DIAGRAM ALIR PROSES

PRARANCANGAN PABRIK ETIL ASETAT PROSES ESTERIFIKASI DENGAN KATALIS AMBERLYST 15 PROGRAM STUDI S-1 TEKNIK KIMIA
KAPASITAS 100.000 TON/TAHUN FAKULTAS TEKNIK
UNIVERSITAS DIPONEGORO
TAHUN 2017
Cold Cold
water water
Cold
water
Cold
water DIAGRAM ALIR PRARANCANGAN PABRIK ETIL ASETAT PROSES ESTERIFIKASI
E-102
1
C-301
1
C-302 C-303 C-304 DENGAN KATALIS AMBERLYST 15 KAPASITAS 100.000 TON/TAHUN
PC PC 1 1
Hot water Hot water PC Condensate PC
90,09 78,55 Hot water Hot water
81,39 E-304 Steam 78,61 1. Abdullah Ardhi Firmansyah (21030113120075)
TC
Dikerjakan Oleh
1,1 Steam AC-301 LC AC-302 LC
2. Reza Nur Rhamadhan (21030113120032)
Condensate AC-303 LC TC AC-304 LC
66,3 3
1,1
Dosen Pembimbing Dr. I Nyoman Widiasa, S.T, M.T.
3 9
PC RC FC RC FC
E-101 50 11 RC FC RC FC

4 1,1 17
UNIT 100 (PRETREATMENT UNIT) UNIT 200 (ETHYL ACETATE T-301 : Ethyl Acetate Tank
11 1,1
P-301 81,4 SYNTHESIS UNIT) E-301 : Heater
FC 1,1
FC
E-302 84,8 FC
P-303 P-305 9 P-306 T-101 : Ethanol Tank
TC FC FC
96,2 1,1 R-201 : Reactor
M-101 D-301 D-302 T-102 : Acetic Acid Tank E-302 : Heater
Cold 1,1
Cold water
PC D-303 80,8 D-304
FC Hot water water 50 10 P-201 : Product Pump
1
TC PC P-101 : Ethanol Pump E-303 : Cooler
1 1,1 FRC
30 FRC PC 5 Steam 9 V-301 16 P-102 : Acetic Acid Pump E-304 : Heater
30 12 14
R-201 Condensate 95,6 Steam FC FC
UNIT 300 (ETHYL ACETATE E-305 : Cooler
Condensate M-101 : Static Mixer
1,2 1,3 Unit Pengolahan Limbah PURIFICATION UNIT)
1,3
Hot water 100,4 PC 1,2 E-101 : Cooler V-301 : Vaporizer
119,6 105,9
LC
TC TC 83,4 D-301 : Distillation Column (DC)
TC TC
4 P-95
E-102 : Start up Heater C-301 : Condenser
LI T-102 LI T-101 2 TC
Steam P-154 Steam P-206 Steam P-269 Steam D-302 : Distillation Column (DC)
1,08 TC C-302 : Condenser
E-301 RE-301 RE-302 D-303 : Distillation Column (DC)
68 LC LC RE-303 RE-304
LC
Condensate
LC
Condensate LC
LC
LC
LC 1 RC : Ratio Control C-303 : Condenser
Cold water Condensate Condensate D-304 : Distillation Column (DC)
P-102 E-303 30
P-201 Hot water C-304 : Condenser
TC
6 10
15
FR C : Flow Ratio Control P-301 : Refluk Pump
Condensate Steam 7
13 E-305 RE-301: Reboiler
LC : Level Control P-302 : Acetic Acid Recycle Pump
RE-302: Reboiler
1 Unit Pengolahan Limbah P-303 : Refluk Pump
P-304 P-307 TC : Temperature Control RE-303: Reboiler
P-302 FC
8 TC
T-301 LI P-304 : DC feed pump
FRC
Cold water FC : Flow Control RE-304: Reboiler
FC
Unit Pengolahan Limbah
Hot P-305 : Refluk Pump
P-101 water
Arus (Kg/jam) LI : Level Indicator P-306 : Refluk Pump
Komponen
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 : Stream Number P-307 : Product Pump
Asam asetat 0.0 11852.8 24743.3 14691.3 368.7 14322.6 12890.3 1432.3 0.0 368.7 368.7 0.1 368.6 0.0 0.0 0.0 0.0 : Pressure (atm) AC-301: Accumulator
Etanol 9658.5 0.0 11856.2 4149.7 3976.5 173.1 155.8 17.3 9437.9 2551.2 11989.1 2041.8 509.3 9426.6 11.4 1414.0 8012.6 AC-302: Accumulator
: Temperature (C)
Etil asetat 0.0 0.0 412.1 15155.0 14936.3 218.7 196.8 21.9 27092.0 215.2 27307.3 215.2 0.0 14554.2 12537.9 2183.1 12371.0 AC-303: Accumulator
Air 122.3 17.8 660.3 3675.9 3202.0 473.9 426.5 47.4 217.5 3103.9 3321.4 93.8 3010.2 140.5 77.0 21.1 119.4 AC-304: Accumulator
Jumlah 9780.8 11870.6 37671.9 37671.9 22483.5 15188.3 13669.5 1518.8 36747.4 6239.1 42986.5 2351.0 3888.1 24121.2 12626.3 3618.2 20503.0