kode KA-42

gs2000

LABORATORIUM KALIBRASI SUHU

BALAI PENELITIAN & PENGEMBANGAN SISTEM KALIBRASI & METROLOGI
PUSLITBANG KIM - LIPI

DATA KALIBRASI No. order : E - 990506

Tanggal : 9 Mei 2000 suhu ruang : {22 + 1}oC

Pelaksana : Agus Budiman kelembaban : {65 + 5}%

Nama alat : Termometer Tahanan Pt100

Merek/Pabrik : ---
Tipe/ No. seri : UH1-Pt100-0200
Rentang ukur : (0 ~ 250) oC
Resolusi : 0.01 o
C

Hasil Pengukuran

alt (Ohm) std (oc) std (Ohm) sd n

99.971 0.327 25.536 0 5
110.2912 26.281 28.1642 0.001095 5
119.6826 50.255 30.5736 0.000548 5
129.6526 75.832 33.1246 0.000548 5
140.7048 104.303 35.9408 0.001643 5
151.027 131.216 38.5802 0.002739 5
159.9606 154.664 40.862 0.00493 5
169.3316 179.41 43.2522 0.00493 5
193.5478 244.566 49.458 0.00164 5
212.5158 296.406 54.3056 0.00164 5

sum = 10
kode KA-42
gs2000

Kobservasi Kprediksi {Kob.- Kpred.}2 SEE

#REF! #REF! #REF! #REF!
std (Ohm) #VALUE! #VALUE! #VALUE!
25.536 0 652.087296 25.536
28.1642 0 793.2221616 28.1642
30.5736 0 934.745017 30.5736
#REF! #REF! #REF! #REF!
#REF! #REF! #REF! #REF!
#REF! #REF!
fak. x = 1 dibuat dengan pers. determinan gauss eleminasi
k a0 a1 a2 a3
#REF! 1 #REF! #REF! #REF!
std (Ohm) 1 std (oc) #VALUE! #VALUE!
25.536 1 0.327 0.106929 0.034966
28.1642 1 26.281 690.691 18152.05
30.5736 1 50.255 2525.565 126922.3

K a0 a1 a2 a3 k
0 0 0 0 0 p1 = 0
0 0 0 0 0 0
0 0 0 0 0 0
0 0 0 0 0
0 0 0 0 0
0 0 0 0 0

pa kor-int
50 0
100 0
150 0
200 0
250 0
300 0
350 0
400 0
450 0
500 0
kode KA-42
gs2000

Kobservasi Kprediksi {Kob.- Kpred.}2SEE

#REF! #REF! #REF! #REF!
std (Ohm) #VALUE! #VALUE! #VALUE!
25.536 0 652.0873 25.536
28.1642 0 793.2222 28.1642
30.5736 0 934.745 30.5736
#REF! #REF! #REF! #REF!
#REF! #REF! #REF! #REF!
#REF! #REF!
fak. x = 1
a0 a1 a2 a3 k a0 a1
#REF! #REF! #REF! #REF! #REF! #REF! #REF! #REF!
#VALUE! #VALUE! #VALUE! #VALUE! #VALUE! #VALUE! #VALUE! #VALUE!
8.350272 0.327 0.106929 0.034966 0.011434 2.730539 0.106929 0.034966
740.1833 26.281 690.691 18152.05 477054 19452.76 690.691 18152.05
1536.476 50.255 2525.565 126922.3 6378479 77215.61 2525.565 126922.3

a0 a1 a2 a3 k a0 a1 a2 a3
0 0 0 0 0 0 0 0 0 p2 =
0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0
0 0 0 0 0
kode KA-42
gs2000

fak. x = 1
a2 a3 k a0 a1 a2 a3
#REF! #REF! #REF! #REF! #REF! #REF! #REF!
#VALUE! #VALUE! #VALUE! #VALUE! #VALUE! #VALUE! #VALUE!
0.011434 0.003739 0.892886 0.034966 0.011434 0.003739 0.001223
477054 12537456 511237.9 18152.05 477054 12537456 3.3E+008
6378479 3.2E+008 3880471 126922.3 6378479 3.2E+008 1.6E+010

