LAMPIRAN

Lampiran 1 Penentuan Kadar Abu Tepung Talas

Bobot sebelum di tanur (gram) Bobot setelah di tanur
U Kadar(%)
Bobot kosong Cawan+sampel Sampel Cawan+abu Abu
1 27.465 32.465 5.000 27.535 0.070 1.4
2 27.420 32.485 5.065 27.495 0.075 1.5
3 28.095 32.095 5.000 28.160 0.065 1.3
Rerata 1.4
Contoh Perhitungan : Ualangan 1
Gram Sampel = (Cawan+Sampel) – (Bobot Kosong)
= 32.465 – 27. 465
= 5.000 gram
Gram Abu = ( Cawan+abu) – ( Bobot Kosong)
= 27.535 – 27. 465
= 0.070 gram
Massa abu
Kadar (%b/b) =Massa sampel 𝑥100%
0.070 𝑔𝑟𝑎𝑚
= 5.000 𝑔𝑟𝑎𝑚 𝑥100%
= 1.4 %b/b

Lampiran 2 Penentuan Kadar Air Tepung Talas

Bobot sebelum di Oven Bobot Setelah di oven

Cawan U (gram) (gram) Kadar (%)
Cawan Kosong Sampel Cawan+sampel Sampel
1 1 3.980 2.095 5.875 1.895
2 3.980 2.095 5.875 1.895
3 3.980 2.095 5.875 1.895
Rerata
2 1 4.005 2.075 5.865 1.860
2 4.005 2.075 5.855 1.850
3 4.005 2.075 5.860 1.855
Rerata
3 1 3.805 2.050 5.640 1.835
2 3.805 2.050 5.645 1.840
3 3.805 2.050 5.640 1.835
Rerata
Contoh Perhitungan : Cawan 1 untuk Ulangan 1
Gram sampel (Oven) = (Cawan+Sampel) – (CawanKosong)
=5.875 – 3.980
 = 1.895 gram
𝐵𝑜𝑏𝑜𝑡 𝑏𝑎𝑠𝑎ℎ−𝐵𝑜𝑏𝑜𝑡 𝐾𝑒𝑟𝑖𝑛𝑔
Kadar air (%b/b) = 𝑥100%
𝐵𝑜𝑏𝑜𝑡 𝑏𝑎𝑠𝑎ℎ
2.095−1.895
= 2.095 𝑥100%
= 9. 5465 %b/b

Lampiran 3 Penentuan Lemak Kasar Tepung Talas

Bobot (gram)
Jenis Jumlah
labu labu+batu Kadar(%)
Sampel siklus
Sampel Kosong didih labu+ekstrak Ekstrak
Kering 2.025 107.150 108.055 108.600 0.545 68 0.2691
Basah 2.000 112.680 113.545 114.030 0.485 54 0.3790
Contoh perhitungan : sampel kering
(Labu+Ekstrak)−(Labu+batu didih)
Kadar Lemak Kasar (%) = x 100%
Bobot Sampel

108.600 gram−108.055 gram

= 𝑥 100%
2.025 garam

= 0.2691 %

Lampiran 4 Standardisasi HCl 0.01 N dengan Na2CO3 0.01 N

Volume (mL) Konsentrasi

Ulangan
Sampel Awal TE 1 TE 2 Terpakai (N)
1 10 0.00 6.40 6.80 6.80 0.01470
2 10 6.80 13.20 13.70 6.90 0.01449
3 10 13.7 20.10 20.50 6.80 0.01470
Rerata 0.01463
Indikator = Jingga Metil
Perubahan warna = Kuning - Merah
Reaksi = 2HCl + Na2CO2 H2CO2 + 2NaCl
Contoh Perhitungan =
Penimbangan Na2CO3
Mg Na2CO3 = BE x V x N
= 53 x 50 x 0.1
= 265 mg = 0.265 gram

Pengenceran
(N x V)1 = (N x V)2
V1 x 0.1 = 100 x 0.01
 100 𝑥 0.01
V1 = 0.1
= 10 Ml

Konsentrasi HCl Ulangan 1

( V x N )HCl = ( V x N )Na2CO3
( 6.8 x N ) HCl = 10 x 0.01
10 𝑥 0.01
N HCl = 6.8
= 0.01470 N

Lampiran 5 Penentuan Kadar Protein dalam Tepung Talas

Volume (mL) Kadar (%)

sampel
Awal Akhir Terpakai Nitrogen Protein
Blanko 11.40 13.10 1.70
Kering 0.10 8.20 8.10 1.3108 8.1925
Basah 8.30 11.20 2.90 0.2458 1.5363
Indikator = Merah Metil
Perubahan warna = Kuning - Merah
Reaksi =
Destruksi = Protein ( NH4)2SO4
Destilasi = ( NH4)2SO4 + 2NaOH 2 NH3 + Na2SO4 + 2H2O
NH3 + H3BO3 NH4 + H2BO3-
+

Titrasi = H2BO3- + H+ H3BO3

Contoh Perhitungan :
𝑁𝐻𝐶𝑙 𝑥 ( 𝑉𝑠𝑎𝑚𝑝𝑒𝑙−𝑉 𝐵𝑙𝑎𝑛𝑘𝑜)0.014
%N = 𝑥 100%
𝐺𝑟𝑎𝑚 𝑆𝑎𝑚𝑝𝑒𝑙
0.01463𝑥 ( 8.1−1.70)0 𝑥 0.014
= 𝑥 100%
0.1 𝑔𝑟𝑎𝑚
= 1. 3108 %
Kadar Protein (%) = %N x 6.25
= 1.3108 x 6.25
= 8. 1925%