Metoda Pengambilan

Contoh Air Limbah

Menurut : SNI 6989.59:2008

NADIA APRILIA (1710815120016)

Dosen Pembimbing
RIZA MIFTAHUL KHAIR, S.T., M.Eng
 Air dan Air Limbah – Bagian 59
Metoda Pengambilan Contoh Air Limbah

1. RUANG LINGKUP
Metoda ini digunakan untuk pengambilan contoh air guna
keperluan pengujian sifat fisika dan kimia air limbah. Content Here

2. ACUAN NORMATIF

SNI 06-6989.1-2004 SNI 06-6989.23-2005

Air dan air limbah – Bagian 1: Air dan air limbah – Bagian 23:
Cara uji daya hantar listrik (DHL). Cara uji suhu dengan termometer.

SNI 06-6989.11-2004
Air dan air limbah – Bagian 11: SNI 06-2420-1991
Cara uji derajat keasaman (pH) Metode pengujian kelindian
dengan menggunakan pH meter. dalam air dengan titrimetrik.

SNI 06-6989.14-2004 SNI 06-2422-1991

Air dan air limbah – Bagian 12:
Metode pengujian keasaman
Cara uji oksigen terlarut secara
yodometri (modifikasi azida).
dalam air dengan titrimetrik.
 3. ISTILAH DAN DEFINISI
3.1
air limbah
sisa dari suatu hasil usaha dan atau kegiatan yang berwujud cair

3.2
kualitas air limbah
sifat-sifat air limbah yang ditunjukkan dengan besaran, nilai atau kadar bahan pencemar atau komponen lain yang terkandung
didalamnya

3.3
contoh sesaat (grab sample)
air limbah yang diambil sesaat pada satu lokasi tertentu

3.4
contoh gabungan waktu
campuran contoh yang diambil dari satu titik pada waktu yang berbeda, dengan volume yang Sama

3.5
contoh gabungan tempat
campuran contoh yang diambil dari titik yang berbeda pada waktu yang sama, dengan volume yang sama
 3. ISTILAH DAN DEFINISI
3.6
contoh gabungan waktu dan tempat
campuran contoh yang diambil dari beberapa titik dalam satu lokasi pada waktu yang berbeda, dengan volume yang sama

3.7
contoh duplikat
contoh yang diambil dari titik pengambilan yang sama dengan rentang waktu antar pengambilan yang sekecil mungkin, duplikat
contoh digunakan untuk menguji ketelitian tata kerja pengambilan contoh

3.8
contoh yang diperkaya (spike sample)
contoh yang ditambah dengan standar yang bersertifikat dalam jumlah tertentu untuk keperluan pengendalian mutu

3.9
contoh yang terbelah (split sample)
contoh dikumpulkan dalam satu wadah, dihomogenkan dan dibagi menjadi dua atau lebih sub contoh dan diperlakukan seperti contoh
,selanjutnya dikirim ke beberapa laboratorium yang berbeda

3.10
Blanko matrik
Media bebas analit yang mempunyai matrik hampir sama dengan contoh yang akan diambil
 3. ISTILAH DAN DEFINISI
3.11
blanko media
media yang digunakan untuk mendeteksi adanya kontaminasi pada media yang digunakan dalam pengambilan contoh
3.12
blanko perjalanan
media yang digunakan untuk mengukur kontaminasi yang mungkin terjadi selama pengambilan dan transportasi contoh
3.13
Kebutuhan Oksigen Biologi/KOB (Biologycal Oxcygen Demand, BOD)
kebutuhan oksigen biokimiawi bagi proses deoksigenasi dalam suatu perairan atau air limbah
3.14
Kebutuhan Oksigen Kimiawi/KOK (Chemical Oxcygen Demand COD)
kebutuhan oksigen kimiawi bagi proses deoksigenasi dalam suatu perairan atau air limbah
3.15
nutrien
senyawa yang dibutuhkan oleh organisme yang meliputi fosfat, nitrogen, nitrit, nitrat dan ammonia
3.16
titik pengambilan contoh air limbah
tempat pengambilan contoh yang mewakili kualitas air limbah
3.17
Bak equalisasi
Bak penampungan air limbah yang bertujuan untuk menghomogenkan beban dan pengaturan airan air limbah
 4. PERALATAN