k a0 a1 a2 a3 k a0 a1 a2 a3
0 0 0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0 0 0
kode KA-42
gs2000

k a0 a1 a2 a3
p3 = 0 0 0 0 0
kode KA-42
gs2000

LABORATORIUM KALIBRASI SUHU

BALAI PENELITIAN & PENGEMBANGAN SISTEM KALIBRASI & METROLOGI
PUSLITBANG KIM - LIPI

ANALISA DATA No. order : E - 990506

Pelaksana : Agus Budiman

Nama alat : Termometer Tahanan Pt100

Merek/Pabrik : ---
Tipe/ No. seri : UH1-Pt100-0200

Ketidakpastian tipe A.

penunjukan k. p-berulang SEE d. bebas d. bebas k. gabungan f. cakupan k. perluasan

alat C o Upb. V(n-1). Veff. Ug. K95. U95.
0 0 0 4 7.1415804 0.1152760029 2.3646243 0.2725844321
0.001095 0.001095 0.0004896989 4 7.1418381 0.115277043 2.3646243 0.2725868916
0.000548 0.000548 0.0002450731 4 7.1416449 0.1152762634 2.3646243 0.2725850481
0.000548 0.000548 0.0002450731 4 7.1416449 0.1152762634 2.3646243 0.2725850481
0.001643 0.001643 0.0007347719 4 7.1421606 0.1152783446 2.3646243 0.2725899693
0.002739 0.002739 0.001224918 4 7.143193 0.1152825107 2.3646243 0.2725998206
0.00493 0.00493 0.002204763 4 7.1468044 0.1152970851 2.3646243 0.2726342835
0.00493 0.00493 0.002204763 4 7.1468044 0.1152970851 2.3646243 0.2726342835
0.00164 0.00164 0.0007334303 4 7.1421585 0.1152783361 2.3646243 0.2725899491
0.00164 0.00164 0.0007334303 4 7.1421585 0.1152783361 2.3646243 0.2725899491

sumber ketidakpastian distribusi faktor d.bebas ketidakpastian av = 0.2725979675

ketidakpastian Ui. nilai C
o
probabilitas cakupan V standar C
o

interpolasi Uint. 0.1235023 normal 1.0767386 7 0.1147003749

C terhadap t

Ketidakpastian tipe B.

sumber ketidakpastian distribusi faktor d.bebas ketidakpastian

ketidakpastian Ui. nilai C
o
probabilitas cakupan V standar oC
sertifikat alat
standar {prt}
Uss. 0.005 normal 1.96
~ 0.0098

alat ukur
standar
Uas. 0.00015 segi
empat
akar. 3
~ 8.66025E-005

{ bridge}
media
kalibrasi
Umk. 0.003 segi
empat
akar. 3
~ 0.0017320508

{tamson bath}
penunjukan
alat
Upa. 0.01 segi
empat
akar. 3
~ 0.0057735027

histerisis Uh. 0 segi

empat
akar. 3
~ 0
kode KA-42
gs2000

LABORATORIUM KALIBRASI SUHU

BALAI PENELITIAN & PENGEMBANGAN SISTEM KALIBRASI & METROLOGI
PUSLITBANG KIM - LIPI

LAPORAN KALIBRASI No. order : E - 990506

SPESIFIKASI ALAT SPESIFIKASI STANDAR

Nama : Termometer Tahanan Pt100 Nama : PRT
Merek/Pabrik : --- Merek/Pabrik : Rosemount
Tipe/No.seri : UH1-Pt100-0200 Tipe/No.seri : R.326
Rentang ukur : (0 ~ 250) oC

