TITRASI

PENGENDAPAN
KELOMPOK 2: 01 IVANNI MEIDA PRATAMA
31181052

02 ADELIA NUR FAUZIAH

31181063

03 ALIEFIA SYERA
31181080
TITRASI
PENGENDAPAN
Titrasi pengendapan atau Argentometri adalah penetapan
kadar zat yang didasarkan atas reaksi pembentukan endapan
dari komponen zat uji dengan titran larutan titer perak
nitrat.Titrasi pengendapan merupakan titrasi yang melibatkan
pembentukan endapan dari garam yang tidak mudah larut
antara titran dan analit.

Reaksi yang mendasari Titrasi Pengendapan :

Ag+ + Cl– → AgCl (s)
Ag+ + I– → AgI (s)
• Infographic Style

PRINSIP

Prinsip titrasi pengendapan adalah

REAKSI PENGENDAPAN yang cepat
mencapai kesetimbangan pada setiap
penambahan titran; tidak ada pengotor
yang menganggu dan diperlukan
indikator untuk melihat titik akhir titrasi.
Metode Titrasi Pengendapan
Metode Mohr : Pembentukan dari sebuah endapan
berwarna
Ion kromat dipergunakan sebagai indikator, dengan
kemunculan awal endapan perak kromat berwarna
kemerah-merahan diambil sebagai titik akhir dari titrasi

Metode Volhard : Pembentukan kompleks berwarna

Pengendapan dari perak tiosianat dalam larutan asam
nitrit, dengan ion besi(III) dipergunakan untuk
mendeteksi kelebihan ion tiosianat

Metode Fajans : Penggunaan Indikator Adsorbsi

Adsorbsi dari sebuah komponen organik berwarna pada
permukaan sebuah endapat dapat menyebabkan
pergeseran elektronik dalam molekul yang mengubah
warnanya.
Larutan Standar : AgNo3

Metode Mohr
Menitrasi Ion halida seperti NaCl
Titran : AgNo3
Indikator : K2CrO4
Reaksi TAT : endapan berwarna merah-bata

Metode Volhard
Menitrasi ion-ion halogenida
Titran :NH4SCN/KSCN
Indikator : larutan Fe3+
Reaksi TAT : endapan putih

Metode Fajans
Menitrasi ion klorida
Indikator : asam lemah/basa lemah, contoh : fluoresein
Reaksi TAT : diserap oleh endapan AgX dan menyebabkan
endapan berwarna merah muda
 Prosedur kerja
A. Pembuatan Larutan Standar AgNO3

B. Penentuan Kadar Nacl dalam garam dapur

METODE MOHR
Titran : AgNO3
Indikator : K2CrO4
Sampel : Nacl
Hasil Pengamatan
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 Perhitungan Titrasi
Diketahui :
V. Agno3 : 20 ml (volume akhir setelah titrasi)
N. Agno3 : 0.05 N
BE. Nacl : 58.5 mol/g
Berat sampel : 0.5 g (500 mg)

Ditanyakan :
Kadar Nacl (%) :

Penyelesaian :

% Nacl : fp x N.AgNo3 x V.AgNo3 x BE.Nacl

X 100 %
Berat sampel

125/25 x 0.05 x 20 x 58.5

X 100 % = 58.5 %
500
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