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LINEARITAS

Absorbansi
Konsentrasi (mg/L)
1 2 3 rata-rata
kurva kalibrasi
0 0.0000 0.0000 0.0000 0.0000 1.8000
5 0.2510 0.2520 0.2520 0.2517 1.6000
1.4000 f(x) = 0.064150476190476 x − 0.0497142857
10 0.5700 0.5700 0.5700 0.5700 R² = 0.995460917783646
15 0.8660 0.8660 0.8660 0.8660 1.2000

absorbansi
20 1.2220 1.2200 1.2200 1.2207 1.0000

25 1.6050 1.6050 1.6040 1.6047 0.8000

slope 0.0642 0.6000


0.4000
intersep (-) 0.0497
0.2000
R^2 0.9955
0.0000
r 0.9977 0 5 10 15
konsentrasi (ppm)

LOD dan LOQ


Konsentrasi (mg/L) y yi y-yi (y-yi)^2
0 0.0000 -0.0497 0.0497 0.0025
5 0.2517 0.2713 -0.0196 0.0004
10 0.5700 0.5923 -0.0223 0.0005
15 0.8660 0.9133 -0.0473 0.0022
20 1.2207 1.2343 -0.0136 0.0002
25 1.6047 1.5553 0.0494 0.0024
jumlah 0.0082
sy/x 0.0453
LOD 2.1174
LOQ 7.0581

PRESISI
Pengulanganabsorbansi Konsentrasikonsentrasi berat aspiri kadar aspirin dalam sampel (%) (b/b)
1 1.8330 29.3255 58.6511 5.8651 11.7302
2 1.8246 29.1947 58.3894 5.8389 11.6779
3 1.8463 29.5327 59.0654 5.9065 11.8131
4 1.8073 28.9252 57.8505 5.7850 11.5701
5 1.8376 29.3972 58.7944 5.8794 11.7589
6 1.8176 29.0857 58.1713 5.8171 11.6343
7 1.8480 29.5592 59.1184 5.9118 11.8237
kadar rerata 11.7154
SD 0.0935
%RSD 0.8

AKURASI
Pengulangan Absorbansi
Konsentrasi (mg/L)
% trueness Parameter Validasi
Nilai yang diukurNilai
1 1.5230 24.4969 Linearitas R^2 0.9955
2 1.5250 24.5280 122.54 LOD LOD 2,1174 mg/
3 1.5230 24.4969 LOQ LOQ 7,0581 mg/
rata-rata 24.5073 presisi %RSD 0.80%
µg
akurasi %Trueness 122.54%
kurva kalibrasi

4150476190476 x − 0.049714285714286
460917783646

10 15 20 25 30
konsentrasi (ppm)

pengulangan
% kadar kafein
1 11.7302
2 11.6779
3 11.8131
4 11.5701
fp 2 5 11.7589
v total 100 mL 6 11.6343
0.1 L 7 11.8237
massa sam 50 mg rata-rata 11.7154
SD 0.0935
%RSD 0.8

Kriteria penerimaan
P
P
P
P
O
Data Pengamatan

Penentuan Linearitas
Absorbansi
Konsentrasi (mg/L)
1 2 3 rata-rata
5 0.2510 0.2520 0.2520 0.2517
10 0.5700 0.5700 0.5700 0.5700
15 0.8660 0.8660 0.8660 0.8660
20 1.2220 1.2200 1.2200 1.2207
25 1.6050 1.6050 1.6040 1.6047

Penentuan Presisi
Absorbansi
Sampel
1 2 3 rata-rata
1 1.8320 1.8320 1.8350 1.8330
2 1.8250 1.8250 1.8240 1.8247
3 1.8450 1.8450 1.8490 1.8463
4 1.8070 1.8100 1.8050 1.8073
5 1.8370 1.8370 1.8390 1.8377
6 1.8150 1.8190 1.8190 1.8177
7 1.8460 1.8480 1.8500 1.8480

Penentuan Akurasi
Absorbansi
Standar (ppm)
1 2 3 rata-rata
20 1.5230 1.5250 1.5230 1.5237

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