LAPORAN PRAKTIKUM ANALISIS KUANTITATIF

TITRASI REDOKS

DISUSUN OLEH:
Kelompok 5

Indra Nopian F.16.056

Khairun Sa’adah F.16.058
Kriscika Guspani F.16.060
Mahdiaty F.16.062
Novia Henjani F.16.067

PROGRAM STUDI FARMASI

SEKOLAH TINGGI ILMU KESEHATAN SARI MULIA

BANJARMASIN

2018

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 DAFTAR ISI

HALAMAN SAMPUL..................................................................................................i
DAFTAR ISI.................................................................................................................ii
PERCOBAAN I IODOMETRI.....................................................................................1
BAB I PENDAHULUAN .......................................................................................... 1
A. Latar Belakang ......................................................................................... 1
B. Kompetensi Praktikum ............................................................................. 2
BAB II TINJAUAN PUSTAKA ................................................................................. 3
A. Deskripsi Bahan Praktikum ...................................................................... 3
B. Deskripsi Bahan Hasil Praktikum ............................................................ 7
BAB III METODE PRAKTIKUM ........................................................................... 12
A. Alat ......................................................................................................... 12
B. Bahan ...................................................................................................... 12
C. Prosedur Kerja ........................................................................................ 12
BAB IV HASIL .......................................................................................................... 15
A. Pembuatan Larutan Natrium Tiosulfat (Na2S203) ................................. 15
B. Perhitungan Normalitas pembakuan dari Natrium Tiosulfat (Na2S2O3)15
C. Perhitungan Kadar Cu (Tambaga) % b/b ............................................... 17
BAB V PEMBAHASAN ........................................................................................... 19
BAB VI KESIMPULAN ............................................................................................ 22
DAFTAR PUSTAKA ................................................................................................. 23
JAWABAN PERTANYAAN .................................................................................... 24

PERCOBAAN IV IODIMETRI ................................................................................ 26

BAB III METODE PRAKTIKUM ........................................................................... 26
A. Alat ......................................................................................................... 26
B. Bahan ...................................................................................................... 26
C. Prosedur Kerja ........................................................................................ 26
BAB IV HASIL .......................................................................................................... 29
A. Perhitungan berat KI.............................................................................. 27
B. Perhtiungan larutan baku I2 ................................................................... 27

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 C. Perhitungan Normalitas pembakuan dari Iodium .................................. 27
D. Perhitungan kadar asam askorbat (Vitamin C) ...................................... 29

BAB V PEMBAHASAN .......................................................................................... 31

BAB VI KESIMPULAN ............................................................................................ 34
DAFTAR PUSTAKA ................................................................................................. 35
JAWABAN PERTANYAAN .................................................................................... 36
PERCOBAAN 3 BROMATOMETRI ....................................................................... 36
BAB III METODE PRAKTIKUM ............................................................................ 36
A. Alat ......................................................................................................... 36
B. Bahan ...................................................................................................... 36
C. Prosedur Kerja ........................................................................................ 36
BAB IV HASIL .......................................................................................................... 40
A. Perhitungan Pembuatan Kalium Bromat (KbrO2) .................................. 40
B. Pembuatan Larutan Natrium Tiosulfat (Na2S2O3) ................................. 40
C. Perhitungan Normalitas pembakuan dari Natrium Tiosulfat) ................. 40
D. Perhtiungan Kadar Isoniazid (INH) % b/b .............................................. 42
BAB V PEMBAHASAN ........................................................................................... 44
BAB VI KESIMPULAN ............................................................................................ 48
DAFTAR PUSTAKA ................................................................................................. 49
JAWABAN PERTANYAAN .................................................................................... 52

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