FORMULIR

PENENTUAN UJI HOMOGENITAS SAMPEL AWAL

Uji Homogenitas Menurut ISO 13528

Parameter : Pengujian Kemurnian dalam sample Belerang
No. Data - 1 Data - 2 Xt,. Xt,. - Xr.,. (Xt,. - Xr.,.)2 Wt W t2
Kemasan %
1 0.0229 0.0254 0.0241 -0.0139 0.0002 0.0025 0.0000
2 0.0317 0.0271 0.0294 -0.0086 0.0001 0.0046 0.0000
3 0.0280 0.0400 0.0340 -0.0040 0.0000 0.0120 0.0001
4 0.0457 0.0339 0.0398 0.0018 0.0000 0.0118 0.0001
5 0.0620 0.0419 0.0520 0.0139 0.0002 0.0202 0.0004
6 0.0334 0.0351 0.0342 -0.0038 0.0000 0.0017 0.0000
7 0.0458 0.0595 0.0526 0.0146 0.0002 0.0137 0.0002
8 0.0000 0.0000
9 0.0000 0.0000
10 0.0000 0.0000

g 7 CVHorwitz = 21-0.5 log C

Xr.,. 0.04 Konsentrasi = 0.04 %
S(Xt,. - Xr.,.)2 0.001 C = 0.0003801181315
Sx 0.0108698 log C = -3.4200814142239
Sx2 0.00011815 0.5 log C = -1.710040707112
SWt2 0.00 1-0.5 log C = 2.710040707112
SW 0.00805134 21-0.5 log C = 6.5434010945929
SW2 6.48241E-05 CVHorwitz = 6.5434010945929 %
SW2/2 3.24121E-05 SHorwitz = 0.0024872653977 %
S 2
x - (S 2
W /2 ) 8.57405E-05 0.3 x SHorwitz = 0.0007461796193 %
SS 0.00925961

KESIMPULAN
SS > 0.3 σ
Sample Tidak Homogen

Disusun oleh : Diperiksa Oleh :

FOR/MIN-QA/150 Rev : 00 Tgl.berlaku : 01/02/2018 hal 1 dari 1 FOR/MIN-QA/150 Rev : 00

 Ash Content: Ash Content: Ash Content: Ash Content: Ash Content:
9.6252 10.6063 10.3428 10.7643 11.9591 9.3218 10.2627 11.3642 10.3795 11.1549
8.6251 9.6063 9.3427 9.7640 10.9590 8.3217 9.2625 10.3642 9.3795 10.1549
1.0001 1.0000 1.0001 1.0003 1.0001 1.0001 1.0002 1.0000 1.0000 1.0000
8.6469 9.6286 9.3645 9.7862 10.9803 8.3441 9.2852 10.3858 9.4035 10.1808
8.6316 9.6119 9.3487 9.7691 10.9645 8.3277 9.2691 10.3696 9.3849 10.1604
0.0153 0.0167 0.0158 0.0171 0.0158 0.0164 0.0161 0.0162 0.0186 0.0204
1.5298 1.6700 1.5798 1.7095 1.5798 1.6398 1.6097 1.6200 1.8600 2.0400
1.612 1.755 1.661 1.802 1.664 1.725 1.699 1.710 1.960 2.155

