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4g

Silica Flash Column Max operating pressure 300 psi / 21 bar

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120g
Silica Flash Column Max operating 250 psi / 17 bar
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Silica Flash Column Max operating pressure 300 psi / 21 bar

12g

Silica Flash Column Max operating pressure 300 psi / 21 bar

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25g

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Silica Flash Column Max operating pressure 300 psi / 21 bar

220g

Silica Flash Column Max operating pressure 250 psi / 17 bar

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800g

40g

Silica Flash Column Max operating pressure 300 psi / 21 bar

330g

Silica Flash Column flash cartridgespsi / 17 bar Max operating 250

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80g

Silica Flash Column Max operating pressure 300 psi / 21 bar

800g

Silica Flash Column Max operating 300 psi / 21 bar

chromatography in every way

Apogee disposable flash columns are machine packed with ultra pure silica gel. The proprietary user friendly design eliminates the need for cumbersome, expensive adapters, valves, or other accessories, thus providing organic chemists fast and easy purifications with high resolution and reproducibility. 25-40m, 60 and 40-63m, 60 Ultrapure silica gel used as a standard packing sorbent, features a narrow particle size distribution, low level of fines and low trace metal content, neutral pH, tightly controlled water content and high surface area, providing scientists the desired reproducible experimental results. Proprietary dry packing technology produces uniform packed sorbent bed with less channeling effect, tighter band and symmetrical peak definition, resulting better resolution and reproducibility. Standard Luer-Lock end fittings enable quick easy connection to commercially available flash systems on the market. Innovative column design offers safety and flexibility with leak free performance.

To order: email: sales@ resolutionsys.com, visit: www.resolutionsys.com or call: 800-572-6653.

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Silica Flash Column Max operating pressure 300 psi / 21 bar

Silica Flash Column Max operating 250 psi / 17

25g

220g
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Reduce Time
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800g

40g

Silica Flash Column Max operating pressure 300 psi / 21 bar

330g

Silica Flash Column Max operating 250 psi / 17 bar

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Using Apogee flash columns significantly reduces the separationFlash Column Silica Silica Flash Column and purification times when compared to traditional glass columns. Max operating 300 psi / 21 Max operating pressure 300 psi / 21 bar

80g

Example:

800g

Reduce Costs
The separation and purification costs in time, apparatus and materials is significantly reduced when compared to traditional flash chromatography.

Reduce Risks
Pre-packed and disposable Apogee columns greatly reduce the risks to human health and the environment.

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Optimizing Flash Chromatography Purification

Thin Layer Chromatography (TLC) is often performed on crude reaction mixtures to determine optimal conditions for purifications by Flash chromatography.

1. Solvent Composition Selection and Strength Adjustment

The optimal solvent composition can be achieved by using different binary eluent which may possess the same solvent strength, but have deferent Rf value for the same pair of compounds. After the optimal solvent composition is found the solvent strength has to be optimized. The optimal eluent strength is established by adjusting the different ratio to keep the Rf value in the range of 0.15 to 0.4.

2. Band Tailing Improvement

The band tailng can be improved by adding more polar solvent into the solvent system or slightly changing the pH of the system, until the spots on the TLC plate become flat shaped and are no longer strip shaped.

3. Column Selection and Loading Capacity

The column selection can be determined by the ratio of Rf value of border upon compounds. Smaller Rf with larger ratio of Rf value means a short column of larger sample size is preferred.

To order: email: sales@ resolutionsys.com, visit: www.resolutionsys.com or call: 800-572-6653.

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Silica Flash Column Max operating pressure 300 psi / 21 bar

Silica Flash Column Max operating 250 psi / 17

25g

220g
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800g

40g

Silica Flash Column Max operating pressure 300 psi / 21 bar

330g

Silica Flash Column Max operating 250 psi / 17 bar

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80g

Silica Flash Column Max operating pressure 300 psi / 21 bar

800g

Silica Flash Column Max operating 300 psi / 21

Apogee Flash Columns

Disposable flash columns represent excellent performance and provide high resolution and reproducibility for both normal phase and reverse phase separations. Ultra pure silica gel (25-40m, 60 and 40 -63, 60) Unique proprietary dry packaging technique Standard Luer-Lock end fittings Innovative column design

Tips for Using Apogee Disposable Flash Cartridges

Apogee flash columns are disposable and for single use (for normal phase cartridges), but with proper handling, Apogee reverse phase cartridges can be reused without sacrificing performance. For multiple uses, simply air dry the flash column using compressed air and store the column in a sealed bag. For safety reasons, do not operate the flash column above the maximum pressure printed on the column body. For optimum use of the flash column, please use eluents which have been filtered throug a 0.45mm filter membrane to remove any impurities.

