BAB III

NERACA MASSA DAN NERACA ENERGI

2.1 Neraca Massa

2.1.1 Neraca Massa Mixer (M-01)

Komponen Massa (Kg/Jam)

H₂O 10.299,074880
Total 10.299,074880

3
M-01 6
5
Komponen Massa (Kg/Jam)
Massa (Kg/Jam) H₂O 10.299,202283
Komponen
H₂O 0,127403 Na₂CO₃ 1.270,335218
Na₂CO₃ 1.270,335218 NaCl 3,567284
NaCl 3,567284 Total 11.573,104784
Total 1.274,029904

TOTALinput : 11.573,104784 Kg/Jam TOTALoutput : 11.573,104784 Kg/Jam

2.1.2 Neraca Massa Akumulator (M-02)

Komponen Massa (Kg/Jam)
C₇H₇Cl 6,383594 Komponen Massa (Kg/Jam)
C₇H₇Cl 2.669,186713 2 H₂O 10.299,202283
C₇H₆Cl₂ 6,383594 M-01 8 C₇H₇Cl 6,383594
7
Total 2.681,953901 C₇H₇Cl 2.669,186713
C₇H₆Cl₂ 6,383594
Na₂CO₃ 1.270,335218
Komponen Massa (Kg/Jam)
NaCl 3,567284
H₂O 10.299,202283
Total 14.255,058685
Na₂CO₃ 1.270,335218
NaCl 3,567284
Total 11.573,104784

TOTALinput : 14.255,058685 Kg/Jam TOTALoutput : 14.255,058685 Kg/Jam

2.1.3 Neraca Massa Reaktor
Komponen Massa (Kg/Jam)
HCl 8,693595
Komponen Massa (Kg/Jam)
CO₂ 411,806465
H₂O 10.299,202283
H₂O 7,374958
C₇H₇Cl 6,383594
C₇H₇Cl 0,023195
C₇H₇Cl 2.669,186713 C₇H₇Cl 0,321539
C₇H₆Cl₂ 6,383594 C₇H₈O 0,156487
Na₂CO₃ 1.270,335218 C₇H₆Cl₂ 0,005109
NaCl 3,567284 C₁₄H₁₄O 0,000136
Total 14.255,058685 Na₂CO₃ 12,471168
NaCl 0,000002
17 Total 440,852653
10
Reaktor
23

Komponen Massa (Kg/Jam)

HCl 11,896366
CO₂ 39,405464
H₂O 10.107,126496
C₇H₇Cl 6,360399
C₇H₇Cl 1,741096
C₇H₈O 2.156,158211
C₇H₆Cl₂ 6,378485
C₁₄H₁₄O 111,962525
Na₂CO₃ 171,205889
NaCl 1.201,937333
Total 13.814,172265

TOTALinput : 14.255,058685 Kg/Jam TOTALoutput : 14.255,024918 Kg/Jam

2.1.4 Neraca Massa Dekanter (DC-01)

Komponen Massa (Kg/Jam) Komponen Massa (Kg/Jam)

HCl 11,896366 HCl 0,525186
CO₂ 39,405464 CO₂ 25,261899
H₂O 10.107,126496 H₂O 0,450305
C₇H₇Cl 6,360399 C₇H₇Cl 0,001500
C₇H₇Cl 1,741096 C₇H₇Cl 0,000243
C₇H₈O 2.156,158211 C₇H₈O 0,010122
C₇H₆Cl₂ 6,378485 C₇H₆Cl₂ 0,000330
C₁₄H₁₄O 111,962525 C₁₄H₁₄O 0,000008
Na₂CO₃ 171,205889 Na₂CO₃ 0,576577
NaCl 1.201,937333 Total 26,826170
Total 13.814,172265 26
25
Komponen Massa (Kg/Jam)
HCl 0,849510
DC-01 28
CO₂ 4,517845
H₂O 167,745216
C₇H₇Cl 5,678842
Komponen Massa (Kg/Jam) 27 C₇H₇Cl 1,621294
HCl 10,521671 C₇H₈O 1.919,146153
CO₂ 9,625720 C₇H₆Cl₂ 5,806204
H₂O 9.938,930975 C₁₄H₁₄O 56,370411
C₇H₇Cl 0,680057 Na₂CO₃ 1,242071
C₇H₇Cl 0,119559 NaCl 89,924304
C₇H₈O 237,001936 Total 2.252,901850
C₇H₆Cl₂ 0,571952
C₁₄H₁₄O 55,592105
Na₂CO₃ 169,387241
NaCl 1.112,013029
Total 11.534,444244

