LABORATORIUM KIMIA ANALISIS

DEPARTEMEN KIMIA FARMASI

FAKULTAS FARMASI
UNIVERSITAS GADJAH MADA

WORKSHEET PRAKTIKUM KIMIA ANALISIS 1

Acara Praktikum : ...........................................................................................................................

Tanggal Praktikum : ………………………………………………………………………………...
Nama : ...........................................................................................................................
No. Mahasiswa : ...........................................................................................................................
Golongan : ...........................................................................................................................
Dosen : ...........................................................................................................................
Pembimbing

A. PRINSIP DAN REAKSI (Pembakuan dan Penetapan Kadar)

LAB KA-FORM-KA 1-003 Rev. 00 Effective Date June 2, 2020

B. DATA DAN PERHITUNGAN

1. Pembuatan Larutan Baku

Perhitungan:
(bisa dikosongkan apabila tidak diminta dalam tugas)

2. Larutan Baku

Bobot penimbangan
Nama senyawa baku
No. senyawa baku primer Volume titran (mL)
primer
(mg)
1.  __ __ __ . __ __ __ . __ __
2.  __ __ __ . __ __ __ . __ __
3. __ __ __ . __ __ __ . __ __

Perhitungan:

No. Nama larutan baku Normalitas (N)

1.   __ . __ __ __ __
2.   __ . __ __ __ __
3. __ . __ __ __ __
Rata-rata __ . __ __ __ __

3. Penimbangan Tablet
Tablet Bobot tablet Tablet Bobot tablet Tablet Bobot tablet

LAB KA-FORM-KA 1-003 Rev. 00 Effective Date June 2, 2020

 (mg) (mg) (mg)
1 __ __ __ . __ 11 __ __ __ . __ 21 __ __ __ . __
2 __ __ __ . __ 12 __ __ __ . __ 22 __ __ __ . __
3 __ __ __ . __ 13 __ __ __ . __ 23 __ __ __ . __
4 __ __ __ . __ 14 __ __ __ . __ 24 __ __ __ . __
5 __ __ __ . __ 15 __ __ __ . __ 25 __ __ __ . __
6 __ __ __ . __ 16 __ __ __ . __ 26 __ __ __ . __
7 __ __ __ . __ 17 __ __ __ . __ 27 __ __ __ . __
8 __ __ __ . __ 18 __ __ __ . __ 28 __ __ __ . __
9 __ __ __ . __ 19 __ __ __ . __ 29 __ __ __ . __
10 __ __ __ . __ 20 __ __ __ . __ 30 __ __ __ . __
Bobot penimbangan keseluruhan tablet __ __ __ __ . __
Rata-rata __ __ __ . __

4. Orientasi

a. Penimbangan sampel
  Bobot penimbangan (mg)
Kertas timbang + sampel __ __ __ . __ mg  
Kertas timbang + sisa sampel __ __ __ . __ mg -  
Sampel __ __ __ . __ mg  

b. Volume titran = __ __ . __ __ mL
c. Hasil orientasi =

5. Pengujian
a. Penimbangan sampel
Sampel 1 Bobot penimbangan (mg)
Kertas timbang + sampel __ __ __ . __ mg  
Kertas timbang + sisa
__ __ __ . __ mg -
sampel  
Sampel __ __ __ . __ mg  

Sampel 2 Bobot penimbangan (mg)

Kertas timbang + sampel __ __ __ . __ mg  
Kertas timbang + sisa
__ __ __ . __ mg -
sampel  
Sampel __ __ __ . __ mg  

LAB KA-FORM-KA 1-003 Rev. 00 Effective Date June 2, 2020

 Sampel 3 Bobot penimbangan (mg)
Kertas timbang + sampel __ __ __ . __ mg  
Kertas timbang + sisa
__ __ __ . __ mg -
sampel  
Sampel __ __ __ . __ mg  

Sampel 4 Bobot penimbangan (mg)

Kertas timbang + sampel __ __ __ . __ mg  
Kertas timbang + sisa
__ __ __ . __ mg -
sampel  
Sampel __ __ __ . __ mg  

b. Volume titran

 Blanko Volume (mL) Sampel  Volume (mL)

Titran 1 __ __ . __ __ Titran 1 __ __ . __ __
Titran 2 __ __ . __ __ Titran 2 __ __ . __ __
Titran 3 __ __ . __ __ Titran 3 __ __ . __ __
Titran 4 __ __ . __ __ Titran 4 __ __ . __ __

Perhitungan:

LAB KA-FORM-KA 1-003 Rev. 00 Effective Date June 2, 2020

C. KESIMPULAN

D. DAFTAR PUSTAKA

Yogyakarta, ........................

(..........................................)

LAB KA-FORM-KA 1-003 Rev. 00 Effective Date June 2, 2020