DAFTAR ISI

KATA PENGANTAR ..................................................................................................

ABSTRAK .................................................................................................................. ii
DAFTAR ISI .............................................................................................................. iii
DAFTAR GAMBAR ................................................................................................. vi
BAB I PENDAHULUAN ........................................................................................... 1
1.1 Latar Belakang ......................................................................................... 1
1.2 Perumusan Masalah ..................................................................................
1.3 Tujuan Percobaan ......................................................................................
1.4 Manfaat Percobaan ....................................................................................
1.5 Ruang Lingkup Percobaan ....................................................................... 2
BAB II TINJAUAN PUSTAKA ............................................................................... 3
2.1 AnalisaKualitatif....................................................................................... 3
2.2 Jenis Analisa...............................................................................................
2.2.1 Analisa Kation...................................................................................
2.2.2 Analisa Anion....................................................................................
2.3 Tahapan Analisa........................................................................................ 5
2.4 Identifikasi Kation Berdasarkan H2S.........................................................
2.4.1 Reagensia ......................................................................................
2.4.2 Reaksi Warna Untuk Fe.................................................................
2.5 Aplikasi Analisa Kualitatif dalam IndustriAnalisis Kualitatif Bahan
Kimia (BKO) Glibenkamid dalam Sediaan Jamu Diabetes yang Beredar
Di Pasaran ...............................................................................................
BAB III METODOLOGI PERCOBAAN ............................................................... 10
3.1 Bahan Percobaandan Fungsi .................................................................. 10
3.1.1 Asam Klorida (HCl) ..................................................................... 10
3.1.2 Asam Nitrat (HNO3) ......................................................................10
3.1.3 Asam Sulfida (H2S) ...................................................................... 11
3.1.4 Aquadest (H2O) ............................................................................. 11
3.1.5 Kalium Heksasianoferat (K4Fe(CN)6) .......................................... 12
3.1.6 Kalium Tiosianat (KCNS) ............................................................ 12
3.1.7 Natrium Hidroksida (NaOH) ........................................................ 13
3.2 Peralatan Percobaandan Fungsi ............................................................. 14
3.2.1 Tabung Reaksi........................................................................... 14
3.2.2 Beaker Glass ............................................................................14
3.2.3 Gelas ukur ................................................................................ 14
3.2.4 Pipet Tetes................................................................................. 15
3.2.5 Rak Tabung............................................................................... 15
3.2.6 Lakmus...................................................................................... 15
3.2.7 Bunsen...................................................................................... 15

3.2.8 Penjepit Tabung........................................................................ 16

3.3 Prosedur Percobaan ................................................................................ 17
3.4 Flowchart Percobaan .............................................................................. 18
BAB IV HASIL DAN PEMBAHASAN ..................................................................20
4.1 Hasil IdentifikasiKation Fe denganReaksiWarna................................... 20
4.1.1 Sampel Air Parit Gelanggang Mahasiswa......................................20
4.1.2 Sampel Air Minuman Pocari Sweat.............................................. 20
4.1.3 Sampel Minuman Bir Bintang...................................................... 20
4.2 Pembahasan Identifikasi Kation Fe dengan Reaksi Warna..................... 20
4.2.1 Sampel Air Parit Gelanggang Mahasiswa......................................21
4.2.2 Sampel Air Minuman Pocari Sweat...............................................22
4.2.3 Sampel Minuman Bir Bintang...................................................... 22
BAB V KESIMPULAN DAN SARAN ................................................................... 24
5.1 Kesimpulan .............................................................................................24
5.2 Saran ....................................................................................................... 24
DAFTAR PUSTAKA ................................................................................................ 26
LAMPIRAN A FOTO HASIL PERCOBAAN.................................................... LA-1
L.A.1 Hasil Percobaan dengan Sampel Air Parit Gelanggang Mahasiswa. .LA-1
L.A.2 Hasil Percobaan dengan Sampel Air Minuman Pocari Sweat...........LA-1
L.A.3 Hasil Percobaan dengan Sampel Minuman Bir Bintang...................LA-2
LAMPIRAN B CURRICULUM VITAE .............................................................LB-1

DAFTAR GAMBAR
Gambar2.1 Flowchart Aplikasidalam Industri Analisis Kualitatif Bahan Kimia
(BKO) Glibenkamid dalam Sediaan Jamu Diabetes yang Beredar Di
Pasaran.....................................................................................................
Gambar 3.1 Tabung Reaksi...................................................................................... 14
Gambar3.2 Beaker Glass......................................................................................... 14
Gambar3.3 Gelas ukur ............................................................................................ 14
Gambar3.4 Pipet Tetes............................................................................................. 15
Gambar3.5 Rak Tabung .......................................................................................... 15
Gambar3.6 Lakmus................................................................................................. 15
Gambar3.7 Bunsen.................................................................................................. 15

Gambar3.8 Penjepit Tabung.................................................................................... 16

Gambar3.12 Flowchart Reaksi Warna Fe dengan Reagensia K4Fe(CN)6
dan KCNS.............................................................................................
Gambar A.1 Foto Hasil Percobaan Sampel Air Parit Gelanggang Mahasiswa
(a) Menggunakan pereaksi K4Fe(CN)6 dan (b) menggunakan
pereaksi KCNS........................................................................... LA-1
Gambar A.2 Foto Hasil PercobaanSampel Air Pocari Sweat
(a)menggunakanpereaksi K4Fe(CN)6 dan (b) menggunakanpereaksi
KCNS................................................................................................LA-1
Gambar A.3 Foto Hasil Percobaan Sampel Bir Bintang (a) menggunakan pereaksi
K4Fe(CN)6 dan (b) menggunakanpereaksi KCNS............................ LA-2