LAMPIRAN

NERACA MASSA
Perhitungan Neraca Massa
Nama Alat
Fungsi

Mixer
Pencampuran H3PO4(s) dengan Pure Water

Kode Alat
Mixer-101

Neraca Masa Total

F3 = Phosporic Acid 85% x 0.05% CPO (Patent, tahun)
= 0.0566138 kgmol/jam
F2 = (Water 15% x 0.05% CPO)/100%= 0.0084921 kgmol/jam
F1 + F2 = F3
F1 = 0.0566138 0.0084921
= 0.0481218 kgmol/jam
Input

Output
Komponen
F1
F2
F3
Komposisi Laju Alir Komposisi Laju Alir Komposisi Laju Alir
H3PO4
1
0.0481
0.85
0.0481
Water
1
0.0085
0.15
0.0085
Sub Total
1
0.0481
1
0.0085
1
0.0566
Total
0.0566 kgmol/jam
0.0566 kgmol/jam

Perhitungan Neraca Massa

Nama Alat
Fungsi

Mixer
Pencampuran H3PO4(l) dengan CPO dan Bleaching Earth

Neraca Masa Total

F4: 113.22767 kgmol/jam
F5: 1% wt CPO
Input = Output
F6 = F3 + F4 + F5.(1)
F6 = 0.0566138 + 113.22767 + 1.1322767
= 114.4165594 kgmol/jam
Water
0.002 F4 = X F6(2)
0.002 (113.22767) = X (114.4165594)
X = 0.0000198%
Trigliserida
0.9563 F4 = X F6.(3)
0.9563 F 4
X=
F6
X = 94.64%
FFA
0.04 F4 = X F6...(4)

Kode Alat
Mixer-102

X=

0.04 F4
F6

X = 3.96%
Fosfatida
0.00003 F4 = X F6...(5)
0.00003 F 4
X=
F6
X = 0.00297%
Tocopherol
0.0008 F4 = X F6...(6)
0.0008 F 4
X=
F6
X = 0.0791%

Caroten
0.00055 F4 = X F6...(7)
0.00055 F 4
X=
F6
X = 0.0544%
Fe
0.0001 F4 = X F6...(8)
0.0001 F 4
X=
F6
X = 0.000989%
Gum
0.00031 F4 = X F6...(9)
0.00031 F 4
X=
F6
X = 0.0306%
Bleching Earth
1 F5 = X F6...(10)
1 F4
X= F
6
X = 1%
H3PO4
0.85 F3 = X F6...(11)
0.85 F 2
X=
F6
X = 0.042%

Kompon
en
Trigliseri
da
FFA

F3
Kompos Laju
isi
Alir

Water
Phospati
da
Tocopher
ol
Caroten

0.15

0.00
85

Fe
Gum
Bleching
Earth
H3PO4
Sub
Total
Total

Input
F4
Kompos Laju
isi
Alir
108.27
0.9563
96
0.04
4.5291

F5
Kompos Laju
isi
Alir
-

0.002

0.2265

0.00003

0.0034

0.0008
0.0005

0.0906
0.0623

0.00001
0.00031

0.0011
0.0351

1.13
23

113.22
77

0.85
1

0.04
81
0.05
66

1.13
23

114.4166 kgmol/jam

Perhitungan Neraca Massa

Output
F6
Komposis
Laju
i
Alir
108.27
0.9464
96
0.0396
4.5291
0.002
2.96883E05

0.2265

0.0008
0.0005
9.89609E06
0.0003

0.0906
0.0623

0.01

1.1442

0.0034

0.0011
0.0351

0.000420
584
0.0481
1.000029 114.41
688
66
114.4166
kgmol/jam

Nama Alat
Fungsi

Bleaching Tank
Menghilangkan Impurities pada CPO

Neraca Masa Total

F6 = F7
F7=114.4165594 kgmol/jam
Input = Output
F6 = F3 + F4 + F5.(1)
F6 = 0.5 + 1000 + 10
= 1010.5 kgmol/jam
Water
0.002 F4 = X F6(2)
0.002 (1000) = X (1010.5)
X = 0.198%
Trigliserida
0.9563 F4 = X F6.(3)
0..9563 F 4
X=
F6
X = 94.64%
FFA
0.04 F4 = X F6...(4)
0.04 F4
X=
F6
X = 3.96%
Phospatida

Kode Alat
R-101

0.00003 F4 = X F6...(5)
0.00003 F 4
X=
F6
X = 0.00297%
Tocopherol
0.0008 F4 = X F6...(6)
0.0008 F 4
X=
F6
X = 0.0791%
Caroten
0.00055 F4 = X F6...(7)
0.00055 F 4
X=
F6
X = 0.0544%
Fe
0.0001 F4 = X F6...(8)
0.0001 F 4
X=
F6
X = 0.000989%
Gum
0.00031 F4 = X F6...(9)
0.00031 F 4
X=
F6
X = 0.0306%

