data area standar vitamin C

No.
1
2
3
4
5
6

Konsentrasi(ppm)
4
8
12
16
20
24

Area
345714
529311
831167
1054009
1375856
1696461

RT
1.99
2.11
2.13
2.13
2.13
2.13

N0.
1
2
3

jenis sampel
twister
kratingdaeng
nitros extra jos

Area
1218007
1642470
2526245

Vol. Kemasan
350 ml
150 ml
50 ml

Area
302216
1909345
2409495
1850403
1973426
2349406

RT

data area standar vitamin C

No.
1
2
3
4
5
6

Konsentrasi(ppm)
4
8
12
16
20
24

2.01
2.05
2.02
2.1
2.1
1.98

hitung kadar vit C gunakan persamaan regresi pertama bisa dibuar kofesien r
dengan membuang salah satu data
Tulis dijurnal tidak perlu diemail lagi

Kurva Kalibrasi Vit.C

buang no 1

Axis Title

area

2000000
1500000
1000000
500000

2000000
1500000
1000000
500000

0
0

kadar Vit C

ma bisa dibuar kofesien regresinya o,997?

0
6

10
8

10

15
20
Konsentrasi (ppm)
12 14 16 18 20 22
Axis Title

Chart Title
Axis Title

RT
2.04
2.32
2.14

f(x) = 67972.9428571429x + 20465.1333

R = 0.9930755067
f(x) = 71974.725x - 54234.8
R = 0.9963433659

3000000
2500000

f(x) = 70493.5785714285x + 812138.4000

R = 0.4698737679

2000000
1500000
1000000
500000
0
0

10

15
20
Axis Title

25

alibrasi Vit.C 1
buang no 1

428571429x + 20465.1333333332
5067
974.725x - 54234.8
63433659
Column D

15
20
Konsentrasi (ppm)
2 14 16 18 20 22
Axis Title

25
24

26

hart Title

5714285x + 812138.400000001
79

15
20
Title

Column D

25

30

30

Data area standar Natrium benzoat 2

No.
1
2
3
4
5
6

N0.
1
2
3

Konsentrasi(ppm)
20.4
40.8
61.2
81.6
102
122.4

Jenis Sampel
twister
kratingdaeng
nitros extra jos

Area
239105
429530
689971
1104704
1153163
1317157

RT (menit)
4.98
4.4
4.6
4.56
4.5
4.72

Area
7282953
991464
7043020

Vol. Kemasan
350 ml
150 ml
50 ml

RT
4.96
4.67
4.61

buat perhitungannya dulu gunakan persamaan regresi dengan r minimal 0,997 buat da

Konsentrasi(ppm)
20.8
41.6
62.4
83.2
104

Area
268569
582431
801516
1133979
1396307

RT
4.38
4.44
4.66
4.53
4.59

f(x) = + 1396307
R = 0

Kurva ka

Luas Area

No.
1
2
3
4
5

1500000
1000000
500000
0
80

100

Axis Title

Chart Title
1400000

f(x) = 11170.7170868347x + 24682.4666666

R = 0.9606577577

1200000
1000000
800000
600000

kadar Vit C

400000
200000
0
0

20

40

60
80
Axis Title

dengan r minimal 0,997 buat data ke 4

f(x) = + 1396307
R = 0
Luas Area

Kurva kalibrasi standar Natrium benzoat

1500000
1000000
500000
0
80

100

120

140
160
Konsentrasi (ppm)

180

200

220

100

120

140

rt Title

8347x + 24682.4666666669

Column C

100

120

140

DATA PENIMBANGAN ZAT STANDAR

stok 1 (100mL)
vit C = 2 mg
Na Benzoat =10,2 mg
kafein = 5 mg

Kondisi HPLC
mobile phase
stationary phase
deteksi
sistem elusi

40 ppm
204 ppm
100 ppm

Data area standar Kafein

No.
1
2
3
4
5
6

Konsentrasi(ppm)
10
20
30
40
50

Area
390095
966034
2643211
3297925
3334077

RT (menit)
2.61
3.13
2.97
3.02
3.17

Data area Kafein pada sampel

No.
1
2
3

No.
1
2
3
4
5

Jenis Sampel
twister
kratingdaeng
nitros extra jos

Konsentrasi(ppm)
10
20
30
40
50

Area
0
4726299
7380240

Vol. Kemasan
350 ml
150 ml
50 ml

Area
351238
2173387
1700482
3721261
4024640

RT

RT
0
2.62
2.82

2.66
2.58
2.58
2.72
2.74

Kurva Kalibrasi Ka
4000000
Area

3500000

f(x) = 82198.55x - 339688.1

R = 0.9058014486

3000000
2000000

4000000
3500000

1500000

f(x) = 82198.55x - 468923.75

R = 0.9482663066

3000000

kadar Vit C
2500000
0
2000000

1000000
500000
0
5

1500000

10 Column
15 C 20

1000000

25
30
Konsentrasi (p

500000
0
5

10

15

20

25 30 35
Axis Title

40

45

50

55

Chart Title
Axis Title

Axis Title

buang no2500000
3

5000000
4000000

f(x) = 88946.78x - 274201.79999999

R = 0.8671954007

3000000
2000000
1000000
0
5

10

15

20

25 30 35
Axis Title

40

45

urva Kalibrasi Kafein 1

x) = 82198.55x - 339688.1
= 0.9058014486

15 C 20
Column

25
30
35
Konsentrasi (ppm)

40

45

50

Chart Title

x) = 88946.78x - 274201.799999999
= 0.8671954007
Column C

15

20

25 30 35
Axis Title

40

45

50

55

55