Prosedur kalibrasi berdasarkan ASTM E 644-91

Hasil Kalibrasi
tanggal : 9 Mei 2000
suhu ruang : {22 + 1}oC
kelembaban : {65 + 5}%
penunjukan W Rt
alat oC Rt/Ro (Ohm)
0 1 100.184
25 1.0991207504 110.1143132556
50 1.1975025841 119.9705988849
75 1.2951455012 129.7528568879
100 1.3920495016 139.4610872646
125 1.4882145853 149.095290015
150 1.5836407524 158.6554651391
175 1.6783280028 168.1416126369
200 1.7722763366 177.5537325083
225 1.8654857537 186.8918247535
250 1.9579562542 196.1558893724

Catatan : -- Alat ini dikalibrasi dengan menggunakan Termometer Tahanan Platina (TTP) standar yang
tertelusur ke standar nasional dan mengacu ke skala suhu internasional (ITS-90).
-- Hubungan nilai W terhadap t, adalah t = a {W-1} + b {W-1} 2
###dimana, a = 255.7596623921
b= -1.413120007
-- Ketidakpastian pengukuran + 0.27oC, dan dinyatakan pada tingkat kepercayaan 95%

Serpong, 16 Mei 2000

Menyetujui,
kode KA-42
gs2000

Hidayat WR. Agus Budiman

ka. laboratorium suhu pelaksana kalibrasi
kode KA-42
gs2000

persamaan hasil interpolasi suhu,

t = a {w-1} + b {w-1}2 + c {w-1}3 .................... + n {w-1}n.

dimana ratio tahanan, W = Rt / Ro

dengan konstanta,
a1 = 255.7597
a2 = -1.41312
a3 = 7.395615

SEE = 0.123502

grafik data kalibrasi

350

300

250

200 Column M
suhu

Column N
150

100

50

0
0.0000 100.0000 200.0000 300.0000 400.0000

tahanan

Ro = 100.184
temp.oc resistance ratio w rt
0 100
25 115.59
50
75
100
125
150
175
200
225
250
275
300
kode KA-42
gs2000
kode KA-42
gs2000

resitance stdoc predoc see

99.9710 0.3270 0 0.123594383
26.2810 26.2810 26.38751 0.040255499
50.2550 50.2550 50.37401 0.044980708
75.8320 75.8320 75.81101 0.00793214
104.3030 104.3030 103.9762 0.123502317
131.2160 131.2160 130.25 0.365129279
154.6640 154.6640 152.9649 0.642213096
179.4100 179.4100 176.7677 0.998708788
244.5660 244.5660 238.163 2.420106167
296.4060 296.4060 286.1368 3.881409306

pers. determinan gauss eleminasi

suhu rt/ro-1
k a1 a2 a3
0.327 0 0 0
26.281 0.103231937 0.010657 0.0011
50.255 0.19717318 0.038877 0.007666
75.832 0.296902102 0.088151 0.026172
104.303 0.407456162 0.166021 0.067646
131.216 0.510708105 0.260823 0.133204
154.664 0.60007002 0.360084 0.216076
179.41 0.693807204 0.481368 0.333977
244.566 0.936039451 0.87617 0.82013
296.406 1.125774475 1.267368 1.426771

sum = 1263.26 4.871162637 3.549519 3.032741 sum =

1/a0 a1/a0 a2/a0 a3/a0

k a1 a2 a3 k
4503.602 17.29028304 14.77297 13.83536 p1 = -19.63694
4483.965 17.29028304 12.59908 10.76477 -8.91602
2812.817 10.76477116 10.08155 9.988268 -4.837871
2803.901 10.76477116 9.197518 8.613769
2255.602 8.61376908 8.534067 8.76335
2250.764 8.61376908 8.067069 7.992426
kode KA-42
gs2000
kode KA-42
gs2000

fak. x = 1
k a1 a2 a3 k a1 a2 a3
0 0 0 0 0 0 0 0
2.713039 0.010657 0.0011 0.000114 0.280072 0.0011 0.000114 1.2E-005
9.908938 0.038877 0.007666 0.001511 1.953777 0.007666 0.001511 0.000298
22.51468 0.088151 0.026172 0.007771 6.684656 0.026172 0.007771 0.002307
42.4989 0.166021 0.067646 0.027563 17.31644 0.067646 0.027563 0.011231
67.01307 0.260823 0.133204 0.068029 34.22412 0.133204 0.068029 0.034743
92.80923 0.360084 0.216076 0.129661 55.69204 0.216076 0.129661 0.077805
124.476 0.481368 0.333977 0.231716 86.36231 0.333977 0.231716 0.160766
228.9234 0.87617 0.82013 0.767674 214.2814 0.82013 0.767674 0.718573
333.6863 1.267368 1.426771 1.606222 375.6555 1.426771 1.606222 1.808244

