konsen Konduk Ca

0.005 0.43 0.0042 Konduk

0.01 1.11 0.0107 3
0.015 1.67 0.0161 2.5 f(x) = 104.6x - 0.011
0.02 1.96 0.0188 R² = 0.9856616746

Konduktvitas (mS)
0.025 2.62 0.025 2

1.5

1
44.967
0.5

0
0 0.005 0.01 0.015 0.02 0.025
Konsentrasi (M)
nduk

0.015 0.02 0.025 0.03

sentrasi (M)
A. Kalibrasi Pompa NaOH dan Etl Asetat
Etl Asetat
Pompa A (CH3COOC2H5) Pompa B (NaOH)
Skala Volume (L)
t (detk) Q (L/detk) t (detk) Q (L/detk) 0.000700

300 0.005 18.05 0.000277 21.50 0.000233 0.000600

350 0.005 14.69 0.000340 15.74 0.000318 0.000500
400 0.005 10.56 0.000473 12.42 0.000403

Q (L/detk)
0.000400
450 0.005 9.00 0.000556 11.01 0.000454
500 0.005 7.79 0.000642 8.76 0.000571 0.000300

0.000200

0.000100

0.000000
2

B. Kalibrasi Kurva Standar Etl Asetat dan NaOH

Konduktvitas (mS)
Konsentrasi (M)
CH3COOC2H5 NaOH Kalibrasi Kurva Standar
0.01 0.05 2.31 0.12
0.02 0.05 4.36
0.10
0.03 0.07 6.65
f(x) = 1.3x + 0.031
Konduktvitas (mS)

0.04 0.08 7.54 0.08 R² = 0.9388888889

0.05 0.10 8.27
0.06

0.04

0.02

0.00
0.005 0.01 0.015 0.02 0.025 0.03
Konsentrasi

C. Kalibrasi Kurva Standar Campuran Etl Asetat dan NaOH

Konsentrasi Konduktvitas (mS) Ca (M)

Campuran (M) Kalibrasi Kurva Standar
0.005 0.43 0.0042 3
0.01 1.11 0.0107
2.5 f(x) = 104.6x - 0.011
0.015 1.67 0.0161 R² = 0.9856616746
Konduktvitas (mS)

0.02 1.96 0.0188 2

0.025 2.62 0.0252
1.5

0.5
 2.5 f(x) = 104.6x - 0.011
R² = 0.9856616746

Konduktvitas (mS)
2

1.5

0.5

0
0 0.005 0.01 0.015
Konsentrasi Camp

D. Perhitungan
Hasil Perhitungan

Q (L/s) F NaOH
Run Cao (M) Ca (M) X
CH3COOC2H5 NaOH (mol/s)
1 0.000277 0.000277 0.025 0.0042 0.8314 6.9252E-06
2 0.000340 0.000340 0.025 0.0107 0.5713 8.5092E-06
3 0.000473 0.000473 0.025 0.0161 0.3572 1.1837E-05
4 0.000556 0.000556 0.025 0.0188 0.2463 1.3889E-05
5 0.000642 0.000642 0.025 0.0252 -0.0061 1.6046E-05

Data Perhitungan Orde Reaksi (n) dan Konstanta kecepatan Reaksi (k)
Laju volumetrik Laju reaksi (- log Ca log (-rA)
No. reaktan (L/s) rA)
1 0.000277 8170.984704 -2.3751 3.9123
2 0.000340 6545.745698 -1.9699 3.8160
3 0.000473 5207.313576 -1.7940 3.7166
4 0.000556 4514.196941 -1.7248 3.6546
5 0.000642 2936.759082 -1.5994 3.4679

0.0300
log (-rA)
0.0250
4.0000
f(x) = - 0.5113585508x + 2.7456375763 3.9000 0.0200
R² = 0.8330128302
3.8000 0.0150
CA
3.7000
0.0100
3.6000
3.5000 0.0050

3.4000 0.0000
3000.00
3.3000
3.2000
-2.5000 -2.3000 -2.1000 -1.9000 -1.7000 -1.5000 -1.3000
Axis Title
 Grafik Kalibrasi Pompa Etl Asetat
0.000700 Grafik Kalibrasi Pom
0.000600 f(x) = 1.88973677109793E-06x - 0.0002982417 0.000600
R² = 0.9903020159
0.000500 f(x) = 1.62581
0.000500 R² = 0.988975
Q (L/detk)

0.000400

Laju Alir (L/detk)

0.000400
0.000300
0.000300
0.000200
0.000200
0.000100

0.000000 0.000100
200 250 300 350 400 450 500 550
0.000000
Skala Pompa 200 250 300 350
Skala Po

ibrasi Kurva Standar Etl Asetat Kalibrasi Kurva Standar NaOH

9.00
8.00 f(x) = 151x + 1.296
R² = 0.9460477683
x + 0.031 7.00
Konduktvitas (mS)

88888889 6.00
5.00
4.00
3.00
2.00
1.00
0.00
5 0.02 0.025 0.03 0.035 0.04 0.045 0.05 0.055 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.04 0.045
Konsentrasi (M) Konsentrasi (M)

ibrasi Kurva Standar Campuran

= 104.6x - 0.011
= 0.9856616746
 = 104.6x - 0.011
= 0.9856616746

0.01 0.015 0.02 0.025 0.03

Konsentrasi Campuran (M)

V/F (L.s/mol) Ʈ (s)

Q total V (L) 1-xa xa/1-xa k = orde 2 #NAME? k= orde 1
636,804.00 7960.05 0.000554 4.41 0.1686 4.929705 0.0247722324 1.7800 0.000224
518,263.20 6478.29 0.000681 4.41 0.4287 1.332739 0.0082289532 0.8470 0.000131
372,556.80 4656.96 0.000947 4.41 0.6428 0.555622 0.0047723979 0.4419 9.488E-05
317,520.00 3969.00 0.001111 4.41 0.7537 0.326738 0.0032928969 0.2827 7.123E-05
274,831.20 3435.39 0.001284 4.41 1.0061 -0.00608 -7.080812245E-05 -0.0061 -1.78E-06

No. X
1 0.8314
0.0300
2 0.5713
0.0250 3 0.3572
f(x) = - 0.000004139x + 0.036936366 4 0.2463
0.0200 R² = 0.9541065054 -0.0061
5
0.0150
CA

0.0100

0.0050

0.0000
3000.00 4000.00 5000.00 6000.00 7000.00 8000.00 9000.00

Ʈ
 Grafik Kalibrasi Pompa NaOH

f(x) = 1.62581366288606E-06x - 0.0002547844

R² = 0.988975077

250 300 350 400 450 500 550

Skala Pompa

ndar NaOH

3 0.035 0.04 0.045 0.05 0.055

si (M)
CA0 Ʈ k Orde 2 k orde 1
0,025 7960.05 0.024772 0.000224
0,025 6478.29 0.008229 0.000131
0,025 4656.96 0.004772 9.49E-05
0,025 3969.00 0.003293 7.12E-05
0,025 3435.39 -7.08E-05 -1.78E-06
 Q (L/s) F NaOH V/F (L
CA0 (M) CA (M) X Ʈ (s)
CH3COOC2H5 NaOH (mol/s) s/mol)
0.000277 0.000277
0.000340 0.000340
0.000473 0.000473
0.000556 0.000556
0.000642 0.000642