4.1 Alat Pengambilan Contoh

Option

Option

Option
4.2 Alat Ukur
Parameter Lapangan B D
C 4.4 Alat Penyimpanan Contoh
Option
4.3 Alat Penyaring
4.1.1 Persyaratan Alat Pengambil Contoh

Kapasitas alat tergantung Terbuat dari bahan yang

dari tujuan pengujian. tidak mempengaruhi
sifat contoh

Mudah dan aman di bawa Mudah dicuci dari bekas

Contoh mudah
contoh sebelumnya
dipindahkan ke dalam
botol penampung tanpa
ada sisa bahan
Tersuspensi di dalamnya
 b) Botol biasa yang diberi pemberat yang
digunakan pada kedalaman tertentu

a) Alat pengambil contoh sederhana

Dalam praktiknya, alat sederhana ini paling sering di

gunakan dan dipakai untuk mengambil air
permukaan atau air sungai kecil yang relatif dangkal.

4.1.2 Jenis Alat Pengambil Contoh

 Alat pengambil contoh secara otomatis yang
4.1.3 Alat Pengambil dilengkapi alat pengatur waktu dan volume
Contoh Air Otomatis yang diambil, digunakan untuk contoh
gabungan waktu dari air limbah, agar
diperoleh kualitas air rata-rata selama
periode tertentu.
4.2 Alat Pengukur Parameter Lapangan

DO meter atau peralatan

untuk metode Winkler Konduktimeter

pH meter Konduktimeter

Turbidimeter 1 set alat pengukur debit

Alat lapangan sebelum digunakan perlu dilakukan kalibrasi.

 4.3 Alat Pendingin 4.5 Alat Penyaring
Alat ini dapat menyimpan contoh pada Alat ini dilengkapi dengan pompa
4°C ± 2°C, digunakan untuk menyimpan isap atau pompa tekan serta
contoh untuk pengujian sifat fisika dan kimia dapat menahan saringan yang
. mempunyai ukuran pori 0,45 μm.

4.4 Alat Ekstraksi (Corong Pemisah)

Corong pemisah terbuat dari bahan

gelas atau teflon yang tembus pan
dang dan mudah memisahkan fase
pelarut dari contoh.
5. Bahan Untuk Kimia Pengawet
Bahan kimia yang digunakan untuk pengawet harus memenuhi persyaratan bahan kimia untuk analisis dan
tidak mengganggu atau mengubah kadar zat yang akan di uji

6. Persyaratan Wadah Contoh

a. b. c. d. e.

Terbuat dari bahan Dapat ditutup Bersih dan Tidak mudah Tidak berinteraksi
gelas atau plastik dengan kuat bebas pecah dengan contoh.
poli etilen (PE) dan rapat kontaminan
atau poli propilen
(PP) atau teflon
(Poli Tetra Fluoro
Etilen, PTFE)
 6.2 PersiapanWadah Contoh
4.3 Alat Pendingin 4.5 Alat Penyaring
Alat ini dapat menyimpan contoh pada Alat ini dilengkapi dengan pompa
4°C ± 2°C, digunakan untuk menyimpan isap atau pompa tekan serta
contoh untuk pengujian sifat fisika dan kimia dapat menahan saringan yang
. mempunyai ukuran pori 0,45 μm.

4.4 Alat Ekstraksi (Corong Pemisah)

Corong pemisah terbuat dari bahan

gelas atau teflon yang tembus pan
dang dan mudah memisahkan fase
pelarut dari contoh.
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