NERACA MASSA

Produksi Dietil Eter

Basis Perhitungan = 50 kg/jam CH3OH

Komponen BM
BM Metanol (CH3OH) = 32
BM Air (H2O) = 18
BM oksigen (O2) = 32
BM formaldehid (CH2O) = 30

1. REAKTOR (R-110)
Fungsi : Sebagai tempat untuk mereaksikan metanol (CH3OH) dan udara (O2)

M1 M3

Reaktor (R-110)

M2

Komposisi bahann baku masuk Reaktor

CH3OH = 99% x 50
H2O = 1% x 50
Jumlah = 100%

Oksigen yang dibutuhkan pada reaksi dalam reaktor adalah 50 %

O2 = 50% x 50.0000

Reaksi : Konversi 99%

CH3OH + 0.5

Mula-mula 1.5469 0.78125

Reaksi 1.5314 0.7657
Sisa 0.0155 0.02
Maka :
Komposisi yang terbentuk
CH3OH methanol mula- mula = 49.5000 kg/jam
O2 Oksigen mula-mula 25.0000 kg/jam
Komposisi yang bereaksi
CH3OH 1.5314 kmol/jam x 32
Komposisi yang sisa
CH3OH 0.0155 kmol/jam x 32
O2 Sisa 0.02 kmol/jam x 18
CH2O 1.5314 kmol/jam x 30
H2O 1.53 kmol/jam x 18

Neraca Massa Reaktor (R-110)

Bahan Masuk Reaktor (kg/jam) Bahan Keluar Reaktor (kg/jam)
Komponen kg/jam Komponen
M1 M3
CH3OH 49.5000 CH2O
H2O = 0.5000 H2O
M2 CH3OH sisa
O2 25.0000 H2O
JUMLAH = 75.0000 JUMLAH =
2. Mixer (M-123)

M5
Mixer M7
(M-123)
M6

Neraca massa total : M5 + M6 + M7

Keterangan :
M5 = Aliran Water Proses masuk mixer
M6 = Aliran NaOH masuk mixer
M7 = Aliran NaOH dan H2O keluar mixer

Menghitung NaOH 35% yang diinginkan keluar dari mixer

NaOH 35% = 35.2482 kg/jam
H2O 52% = 65% x 35.2482
Menghitung NaOH 48% yang tersedia
NaOH 48% = NaOH 35%
= 35.2482 kg/jam
H2O 52% = 52% x 35.2482
= 38.1856 kg/jam
Menentukan kebutuhan H2O yang harus ditambahkan
H2O = 65.4609 - 38.1856
= 27.2754 kg/jam

Neraca Massa Mixer (M-123)

Bahan Masuk Mixer (kg/jam) Bahan Keluar Mixer (kg/jam)
NaOH 48% NaOH 35%
NaOH = 35.2482 NaOH =
H2O = 38.1856 H2O =
Water proses
H2O = 27.2754
JUMLAH = 100.7091 JUMLAH =
kg/jam = 49.5000 kg/jam = 1.546875 kmol/jam
kg/jam = 0.5000 kg/jam = 0.027778 kmol/jam
= 50.0000 kg/jam = 1.574653 kmol/jam

kg/jam = 25.0000 kg/jam = 0.78125 kmol/jam

O2 99% CH2O + H2O

H2SO4

1.5314 1.5314
1.5314 1.5314

= 1.5469 kmol/jam
= 0.7813 kmol/jam

kg/mol = 49.0050 kg/jam

kg/mol = 0.4950 kg/jam

 kg/mol = 0.27984375 kg/jam
kg/mol = 45.9422 kg/jam
kg/mol = 27.5653125 kg/jam

10)
n Keluar Reaktor (kg/jam)
kg/jam
M3
45.9422
27.5653
0.4950
0.5000
74.5025
 / 35% = 65.4609 kg/jam

/ 48%

3)
an Keluar Mixer (kg/jam)
NaOH 35%
35.2482
65.4609

100.7091