M&C/ALPHA ECC BD POC
SITE MANAGER Tran Linh Khang
CHEMICAL CLEANING SUPERVISOR Trinh Ngoc Nghi
SAFETY OFFICER
Troy DeFelioe
QUALITY CONTROLLER Nguyen Gia Phong
CHEMICAL TEAM LEADER Vincent Trias
EQUIPMENT TEAM LEADER Le Minh Long
I
Tran Tuan Thanh
ANALYST TREATMENT OFFICER Tran Quoc Tuyen EQUIPMENT OPERATOR Nguyen Van Chuc EQUIPMENT OPERATOR
Nguyen Quang Hoa

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BIEN DONG PETROLEUM OPERATING COMPANY

Alpha ECC Chemical Cleaning Standard Operating Procedure

PTSC M&C/ALPHA ECC

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

5.0 PROCEDURE 5.1 Gen eral Requirements

5.1.5. drawings. 5.1.6. (chemical

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

Chemical cleaning equipment and connection work

Original NAACO Vit nam NAACO Vit nam USA

Japan QME Flex Italia Technology

10. Pressure gauge for nitrogen

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

5.4 Preparation for chemical cleaning

Document No.: E1001-ALPHAECC-0023 Revision No.: B1 Date:

Alpha ECC - Standard Procedure for Chemical Cleaning

5.5 Chemical cleaning steps

PICKLING WITH ACID

5.5.2 Brief description of the process Brief description of the process

DRYING / NITROGEN PURGING

Document No.: E1001-ALPHAECC-0023 Revision No.: B1

Alpha ECC - Standard Procedure for Chemical Cleaning

5.6 Specific steps for LEAK TEST & WATER FLUSHING

CLEANING CIRCUIT FILLING

CIRCULATION LEAK TEST

WATER FLUSHING COMPLETE/ PUMP STRAINER CLEAN ? YES

a. Flow velocity check b. Leakage check

PREPARE FOR DEGREASING STEP 2

5.6.1 Leak test & water flushing control parameters

5.6.2 Leak test & water flushing acceptance criteria

Document No.: E1001-ALPHAECC-0023 Revision No.: B1

Alpha ECC - Standard Procedure for Chemical Cleaning

5.6.3 Leak test & water flushing description - Step 1

Document No.: E1001-ALPHAECC-0023 Revision No.: B1

Alpha ECC - Standard Procedure for Chemical Cleaning

5.7 Specific steps for DEGREASING

2-7 RINSING WITH WATER

a. pH check < 8.5

2-8 PREPARE TO PICKLE WITH ACID STEP 3

5.7.1 Degreasing control parameters

5.7.2 Degreasing acceptance criteria

Document No.: E1001-ALPHAECC-0023 Revision No.: B1

Alpha ECC - Standard Procedure for Chemical Cleaning

5.7.3 Degreasing description - Step 2

Document No.: E1001-ALPHAECC-0023 Revision No.: B1

Alpha ECC - Standard Procedure for Chemical Cleaning

5.8 Specific steps for PICKLING WITH ACID

3-1 FILLING CIRCUIT WITH WATER a. Temperature check c. Leak check

3-7 RINSING WITH WATER

a. Cleanliness check, ISO 4406:1999 b. pH check 7-9

3-8 PREPARE TO PASSIVATION STEP 4

5.8.1 Pickling control parameters

5.8.2 Pickling acceptance criteria