Er. Raj Kumar Kunwar pal Lect. Of chemical deptt. Che ’05’ 522020664 Packed Column Types of Packing Ring
Saddle Structured Packing Operating conditions: 1. Countercurrent flow of liquid and gas through packing:
• Generally liquid as water is flowing
downward direction through the column and gas is flowing in the upward direction through the column.
• At a fixed gas velocity, the gas-pressure
drop increases with increases liquid rate. • This is because of the reduced free cross section available for flow of gas.
• Than the liquid holdup increases rapidly
with gas rate.
• The free area for gas flow become
smeller, and pressure drop rises more rapidly. This is known as loading. • Further increase in gas velocity, the drop pressure rises more rapidly.
• In the column the liquid become the
continuous phase, and the flooding point has been reached.
• The liquid rapidly accumulate, and the
entire column may fill with liquid. this is called flooding. Tower Operation • Liquid in tower reduces space available for gas flow – Result is higher P • Loading – gas flow rate at which liquid hold-up starts to increase • Flooding – gas flow rate at which liquid rapidly accumulates and column fills with liquid Contact between Liquid & Gas • Ideally, once distributed over top of packing, liquid flows in thin films all over packing surface all the way down the tower • Actually, films are thinner in some places, thicker in others – Liquid collects in rivulets and flows along localized paths • Channeling – much of packing surface is dry, or covered by a stagnant film of liquid – Esp. at low liquid flow rates Pressure Drop and Limiting Flow Rates • Typical data for P in a packed tower P per unit of packing depth is from fluid friction • Gy = u0y – Gy = gas flow rate – u0 = superficial gas velocity y = density of gas • When the packing is dry, the line so obtained is straight and has a slope of about 1.8.
• If the packing is irrigated with a constant
flow of liquid, the relationship between pressure drop and gas flow rate initially follows a line parallel to that for dry packing.
• The pressure drop is greater than that in
the dry packing, because the liquid in the tower reduces the space available for gas flow. Flooding Velocities for Intalox Saddles in Air-Water System • The flooding velocity depends on the type and size of packing and the liquid mass velocity. Generalized Correlations for Pressure Drop in Packed Columns • A generalized and widely used correlation for estimating pressure drop in packed column is given in fig. where Gx and Gy are in lb/ft2.s, µx is in Cp, and ρx and ρy are in lb/ft3. Empirical Equation for Limiting Pressure Drop
Pflood = 0.115Fp0.7
Pflood = Pressure drop at flooding, in H2O/ft
of packing.
• Fp = packing factor, dimensionless
Mass transfer coefficients for Packed tower: • When a packed tower is operated under usual manner the rate of solute transfer can be computed from measured values of the rate of gas and liquid flow.
• Because of the impossibility of measuring
solute concentration at the gas liquid interface, the resulting rate of mass transfer can be expressed only as overall coefficient. • Overall volumetric coefficients are denoted by: Kxa, Kya, Kga, Foga, Fola, etc.
• The individual fluid mass transfer
coefficients are Kx, Ky, Fl, Fg.
To obtain individual coefficient
• the general approach has been to choose
experimental condition such that the resistance to mass transfer in the gas phase is negligible in comparison with that in the liquid. Liquid holdup • It is found that the total holdup ΦLt is made up of two parts,
ΦLt = ΦLo + ΦLs
• Where ΦLs is the static and ΦLo is the
operating, or moving, holdup, each expressed as volume liquid / packed volume. Co current flow of gas and liquid • Co current flow of gas and liquid (usually downward) through bed is used for catalytic chemical rxn between component of the fluid. • The catalyst usually same active substance supported upon granular ceramic material. • This type of arrangement are known as trickle- bed reactor. Thank you