FISHBONE
20 0.9236
25 1.1335 0.4
r 0.9997 0.2
slope 0.0454
0
intersep 0.0029
0 5 10kons(mg/L)
15 20 25 30
Data Sampel
Bobot Bobot Csampel Ctab
Sampel Abs Vol (L) Cterukur (mg/L)
sampel (kg) tablet (kg) (mg/Kg) (mg/tab)
1 0.4118 0.0000100 0.000225 0.10 9.0025 90024.95 20.26
2 0.4397 0.0000100 0.000225 0.10 9.6167 96167.23 21.64
3 0.4537 0.0000102 0.000225 0.10 9.9249 97303.32 21.89
y=a+bx
DATA KETIDAKPASTIAN ASL KURVA KALIBRASI (µReg)
Xi Yi Yc (Yi-Yc)2 (Xi-Xr)2
0 0.0115 0.0029 0.0000743 156.25
5 0.2259 0.2300 0.0000168 56.25
10 0.4418 0.4571 0.0002344 6.25
15 0.6877 0.6842 0.0000121 6.25
20 0.9236 0.9113 0.0001504 56.25
25 1.1335 1.1385 0.0000245 156.25
∑ 12.5 0.0005124 437.5000
n-2 4
RSD 0.0113181796449866
RSD/b 0.249173661828238
1+(1/n) 1.16666666666667
b 2
0.002063
yo 0.4351
yr 0.5707
(yo-yr)2
0.0184
Ö(1+(1/n)+((yo-yr)²/(b²*(xi-xr)²)))
1.08951215328209
µReg 0.271477732839667
KETIDAKPASTIAN GABUNGAN
Sumber Ketidakpastian satuan µXi Xi (µXi/Xi)²
Kurva kalibrasi mg/L 0.271477733 9.5147 0.0008141
Presisi Metode mg/kg 2260.69 94498 0.0005723
Volume sampel mL 0.134288247 100 0.0000018
Penimbangan gram 0.0002828 0.0101 0.0007894
S 0.0021777
µCs/Cs 0.0466653
µCs 4409.80153
u 8819.60306
Cs±u 94498±8820 mg/kg
9,45±0,90 %b/b
N