924.5435 3.549519 3.032741 2.840259 sum = 792.4503 3.032741 2.840259 2.813978

a1 a2 a3 k a1 a2 a3 k a1
0 -2.173892 -3.070591 19.38246 0 1.921792 2.988012 p2 = 2.022757 0
0 -0.884033 -1.374499 17.3597 0 1.921792 2.714504 0.113079 0
0 -0.466998 -0.770924 4.276838 0 0.412841 0.681523
4.163759 0 0.412841 0.641888
kode KA-42
gs2000
kode KA-42
gs2000

fak. x = 1
k a1 a2 a3
0 0 0 0
0.028912 0.000114 1.2E-005 1.2E-006
0.385232 0.001511 0.000298 5.9E-005
1.984688 0.007771 0.002307 0.000685
7.05569 0.027563 0.011231 0.004576
17.47854 0.068029 0.034743 0.017743
33.41912 0.129661 0.077805 0.046689
59.91879 0.231716 0.160766 0.111541
200.5758 0.767674 0.718573 0.672612
422.9034 1.606222 1.808244 2.035675

sum = 743.7502 2.840259 2.813978 2.889581

a2 a3 k a1 a2 a3 k a0
0 0.273508 0.030928 0 0 0.010841 p3 = -0.049244 0
0 0.039635 0.080172 0 0 0.010841

5.649766 2.852995
kode KA-42
gs2000
kode KA-42
gs2000

a1 a2 a3
0 0 0
kode KA-42
gs2000
 wreg3

persamaan hasil interpolasi ratio tahanan,

w = 1 + a {t/100} + b {t/100}2 + c {t/100}3 .................... + n {t/100} n.

dimana ratio tahanan, W = Rt / Ro

dengan konstanta,
a1 = 0.397961
a2 = -0.005911
a3 = -3E-005

SEE = 0.000711

grafik data kalibrasi

2.5

2
ratio tahanan

1.5 Column K
Column L
1

0.5

0
0.0000 0.5000 1.0000 1.5000 2.0000 2.5000 3.0000 3.5000
ratio suhu

alt oC alt t/100 rt/ro

0 0 1
25 0.25 1.099121
50 0.5 1.197503
75 0.75 1.295146
100 1 1.39205
125 1.25 1.488215
150 1.5 1.583641
175 1.75 1.678328
200 2 1.772276
225 2.25 1.865486
250 2.5 1.957956
275 2.75 2.049688
300 3 2.140681

Page 19
 wreg3

t/100 w obs w pred see

0.0033 1.0000 1.001301 0.000492
0.2628 1.1032 1.10418 0.000358
0.5026 1.1972 1.198502 0.000502
0.7583 1.2969 1.298382 0.000559
1.0430 1.4075 1.408654 0.000453
1.3122 1.5107 1.51201 0.000492
1.5466 1.6001 1.601362 0.000488
1.7941 1.6938 1.694954 0.000434
2.4457 1.9360 1.93792 0.000711
2.9641 2.1258 2.127645 0.000707

pers. determinan gauss eleminasi

suhu rt/ro-1
k a1 a2 a3
1 1 0.00327 1.1E-005 3.5E-008
1.103232 1 0.26281 0.069069 0.018152
1.197173 1 0.50255 0.252557 0.126922
1.296902 1 0.75832 0.575049 0.436071
1.407456 1 1.04303 1.087912 1.134724
1.510708 1 1.31216 1.721764 2.25923
1.60007 1 1.54664 2.392095 3.69971
1.693807 1 1.7941 3.218795 5.77484
1.936039 1 2.44566 5.981253 14.62811
2.125774 1 2.96406 8.785652 26.0412