Bleching Earth
1 F5 = X F6...(10)
1 F4
X= F
6
X = 10.105%
H3PO4
0.85 F3 = X F6...(11)
0.85 F 2
X=
F6
X = 0.042%
Komponen

Input
F6

Output
F7

Trigliserida
FFA
Water
Phospatida
Tocopherol
Caroten
Fe
Gum
Bleching Earth
Spent Earth
H3PO4
Sub Total
Total

Nama Alat
Fungsi

Komposisi
Laju Alir
0.9464
108.2796
0.0396
4.5291
0.0019
0.2265
2.96883E-05
0.0034
0.0007
0.0906
0.0005
0.0623
9.89609E-06
0.0011
0.0003
0.0351
0.01
1.1442
0.0004
0.0481
1
114.4166
114.4166 kgmol/jam

Komposisi
Laju Alir
0.9464
108.2796
0.0396
4.5291
0.0019
0.2265
0.0003
0.0351
0.0109
1.2459
0.0004
0.0481
0.999544132
114.4166
114.4166 kgmol/jam

Perhitungan Neraca Massa

Niagara Filter & Bag Filter
Memisahkan Fatty Acid dengan Gliserin

Kode Alat
F-101 & F-102

Perhitungan Neraca Massa

Nama Alat
Fungsi

Reaktor
Memisahkan Fatty Acid dengan Gliserin

Kode Alat
R-101

Diketahui:
F10 = 324.83889 kgmol/jam
F11 = 325.03585 kgmol/jam
F12 = 112.8387616 kgmol/jam
Water
0.2% F9 = X F12...(1)
0.002 F 9
X=
F12
X = 0.9%
FFA
4% F9 = X F12...(2)
4 F9
X= F
12
X = 4.04%

Perhitungan Neraca Massa

Nama Alat
Fungsi

Evaporator
Memisahkan Gliserin dengan Water

Diketahui:
F11: 325.03585 kgmol/jam

Kode Alat
EV-101

(Glyserin) 0.3298 F11 = 0.001 F21 + 0.99 F22 (x1)

(Water)

0.6702 F11 = 0.99 F21 + 0.01 F22 (x99)

F21 =

10394.6465
98.901

F21 = 105.10259 kgmol/jam

0.3298 (325.03585) = 0.001 (105.10259) + 0.99 F22
F22 = (107.19628 0.10510259)/0.99
F22 = 219.93326 kgmol/jam

Perhitungan Neraca Massa

Nama Alat
Fungsi

Kolom Destilasi
Memisahkan Myristic Acid dengan Asam Lemak

Diketahui:
F12: 112.8387615 kgmol/jam
Myristic Acid

Kode Alat
D-101

0.02563 F12 = 0.9996 F14...(2)

0.02563 F 12
F14 =
0.9996
F14 = 2.819752331 kgmol/jam
F12 = F13 + F14
F13 = F12 F14
F13 = 110.0190092 kgmol/jam

Perhitungan Neraca Massa

Nama Alat
Fungsi

Destilasi
Memisahkan Palmitic Acid dengan Fatyy Acid

Diketahui:
F14 = 110.0190092 kgmol/jam
Palmitic Acid
0.4659 F14 = 0.9998 F15...(1)
0.467 F 14
F15 =
0.9998
F15 = 51.216902697 kgmol/jam
F14 = F15 + F16

Kode Alat
D-102

F16 = F14 F15

F16 = 58.81205065 kgmol/jam
Stearic Acid
0.4656 F14 = X F16...(1)
0.4036 F 14
X=
F 16
X = 0.08711 %
Oleic Acid
0.4036 F15 = X F16...(1)
0.4036 F 15
X=
F 16
X = 75.49 %
Linoleic Acid
0.08278 F15 = X F16...(1)
0.08278 F 15
X=
F 16
X = 0.1549 %

Nama Alat
Fungsi

Perhitungan Neraca Massa

Reaktor Fixed Bed
Mereaksikan Palmitic Acid dengan gas Hidrogen

Diketahui:
F15 = 51.21602697 kgmol/jam
Asam Palmitat + 2H2 Alkohol lemak + H2O
51.20695859

102.4320539

Kode Alat
R-102

50.69488897

101.3897779

50.69488897

50.69488897

0.521137997

1.02413916

50.69488897

50.69488897

F18 = F15 + F17

F18 = 153.6299441
Hidrogen
F17 = 102.4320539
Water
0.000177061 F15 = X F18
X = 0.670019479

Perhitungan Neraca Massa

Nama Alat
Fungsi

Destilasi
Memisahkan Air dan Fatty Alcohol

Diketahui:
F20: 51.15151515 kgmol/jam
0.32998F18 - 0.001F19 = 50.64 (x999)
0.67002F18 - 0.999F19 = 0.511515152 (x1)
F18 = (50588.84848/ 328.98)
F18 = 153.7748449 kgmol/jam

Kode Alat
D-103

F18 F20 = F19

F19 = 102.6233297 kgmol/jam