condenser
D/F can be increased by:
D 1. Higher temperature
F
(isothermal flash)
2. Lower pressure (adiabatic
heat W flash)
Continuous Multistage Distillation
D/F = 0
D/F = 0
xD falls as D/F
increases
Continuous Multistage Distillation
D1
D0
W2
F W1
W0
y
1 f
x
xF
xD2 = 0.872 f f
xD1 = 0.763
If we have a feed
composition of 30%:
xD0 = 0.584
Temperature
determines D/F in each
stage, hence the
gradient
D1
D0
W2
F W1
W0
This approach will give us the desired separation, but each stage
needs/results in:
Why not let the vapour from the previous stage provide the
heat to vaporise some of the liquid – then we don’t need a
condenser or a ‘heater’ for each stage.
L2
Some of the top product is returned to
the top stage as a ‘reflux’
L1
Continuous Multistage Distillation
1. Energy Input and Condenser
2. Waste Stream
3. Dedicated Flash Vessel
Counter-current ‘Stripping’
process
W
Continuous Multistage Distillation
1. Energy Input and Condenser
2. Waste Stream
3. Dedicated Flash Vessel
Can we carry out the Stripping and Rectifying operations in a single piece of
equipment?
In practice, we stack the stages on top of each other – this is the standard
distillation column.
Binary Counter-Current Plate (Trayed) Column
Condenser
Reflux
Top product
Feed
Stripping section
Reboiler
Bottom product
Continuous Multistage Distillation
Liquid flows to
condenser tray beneath
F D
hea W
t
If we bubble the vapour through the liquid in the next stage, there is
insufficient time to achieve equilibrium.