TOTALinput : 13.814,172265 Kg/Jam TOTALoutput : 13.814,172265 Kg/Jam

2.1.5 Neraca Massa Menara Destilasi (MD-01)

Komponen Massa (Kg/Jam)

HCl 0,849510 Komponen Massa (Kg/Jam)
CO₂ 4,517845 HCl 0,849510
H₂O 167,745216 CO₂ 4,517845
C₇H₇Cl 5,678842 33 H₂O 167,745216
C₇H₇Cl 1,621294 C₇H₇Cl 5,678842
C₇H₈O 1.919,146153 C₇H₇Cl 1,621293
C₇H₆Cl₂ 5,806204 C₇H₈O 1.919,133957
C₁₄H₁₄O 56,370411 C₇H₆Cl₂ 5,805869
31 MD-01
Na₂CO₃ 1,242071 C₁₄H₁₄O 0,421961
NaCl 89,924304 Na₂CO₃ 1,242071
Total 2.252,901850 NaCl 0,031229
Total 2.107,047793

32

Komponen Massa (Kg/Jam)

C₇H₇Cl 0,000001
C₇H₈O 0,012196
C₇H₆Cl₂ 0,000335
C₁₄H₁₄O 55,948450
NaCl 89,893075
Total 145,854057

TOTALinput : 2.252,901850 Kg/Jam TOTALoutput : 2.252,901850 Kg/Jam

2.1.6 Neraca Massa Menara Destilasi (MD-02)

Komponen Massa (Kg/Jam) Komponen Massa (Kg/Jam)

HCl 0,849510 HCl 0,849510
CO₂ 4,517845 CO₂ 4,513979
H₂O 167,745216 H₂O 166,427625
C₇H₇Cl 5,678842 35 C₇H₇Cl 4,600320
C₇H₇Cl 1,621293 C₇H₇Cl 1,179651
C₇H₈O 1.919,133957 C₇H₈O 32,693179
C₇H₆Cl₂ 5,805869 C₇H₆Cl₂ 1,419643
C₁₄H₁₄O 0,421961 Na₂CO₃ 1,235780
Na₂CO₃ 1,242071 34 MD-02 Total 212,917943
NaCl 0,031229
Total 2.107,047793

36

Komponen Massa (Kg/Jam)

HCl 0,000344
CO₂ 0,003866
H₂O 1,317592
C₇H₇Cl 1,078522
C₇H₇Cl 0,441641
C₇H₈O 1.886,440962
C₇H₆Cl₂ 4,386224
C₁₄H₁₄O 0,421731
Na₂CO₃ 0,006291
NaCl 0,031215
Total 1.894,129789

TOTALinput : 2.107,047793 Kg/Jam TOTALoutput : 2.107,047793 Kg/Jam

2.2 Neraca Energi

3 Neraca Energi Heat Exchanger (HE-01)

Qc = 6.616.498,525 J/s

7 8
Tc,in = 30 oC Tc,out = 95 oC
H-01
22 21
Th,out = 101,3 Co Th,in = 143,4 oC

Qh = - 6.616.498,525 J/s
4 Neraca Energi Pompa (P-01)
W = 18.425,1683 J/s

Tin = 30oC 15 16 Tout = 30oC

P-02
Pin = 1 atm Pout = 5,92 atm