1 Kalibrasi spektrofotometri

y
2
4
6
8
10
30

1.69897
1.39794
1.22185
1.09691
1.00000
6.4156687756

2 Data Pengamatan absorbansi larutan warna 60 dan 40 0C untuk t=10,20,30,40

%T

57.8
57.6
52.2
52.3
46.8
46.9
43.2
43.3
40.5
40.6

10
20
30
40
50

%T
10
20
30
40
50

Absorbansi

67.4
67.5
62.3
62.5
60.7
60.3
58.9
58.7
56.3
40.6

0.2381
0.2396
0.2823
0.2815
0.3298
0.3288
0.3645
0.3635
0.3925
0.3915

Absorbansi
0.1713
0.1707
0.2055
0.2041
0.2168
0.2197
0.2299
0.2314
0.2495
0.3915

t
10
20
30
40
50

t
10
20
30
40
50

Suhu Pelarut(0C)
40
40
40
40
40
40
40
40
40
40

Pikno kosong(g)

Suhu Pelarut(0C)
60
60
60
60
60
60
60
60
60
60

4 Panjang gelombang maksimum

%T
A
400
62.5
400
35
400
31.7
400
31.7
400
32.3

19.23
19.23
19.23
19.23
19.23
19.23
19.23
19.23
19.23
19.23

1
19.23
19.23
19.23
19.23
19.23
19.23
19.23
19.23
19.23
19.23

0.20412
0.45593
0.49894
0.49894
0.49080

xy

x2
3.3979
5.5918
7.3311
8.7753
10.0000
35.0961

4
16
36
64
100
220

60 dan 40 0C untuk t=10,20,30,40,50 menit

Arata-rata
0.2388
0.2819
0.3293
0.3640
0.3920

Arata-rata
0.1710
0.2048
0.2182
0.2306
0.3205

Konsentrasi Fe(ppm)

Konsentrasi Fe(ppm) rata-rata

52.35338
52.77153
64.6470824994
64.4161975369
77.8205963683
77.5630992458
87.4767369959
87.1978065685
95.2624935515
94.964990673

52.5625

Konsentrasi Fe(ppm)

Konsentrasi Fe(ppm) rata-rata

33.8166954069
33.6378408803
43.308875928
42.9222174044
46.4475858124
47.2451910722
50.0790847814
50.4894163201
55.5254458746
94.964990673

64.5316
77.6918
87.3373
95.1137

33.7273
43.1155
46.8464
50.2843
75.2452

Pikno+isi(g)

Densitas()

43.88
43.89
43.93
43.92
43.99
43.97
44.1
44.09
44.62
44.63

Pikno+isi(g)

44.11
44.1
44.21
44.22
44.25
44.27
45.02
45.05
45.17
45.18

0.9860
0.9864
0.9880
0.9876
0.9904
0.9896
0.9948
0.9944
1.0156
1.0160

Densitas()
0.99520
0.99480
0.99920
0.99960
1.00080
1.00160
1.03160
1.03280
1.03760
1.03800

rata-rata
0.9862
0.9878
0.9900
0.9946
1.0158

rata-rata
0.9950
0.9994
1.0012
1.0322
1.0378

Berat produk
24.65
24.66
24.7
24.69
24.76
24.74
24.87
24.86
25.39
25.4

Berat produk
24.88
24.87
24.98
24.99
25.02
25.04
25.79
25.82
25.94
25.95

V
BM

100
162.5

ml
g/gmol

N1
2
4
6
8
10

V2
2
4
6
8
10

Vpikno
Berat Bahan baku

25
70

ml
gram

ppm
100

L
0.1

berat
10

Fe dalam FeSO4
0.0017857143

Berat Fe yg ditimbang (g)

0.2901785714

y = -0,0849x + 1,7928

sentrasi Fe(ppm) rata-rata

52.5625
64.5316
77.6918
87.3373
95.1137

No
1
2
3
4
5

sentrasi Fe(ppm) rata-rata

33.7273
43.1155
46.8464
50.2843
75.2452

No
1
2
3
4
5

%yield

%yield rata-rata
95.27%
95.30%
95.46%
95.42%
95.69%
95.61%
96.12%
96.08%
98.13%
98.16%

%Yield

95.2850%

95.4396%

95.6522%

96.0966%

98.1449%

%yield rata-rata

96.1546%
96.1159%
96.5411%
96.5797%
96.6957%
96.7729%
99.6715%
99.7874%
100.2512%
100.2899%

g
0.1

No

No

96.1353%

96.5604%

96.7343%

99.7295%

100.2705%

f(x) = NaNx + NaN

R = 0

Chart Title
0.60000
0.50000
0.40000

Absorbansi (A)