sum = 14.87116 10 12.6326 24.08416 54.11896 sum =

1/a0 a1/a0 a2/a0 a3/a0

k c a1 a2 a3 k
218.7804 126.326 240.8416 541.1896 1335.931 p1 = 30.91891
187.8614 126.326 159.5826 304.2455 683.6632 38.93059
565.8446 304.2455 683.6632 1687.628 4410.417 107.7813
526.914 304.2455 580.0465 1303.409 3217.477
2531.9 1303.409 3217.477 8408.497 22777.85
2424.119 1303.409 2928.862 7229.918 18894.54

Page 20
 wreg3

fak. x = 1
k a1 a2 a3 k
0.00327 0.00327 1.1E-005 3.5E-008 1.1E-010 1.1E-005 1.1E-005
0.28994 0.26281 0.069069 0.018152 0.004771 0.076199 0.069069
0.601639 0.50255 0.252557 0.126922 0.063785 0.302354 0.252557
0.983467 0.75832 0.575049 0.436071 0.330682 0.745783 0.575049
1.468019 1.04303 1.087912 1.134724 1.183552 1.531188 1.087912
1.982291 1.31216 1.721764 2.25923 2.964471 2.601083 1.721764
2.474732 1.54664 2.392095 3.69971 5.72212 3.82752 2.392095
3.03886 1.7941 3.218795 5.77484 10.36064 5.452018 3.218795
4.734894 2.44566 5.981253 14.62811 35.77539 11.57994 5.981253
6.300923 2.96406 8.785652 26.0412 77.18768 18.67631 8.785652

21.87804 12.6326 24.08416 54.11896 133.5931 sum = 44.79241 24.08416

c a1 a2 a3 k c a1 a2 a3
0 81.25897 236.9441 652.2676 3203.712 0 8419.78 24551.34 67585.77
0 103.6166 384.2185 1192.941 3163.46 0 8419.78 31221.2 96937.15
0 288.6148 1178.579 3883.303 11235.94 0 29905.29 110891.1 344300.4
11167.93 0 29905.29 122120.3 402374.7

Page 21
 wreg3

fak. x = 1
a1 a2 a3 k a1 a2
3.5E-008 1.1E-010 3.7E-013 3.5E-008 3.5E-008 1.1E-010 3.7E-013
0.018152 0.004771 0.001254 0.020026 0.018152 0.004771 0.001254
0.126922 0.063785 0.032055 0.151948 0.126922 0.063785 0.032055
0.436071 0.330682 0.250762 0.565542 0.436071 0.330682 0.250762
1.134724 1.183552 1.23448 1.597075 1.134724 1.183552 1.23448
2.25923 2.964471 3.88986 3.413037 2.25923 2.964471 3.88986
3.69971 5.72212 8.850059 5.919795 3.69971 5.72212 8.850059
5.77484 10.36064 18.58802 9.781465 5.77484 10.36064 18.58802
14.62811 35.77539 87.49443 28.3206 14.62811 35.77539 87.49443
26.0412 77.18768 228.7889 55.35772 26.0412 77.18768 228.7889

54.11896 133.5931 349.1298 sum = 105.1272 54.11896 133.5931 349.1298

k c a1 a2 a3 k c a1
p2 = 40.25248 0 0 -6669.857 -29351.39 -453625 0 0
68.01127 0 0 -11229.19 -58074.32 -452003 0 0

0.381641 -0.000392

Page 22
 wreg3

a3
1.2E-015
0.000329
0.016109
0.190158
1.2876
5.104119
13.68786
33.34877
213.9816
678.144

945.7606

a2 a3 k c a1 a2 a3
74897059 3.9E+008 p4 = -1622.846 0 0 0 57755189
74897059 3.3E+008

Page 23