Ash Content: Ash Content: Ash Content: Ash Content: Ash Content:
11.4976 13.0522 10.9758 10.9860 11.0418 10.9626 10.5070 10.0997 11.3161 11.2685
10.4976 12.0522 9.9758 9.9859 10.0418 9.9626 9.5069 9.0995 10.3161 10.2683
1.0000 1.0000 1.0000 1.0001 1.0000 1.0000 1.0001 1.0002 1.0000 1.0002
10.5184 13.0739 9.9976 10.0080 10.0629 9.9844 9.5283 9.1223 10.3408 10.2937
10.5036 13.0586 9.9815 9.9921 10.0473 9.9670 9.5127 9.1053 10.3224 10.2737
0.0148 0.0153 0.0161 0.0159 0.0156 0.0174 0.0156 0.0170 0.0184 0.0200
1.4800 1.5300 1.6100 1.5898 1.5600 1.7400 1.5598 1.6997 1.8400 1.9996
1.558 1.608 1.694 1.675 1.644 1.832 1.643 1.792 1.938 2.107
 Moisture Content Moisture Content Moisture Content
28.802 33.0118 32.1435 32.0877 27.081 31.7691
1.5576 27.8019 32.0117 31.1435 31.0876 26.0809 30.7689
1.6083 28.7513 32.9634 32.0946 32.0364 27.0304 31.7198
1.6115 5.07 4.84 4.89 5.13 5.06 4.93
1.6430
1.6438
1.6611
1.6640
1.6751
1.6940 Moisture Content Moisture Content Moisture Content
1.6985 29.8128 28.5077 31.0607 31.3758 30.4331 30.3638
1.7105 28.8128 27.5076 30.0605 30.3757 29.433 29.3637
1.7249 29.7630 28.459 31.0111 31.3249 30.3821 30.3138
1.7549 4.98 4.87 4.96 5.09 5.10 5.00
1.7925
1.8019
1.8316
1.9385
1.9599
2.1070
2.1546
Moisture Content Moisture Content
31.5781 29.9312 30.5256 28.8019
30.5781 28.931 29.5255 27.8019
31.5258 29.8783 30.4746 28.7487
5.23 5.29 5.10 5.32

Moisture Content Moisture Content

30.598 28.0778 31.9598 29.8129
29.5977 27.0775 30.9598 28.8128
30.5474 28.026 31.9090 29.7619
5.06 5.18 5.08 5.10
 Moisture Content Moisture Content Moisture Content Moisture Content Moisture Content
28.802 33.0118 32.1435 32.0877 27.081 31.7691 31.5781 29.9312 30.5256
27.8019 32.0117 31.1435 31.0876 26.0809 30.7689 30.5781 28.931 29.5255
28.7513 32.9634 32.0946 32.0364 27.0304 31.7198 31.5258 29.8783 30.4746
5.07 4.84 4.89 5.13 5.06 4.93 5.23 5.29 5.10

Moisture Content Moisture Content Moisture Content Moisture Content Moisture Content
29.8128 28.5077 31.0607 31.3758 30.4331 30.3638 30.598 28.0778 31.9598
28.8128 27.5076 30.0605 30.3757 29.433 29.3637 29.5977 27.0775 30.9598
29.7630 28.459 31.0111 31.3249 30.3821 30.3138 30.5474 28.026 31.9090
4.98 4.87 4.96 5.09 5.10 5.00 5.06 5.18 5.08

Volatile Matter Volatile Matter Volatile Matter Volatile Matter Volatile Matter
14.8631 13.1007 14.8483 13.0309 14.9345 12.2778 15.0389 12.8531 12.2699
13.8630 12.1006 13.8482 12.0309 13.9345 11.2777 14.0388 11.8531 11.2697
14.6905 12.9329 14.6832 12.8607 14.7673 12.1195 14.8780 12.6871 12.1007
12.1888 11.9388 11.6183 11.8905 11.6605 10.8994 10.8584 11.3111 11.8171

Volatile Matter Volatile Matter Volatile Matter Volatile Matter Volatile Matter
12.4136 13.9449 14.1787 15.1868 13.3228 14.8654 14.3764 13.8490 14.8626
11.4136 12.9447 13.1786 14.1866 12.3227 13.8654 13.3763 12.849 13.8626
12.2454 13.7794 14.0096 15.0187 13.153 14.6964 14.2107 13.6816 14.6933
11.8400 11.6772 11.9493 11.7171 11.8788 11.9005 11.5099 11.5616 11.8500
Moisture Content
28.8019
27.8019
28.7487
5.32

Moisture Content
29.8129
28.8128
29.7619
5.10
10.8584
10.8994
11.3111
11.5099
11.5616
Volatile Matter 11.6183
13.3179 11.6605
12.3177 11.6772
13.1358 11.7171
12.8864 11.8171
11.8400
11.8500
Volatile Matter 11.8788
14.9276 11.8905
13.9276 11.9005
14.7554 11.9388
12.1205 11.9493
12.1205
12.1888
12.8864