0.30000
0.20000
0.10000
0.00000
350

400

450

500

550

Panjang gelo

1.80000
1.60000

t (menit)
10
20
30
40
50

%T
57.8
57.6
52.2
52.3
46.8
46.9
43.2
43.3
40.5
40.6

Absorbansi
0.238
0.2395
0.2823
0.2815
0.3297
0.3288
0.3645
0.3635
0.3925
0.3914

A rata-rata

f(x) = - 0.084948500
R = 0.9473245636

1.40000
1.20000

0.2387

1.00000
Absorbansi
(y)
0.80000

0.2819

0.60000
0.40000

0.3292
0.364

0.20000
0.00000
1

0.3919

2 3 4 5 6 7
Konsentrasi larutan

98.50%
98.00%

t (menit)
10
20
30
40
50

%T
67.4
67.5
62.3
62.5
60.7
60.3
58.9
58.7
56.3
40.6

Absorbansi
0.1713
0.1707
0.2055
0.2041
0.2168
0.2197
0.2299
0.2314
0.2495
0.3914

97.50%

A rata-rata

f(x) = 0.00063
R = 0.756838

97.00%

0.171
0.2048

96.50%
%yield

96.00%
95.50%
95.00%

0.2182
0.2306
0.2487

94.50%
94.00%
93.50%
5

10

15

20

Wa

98.50%

t (menit)
10
20
30
40
50

t (menit)
10
20
30
40
50

98.00%

Piknometer
kosong Piknometer isi
19.23
43.88
19.23
43.89
19.23
43.93
19.23
43.92
19.23
43.99
19.23
43.97
19.23
44.1
19.23
44.09
19.23
44.62
19.23
44.63

(gr/ml)
0.986
0.9864
0.988
0.9876
0.9904
0.9896
0.9948
0.9944
1.0156
1.016

rata-rata

Piknometer
kosong Piknometer isi
19.23
44.11
19.23
44.1
19.23
44.21
19.23
44.22
19.23
44.25
19.23
44.27
19.23
45.02
19.23
45.05
19.23
45.17
19.23
45.18

(gr/ml)
0.9952
0.9948
0.9992
0.9996
1.0008
1.0016
1.0316
1.0328
1.0376
1.038

rata-rata

97.50%
97.00%

0.9862
0.9878

96.50%
% yield

96.00%
95.50%
95.00%

0.99

94.50%
94.00%

0.9946

93.50%
0.9800

1.0158

0.995

101.0000%
100.0000%

0.9994

99.0000%

1.0012
1.0322

98.0000%
% yield

97.0000%
96.0000%

1.0378

95.0000%

94.0000%
0.98

101.0000%
100.0000%
99.0000%
98.0000%
% yield

97.0000%
96.0000%
95.0000%
94.0000%

f(
R

99.0000%
98.0000%
% yield

97.0000%
96.0000%
95.0000%
94.0000%
5

Chart Title

450

500

550

600

Panjang gelombang ()

650

700

750

800

10

00

00

f(x) = - 0.0849485002x + 1.7928247564

R = 0.9473245636

00

00
Column E

00
)
00

Linear (Column E)

00

00

00

00
1

2 3 4 5 6 7 8
Konsentrasi larutan(x)

10 11

98.50%
98.00%
97.50%
f(x) = 0.0006376812x + 0.9421835749
R = 0.7568386523

97.00%
96.50%

Column J

96.00%

Linear (Column J)

95.50%
95.00%
94.50%
94.00%
93.50%
5

10

15

20

25

30

Waktu (t)

35

40

45

50

55

98.50%
98.00%

f(x) = 0.9661835749x + 3.79170014606284E-015

R = 1

97.50%
97.00%
96.50%
% yield

96.00%
Column J

95.50%

Linear (Column J)

95.00%
94.50%
94.00%
93.50%
0.9800

0.9900

1.0000

1.0100

1.0200

Densitas ()

101.0000%
100.0000%
99.0000%

f(x) = 0.9661835749x - 2.38736675863216E-015

R = 1

98.0000%
% yield

97.0000%

Column J
Linear (Column J)

96.0000%
95.0000%
94.0000%
0.98000 1.00000 1.02000 1.04000 1.06000
Densitas ()

101.0000%
100.0000%
99.0000%
98.0000%
% yield

97.0000%
96.0000%
95.0000%
94.0000%

f(x) = 0.0011323671x + 0.9446570048

R = 0.8546611182
Column J
Linear (Column J)

99.0000%

R = 0.8546611182

98.0000%
% yield

Column J

97.0000%

Linear (Column J)

96.0000%
95.0000%
94.0000%
5

10 15 20 25 30 35 40 45 50 55
Waktu (t)