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HE, High Efficiency, High Pressure. 300psi max

73-HE6213-004 73-HE6213-012 73-HE6213-025 73-HE6213-040 73-HE6213-080 73-HE6213-120 73-HE6213-220 73-HE6213-330 Apogee 4g Flash Cartridge HE-HP (High Efficiency and Pressure) Ultra Pure Silica 25-40m, 60 Apogee12g Flash Cartridge HE-HP (High Efficiency and Pressure) Ultra Pure Silica 25-40m, 60 Apogee 25g Flash Cartridge HE-HP (High Efficeincy and Pressure) Ultra Pure Silica 25-40m, 60 Apogee 40g Flash Cartridge HE-HP (High Efficeincy and Pressure) Ultra Pure Silica 25-40m, 60 Apogee 80g Flash Cartridge HE-HP (High Efficiency and Pressure) Ultra Pure Silica 25-40m, 60 Apogee 120g Flash Cartridge HE-HP (High Efficiency and Pressure) Ultra Pure Silica 25-40m, 60 Apogee 220g Flash Cartridge HE-HP (High Efficeincy and High Pressure) Ultra Pure Silica 25-40m, 60 Apogee 330g Flash Cartridge HE-HP (High Efficeincy and High Pressure) Ultra Pure Silica 25-40m, 60
To order: email: sales@ resolutionsys.com, visit: www.resolutionsys.com or call: 800-572-6653.

Qty. 20 $132.00 20 $158.00 20 $179.00 20 $239.40 10 $168.50 10 $259.70 10 $485.00 10 $642.50

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Silica Flash Column Max operating pressure 300 psi / 21 bar

Silica Flash Column Max operating 250 psi / 17

25g

220g
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800g

40g

Silica Flash Column Max operating pressure 300 psi / 21 bar

330g

Silica Flash Column Max operating 250 psi / 17 bar

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80g

Silica Flash Column Max operating pressure 300 psi / 21 bar

800g

Silica Flash Column Max operating 300 psi / 21

SS-HP, Standard Silica and High Pressure Cartridges, 100psi max

73-SS6212-004 Apogee 4g SS-HP Cartridge (Standard Silica and High Pressure) Ultra Pure Silica 40-63m, 60 Apogee 12g SS-HP Cartridge (Standard Silica and High Pressure) 73-SS6212-012 73-SS6212-025 73-SS6212-040 73-SS6212-080 73-SS6212-120 73-SS6212-220 73-SS6212-330 Ultra Pure Silica 40-63m, 60 Apogee 25g SS-HP Cartridge (Standard Silica and High Pressure) Ultra Pure Silica 40-63m, 60 Apoge 40g SS-HP Cartridge (Standard Silica and High Pressure) Ultra Pure Silica 40-63m, 60 Apogee 80g SS-HP Cartridge (Standard Silica and High Pressure) Ultra Pure Silica 40-63m, 60 Apogee 120g SS-HP Cartridge (Standard Silica and High Pressure) Ultra Pure Silica 40-63m, 60 Apogee 220g SS-HP Cartridge (Standard Silica and High Pressure) Ultra Pure Silica 40-63m, 60 Apogee 330g SS-HP Cartridge (Standard Silica and High Pressure) Ultra Pure Silica 40-63m, 60

Qty. 20 $100.00 20 $132.00

20 $152.00 20 $210.00 10 $143.00 10 $212.00 10 $448.75 10 $616.25

www.resolutionsys.com

Solution Preparation System

The foundation of analytical chemistry is accurate, documented solution preparation and solvent mixing. The PhasePrep II is a new instrument designed to document and prepare solutions and mix solvents for HPLC mobile phases, titrations, extractions etc.

(800) 572 - 6653 Fax: (616) 396 - 7520 590 East 32nd Street, Holland, MI 49423 info@resolutionsys.com

www.resolutionsys.com
RSI.413.F1-E